Technical Papers
Oct 21, 2020

Characterization of Damage and Healing of Cement Matrices Based on Fly Ash under Repeated Loading

Publication: Journal of Materials in Civil Engineering
Volume 33, Issue 1

Abstract

This paper investigates damage and healing of cementitious materials based on fly ash (FA) with a special focus on the effect of repeated loading on the self-healing performance. In total, 90 prism specimens and 33 cylinder specimens were prepared and tested. Variables including the FA replacement ratio and preloading level were considered. Different methods were adopted to evaluate the self-healing performance, i.e., mechanical tests, acoustic emission (AE) analysis, water absorption measurement, and scanning electron microscope (SEM) observation. Test results revealed that an appropriate amount of cement replaced by FA was beneficial to the self-healing performance of the specimens subjected to a high level of repeated preloading, where the strength increased by 11% and the water absorption rate decreased by 12%, in comparison with that of the undamaged specimens. This was attributed to the active hydration of FA, which was confirmed by an energy dispersive X-ray spectroscopy (EDS) analysis. This study extends understanding of the self-healing performance when subjected to repeated loading and provides some useful suggestions for the self-healing technique based on mineral additives.

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Data Availability Statement

All data, models, and code generated or used during the study appear in the published article.

Acknowledgments

The authors gratefully acknowledge the financial supports provided by the National Natural Science Foundation of China (Nos. 51878485 and 51938013) and the Top Interdisciplinary Funds of Civil Engineering for Tongji University. Thanks also go to Professor Xiang-Lin Gu for his guidance. Furthermore, the help from undergraduate students Lian-Zhi Zhang and Rui-Qi Deng is appreciated.

References

Ahn, T. H., and T. Kishi. 2010. “Crack self-healing behavior of cementitious composites incorporating various mineral admixtures.” J. Adv. Concr. Technol. 8 (2): 171–186. https://doi.org/10.3151/jact.8.171.
ASTM. 2013. Standard test method for measurement of rate of absorption of water by hydraulic-cement concretes. ASTM C1585. West Conshohocken, PA: ASTM.
Blaiszik, B. J., M. M. Caruso, D. A. McIlroy, J. S. Moore, S. R. White, and N. R. Sottos. 2009. “Microcapsules filled with reactive solutions for self-healing materials.” Polymer 50 (4): 990–997. https://doi.org/10.1016/j.polymer.2008.12.040.
Castro, J., D. Bentz, and J. Weiss. 2011. “Effect of sample conditioning on the water absorption of concrete.” Cem. Concr. Compos. 33 (8): 805–813. https://doi.org/10.1016/j.cemconcomp.2011.05.007.
Chahal, N., R. Siddique, and A. Rajor. 2012. “Influence of bacteria on the compressive strength, water absorption and rapid chloride permeability of fly ash concrete.” Constr. Build. Mater. 28 (1): 351–356. https://doi.org/10.1016/j.conbuildmat.2011.07.042.
De Rooij, M., K. Van Tittelboom, N. De Belie, and E. Schlangen. 2011. Self-healing phenomena in cement-based materials. Dordrecht, Netherlands: Springer.
Dong, B. Q., G. H. Fang, Y. S. Wang, Y. Q. Liu, S. X. Hong, J. C. Zhang, S. M. Lin, and F. Xing. 2017. “Performance recovery concerning the permeability of concrete by means of a microcapsule based self-healing system.” Cem. Concr. Compos. 78 (Apr): 84–96. https://doi.org/10.1016/j.cemconcomp.2016.12.005.
Edvardsen, C. 1999. “Water permeability and autogenous healing of cracks in concrete.” ACI Mater. J. 96 (4): 448–454.
Fan, S., and M. Li. 2014. “X-ray computed microtomography of three-dimensional microcracks and self-healing in engineered cementitious composites.” Smart Mater. Struct. 24 (1): 015021. https://doi.org/10.1088/0964-1726/24/1/015021.
General Administration of Quality Supervision, Inspection, and Quarantine of the People’s Republic of China. 2007. Common portland cement. GB 175-2007. Beijing: General Administration of Quality Supervision, Inspection, and Quarantine of the People’s Republic of China.
Granger, S., A. Loukili, G. Pijaudier-Cabot, and G. Chanvillard. 2007. “Experimental characterization of the self-healing of cracks in an ultra high performance cementitious material: Mechanical tests and acoustic emission analysis.” Cem. Concr. Res. 37 (4): 519–527. https://doi.org/10.1016/j.cemconres.2006.12.005.
Hearn, N. 1996. “Effect of shrinkage and load-induced cracking on water permeability of concrete.” ACI Mater. J. 96 (2): 234–241.
Hearn, N. 1998. “Self-sealing, autogenous healing and continued hydration: What is the difference?” Mater. Struct. 31 (8): 563. https://doi.org/10.1007/BF02481539.
Hearn, N., and G. Lok. 1998. “Measurement of permeability under uniaxial compression: A test method.” ACI Mater. J. 95 (6): 691–694.
Jiang, Z. W., Z. C. Yuan, and W. T. Li. 2019. “Acoustic emission analysis of characteristics of healing products in steam-cured cementitious materials with mineral additives.” Constr. Build. Mater. 201 (Mar): 807–817. https://doi.org/10.1016/j.conbuildmat.2018.12.140.
Kaiser, J. 1950. “A study of acoustic phenomena in tensile tests.” Ph.D. dissertation, Dept. of Maschinenwesen und Elektrotchnik, Technical Univ. of Munich.
Keskin, S. B., O. K. Keskin, O. Anil, M. Şahmaran, A. Alyousif, M. Lachemi, L. Amleh, and A. F. Ashour. 2016. “Self-healing capability of large-scale engineered cementitious composites beams.” Composites, Part B. 101 (Sep): 1–13. https://doi.org/10.1016/j.compositesb.2016.06.073.
Li, W. T., Z. W. Jiang, and Z. H. Yang. 2017. “Acoustic characterization of damage and healing of microencapsulation-based self-healing cement matrices.” Cem. Concr. Compos. 84 (Nov): 48–61. https://doi.org/10.1016/j.cemconcomp.2017.08.013.
Li, W. T., Z. W. Jiang, and Q. Q. Yu. 2020. “Multiple damaging and self-healing properties of cement paste incorporating microcapsules.” Constr. Build. Mater. 255 (Sep): 119302. https://doi.org/10.1016/j.conbuildmat.2020.119302.
Liu, X., X. Sheng, J. K. Lee, and M. R. Kessler. 2009. “Synthesis and characterization of melamine-urea-formaldehyde microcapsules containing ENB-based self-healing agents.” Macromol. Mater. Eng. 294 (6–7): 389–395. https://doi.org/10.1002/mame.200900015.
Malhotra, V. M., M. H. Zhang, P. H. Read, and J. Ryell. 2000. “Long-term mechanical properties and durability characteristics of high-strength/high-performance concrete incorporating supplementary cementing materials under outdoor exposure conditions.” ACI Mater. J. 97 (5): 518–525.
Maltais, Y., and J. Marchand. 1997. “Influence of curing temperature on cement hydration and mechanical strength development of fly ash mortars.” Cem. Concr. Res. 27 (7): 1009–1020. https://doi.org/10.1016/S0008-8846(97)00098-7.
Martin, L. H. J., F. Winnefeld, E. Tschopp, C. J. Müller, and B. Lothenbach. 2017. “Influence of fly ash on the hydration of calcium sulfoaluminate cement.” Cem. Concr. Res. 95 (May): 152–163. https://doi.org/10.1016/j.cemconres.2017.02.030.
Ministry of Housing and Urban-Rural Development of the People’s Republic of China. 2002. Standard for test method of mechanical properties on ordinary concrete. GB/T 50081-2002. Beijing: Ministry of Housing and Urban-Rural Development of the People’s Republic of China.
Mohammed, T. U., N. Otsuki, M. Hisada, and T. Shibata. 2001. “Effect of crack width and bar types on corrosion of steel in concrete.” J. Mater. Civ. Eng. 13 (3): 194–201. https://doi.org/10.1061/(ASCE)0899-1561(2001)13:3(194).
Öztürk, O., G. Yıldırım, Ü. S. Keskin, H. Siad, and M. Sahmaran. 2020. “Nano-tailored multi-functional cementitious composites.” Composites, Part B 182 (Feb): 107670. https://doi.org/10.1016/j.compositesb.2019.107670.
Pour-Ghaz, M., and J. Weiss. 2010. “Quantifying damage due to aggregate expansion in cement matrix.” ACI Spec. Publ. 270: 101–114.
Qian, S., J. Zhou, M. R. De Rooij, E. Schlangen, G. Ye, and K. van Breugel. 2009. “Self-healing behavior of strain hardening cementitious composites incorporating local waste materials.” Cem. Concr. Compos. 31 (9): 613–621. https://doi.org/10.1016/j.cemconcomp.2009.03.003.
Qian, S. Z., J. Zhou, and E. Schlangen. 2010. “Influence of curing condition and precracking time on the self-healing behavior of engineered cementitious composites.” Cem. Concr. Compos. 32 (9): 686–693. https://doi.org/10.1016/j.cemconcomp.2010.07.015.
Roig-Flores, M., S. Moscato, P. Serna, and L. Ferrara. 2015. “Self-healing capability of concrete with crystalline admixtures in different environments.” Constr. Build. Mater. 86 (Jul): 1–11. https://doi.org/10.1016/j.conbuildmat.2015.03.091.
Sahmaran, M., G. Yildirim, G. H. Aras, S. B. Keskin, O. K. Keskin, and M. Lachemi. 2017. “Self-healing of cementitious composites to reduce high CO2 emissions.” ACI Mater. J. 114(1): 93–104.
Şahmaran, M., S. B. Keskin, G. Ozerkan, and I. O. Yaman. 2008. “Self-healing of mechanically-loaded self consolidating concretes with high volumes of fly ash.” Cem. Concr. Compos. 30 (10): 872–879. https://doi.org/10.1016/j.cemconcomp.2008.07.001.
Şahmaran, M., and V. C. Li. 2009. “Durability properties of micro-cracked ECC containing high volumes fly ash.” Cem. Concr. Res. 39 (11): 1033–1043.
Şahmaran, M., G. Yildirim, and T. K. Erdem. 2013. “Self-healing capability of cementitious composites incorporating different supplementary cementitious materials.” Cem. Concr. Compos. 35 (1): 89–101.
Şahmaran, M., G. Yildirim, R. Noori, E. Ozbay, and M. Lachemi. 2015. “Repeatability and pervasiveness of self-healing in engineered cementitious composites.” ACI Mater. J. 112 (4): 513–522.
Samaha, H. R., and K. C. Hover. 1992. “Influence of microcracking on the mass transport properties of concrete.” ACI Mater. J. 89 (4): 416–424.
Siad, H., M. Lachemi, M. Sahmaran, and K. M. A. Hossain. 2017. “Mechanical, physical, and self-healing behaviors of engineered cementitious composites with glass powder.” J. Mater. Civ. Eng. 29 (6): 4017016. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001864.
Siad, H., M. Lachemi, M. Sahmaran, and K. M. A. Hossain. 2018. “Advanced engineered cementitious composites with combined self-sensing and self-healing functionalities.” Constr. Build. Mater. 176 (Jul): 313–322. https://doi.org/10.1016/j.conbuildmat.2018.05.026.
Snoeck, D., and N. De Belie. 2016. “Repeated autogenous healing in strain-hardening cementitious composites by using superabsorbent polymers.” J. Mater. Civ. Eng. 28 (1): 04015086. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001360.
Snoeck, D., K. Van Tittelboom, S. Steuperaert, P. Dubruel, and N. De Belie. 2014. “Self-healing cementitious materials by the combination of microfibres and superabsorbent polymers.” J. Intell. Mater. Syst. Struct. 25 (1): 13–24. https://doi.org/10.1177/1045389X12438623.
Souradeep, G., and H. W. Kua. 2016. “Encapsulation technology and techniques in self-healing concrete.” J. Mater. Civ. Eng. 28 (12): 04016165. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001687.
Sugiyama, T., T. W. Bremner, and T. A. Holm. 1996. “Effect of stress on gas permeability in concrete.” ACI Mater. J. 93 (5): 443–450.
Swamy, R. N., S. A. R. Ali, and D. D. Theodorakopoulos. 1983. “Early strength fly-ash concrete for structural applications.” ACI J. Proc. 80 (5): 414–423.
Ter Heide, N., and E. Schlangen. 2007. “Self-healing of early age cracks in concrete.” In Proc., 1st Int. Conf. on Self Healing Materials. Dordrecht, Netherlands: Springer.
Termkhajornkit, P., T. Nawa, and K. Kurumisawa. 2006. “Effect of water curing conditions on the hydration degree and compressive strengths of fly ash-cement paste.” Cem. Concr. Compos. 28 (9): 781–789. https://doi.org/10.1016/j.cemconcomp.2006.05.018.
Termkhajornkit, P., T. Nawa, Y. Yamashiro, and T. Saito. 2009. “Self-healing ability of fly ash-cement systems.” Cem. Concr. Compos. 31 (3): 195–203. https://doi.org/10.1016/j.cemconcomp.2008.12.009.
Thao, T. D. P., T. J. S. Johnson, Q. S. Tong, and P. S. Dai. 2009. “Implementation of self-healing in concrete—Proof of concept.” IES J. Part A: Civ. Struct. Eng. 2 (2): 116–125. https://doi.org/10.1080/19373260902843506.
Van Der Zwaag, S. 2007. Self-healing materials: An alternative approach to 20 centuries of materials science. Dordrecht, Netherlands: Springer.
Van Tittelboom, K., and N. De Belie. 2013. “Self-healing in cementitious materials-A review.” Materials 6 (6): 2182–2217. https://doi.org/10.3390/ma6062182.
Van Tittelboom, K., N. De Belie, D. Van Loo, and P. Jacobs. 2011. “Self-healing efficiency of cementitious materials containing tubular capsules filled with healing agent.” Cem. Concr. Compos. 33 (4): 497–505. https://doi.org/10.1016/j.cemconcomp.2011.01.004.
Van Tittelboom, K., E. Gruyaert, H. Rahier, and N. De Belie. 2012. “Influence of mix composition on the extent of autogenous crack healing by continued hydration or calcium carbonate formation.” Constr. Build. Mater. 37 (Dec): 349–359. https://doi.org/10.1016/j.conbuildmat.2012.07.026.
Wang, J. Y., N. De Belie, and W. Verstraete. 2012. “Diatomaceous earth as a protective vehicle for bacteria applied for self-healing concrete.” J. Ind. Microbiol. Biotechnol. 39 (4): 567–577. https://doi.org/10.1007/s10295-011-1037-1.
Wang, J. Y., D. Snoeck, S. Van Vlierberghe, W. Verstraete, and N. De Belie. 2014. “Application of hydrogel encapsulated carbonate precipitating bacteria for approaching a realistic self-healing in concrete.” Constr. Build. Mater. 68 (Oct): 110–119. https://doi.org/10.1016/j.conbuildmat.2014.06.018.
Yang, Y. Z., M. D. Lepech, E. H. Yang, and V. C. Li. 2009. “Autogenous healing of engineered cementitious composites under wet-dry cycles.” Cem. Concr. Res. 39 (5): 382–390. https://doi.org/10.1016/j.cemconres.2009.01.013.
Yildirim, G., G. H. Aras, Q. S. Banyhussan, M. Sahmaran, and M. Lachemi. 2015a. “Estimating the self-healing capability of cementitious composites through non-destructive electrical-based monitoring.” NDT E Int. 76 (Dec): 26–37. https://doi.org/10.1016/j.ndteint.2015.08.005.
Yildirim, G., H. Hamidzadeh, S. Yesilmen, and M. Sahmaran. 2018. “Self-healing performance of aged cementitious composites.” Cem. Concr. Compos. 87 (Feb): 172–186.
Yildirim, G., O. K. Keskin, S. B. Keskin, M. Sahmaran, and M. Lachemi. 2015b. “A review of intrinsic self-healing capability of engineered cementitious composites: Recovery of transport and mechanical properties.” Constr. Build. Mater. 101: 10–21.
Yildirim, G., M. Sahmaran, and H. U. Ahmed. 2015c. “Influence of hydrated lime addition on the self-healing capability of high-volume fly ash incorporated cementitious composites.” J. Mater. Civ. Eng. 27 (6): 04014187. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001145.
Zhang, Z. G., S. Z. Qian, and H. Ma. 2014. “Investigating mechanical properties and self-healing behavior of micro-cracked ECC with different volume of fly ash.” Constr. Build. Mater. 52 (Feb): 17–23. https://doi.org/10.1016/j.conbuildmat.2013.11.001.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 33Issue 1January 2021

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Received: Feb 10, 2020
Accepted: Jun 24, 2020
Published online: Oct 21, 2020
Published in print: Jan 1, 2021
Discussion open until: Mar 21, 2021

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Zhen-Yu Chen [email protected]
Graduate Student, Key Laboratory of Performance Evolution and Control for Engineering Structures, Ministry of Education, Tongji Univ., Shanghai 200092, China; Dept. of Structural Engineering, Tongji Univ., Shanghai 200092, China. Email: [email protected]
Associate Researcher, Key Laboratory of Advanced Civil Engineering Materials, Ministry of Education, Tongji Univ., Shanghai 201804, China. Email: [email protected]
Associate Professor, Key Laboratory of Performance Evolution and Control for Engineering Structures, Ministry of Education, Tongji Univ., Shanghai 200092, China; Dept. of Structural Engineering, Tongji Univ., Shanghai 200092, China (corresponding author). ORCID: https://orcid.org/0000-0003-1772-3195. Email: [email protected]

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