Technical Papers
Oct 31, 2022

Impact of Laboratory Long-Term Aging Procedures on Intermediate-Temperature Behavior of Asphalt Binders in Asphalt Fine Aggregate Matrix Mixtures

Publication: Journal of Transportation Engineering, Part B: Pavements
Volume 149, Issue 1

Abstract

The durability of asphalt mixtures and flexible pavements are closely related to the properties of the asphalt fine aggregate matrix (FAM) with aging. However, there are still no uniform aging procedures specified for laboratory-prepared FAM. In this study, the intermediate-temperature behavior of FAM under various accelerated aging procedures was investigated at the binder scale to reveal the influence of the FAM aging. Three different long-term aging procedures were considered, including loose mixes aging (95°C and 135°C) and pressure aging vessel (PAV) protocols. Frequency sweep test and linear amplitude sweep (LAS) test were carried out on binders extracted from aged FAMs. Rheological tests were also performed on corresponding binders with standard PAV procedure to show the impact of FAM during the aging process. Moreover, an aging kinetics model was put forward to qualify the linear rheological property evolutions for fast and constant aging reaction stages under various aging conditions. The results show that 135°C loose FAM mixes aging significantly reduces the fatigue performance of styrene-butadiene-styrene (SBS) modified binder, and employing 95°C loose mixes aging and PAV aging procedures can avoid this adverse effect. Moreover, to match the aging degree of asphalt and FAM, an aging duration more than 40 h is recommended.

Get full access to this article

View all available purchase options and get full access to this article.

Data Availability Statement

All data, models, and code generated or used during the study appear in the published article.

References

AASHTO. 2015. Standard practice for mixture conditioning of hot-mixasphalt (HMA). AASHTO R 30-02. Washington, DC: AASHTO.
AASHTO. 2018. Standard method of test for estimating fatigue resistance of asphalt binder using the linear amplitude sweep. American association of state highway and transportation officials. ASHTO TP 101-18. Washington, DC: AASHTO.
AI (Asphalt Institute). 2003. Superpave performance graded asphalt binder specification and testing. Superpave Series No. 1(SP-1). Lexington, KY: AI.
Asadi, B., N. Tabatabaee, and R. Hajj. 2021. “Use of linear amplitude sweep test as a damage tolerance or fracture test to determine the optimum content of asphalt rejuvenator.” Constr. Build. Mater. 300 (Sep): 123983. https://doi.org/10.1016/j.conbuildmat.2021.123983.
ASTM. 2015. Standard test method for viscosity determination of asphaltat elevated temperatures using a rotational viscometer. ASTM D4402/D4402M. West Conshohocken, PA: ASTM.
ASTM. 2017. Standard practice for recovery of asphalt from solution using the rotary evaporator. ASTM D5404M. West Conshohocken, PA: ASTM.
Bahia, H. U., H. Zhai, M. Zeng, Y. Hu, and P. Turner. 2002. “Development of binder specification parameters based on characterization of damage behavior. J. Assoc. Asphalt Paving Technol. 70: 442–470.
Cao, W., and C. Wang. 2018. “A new comprehensive analysis framework for fatigue characterization of asphalt binder using the Linear Amplitude Sweep test.” Constr. Build. Mater. 171 (May): 1–12. https://doi.org/10.1016/j.conbuildmat.2018.03.125.
Chen, H., Y. Zhang, and H. U. Bahia. 2021. “Estimating asphalt binder fatigue at multiple temperatures using a simplified pseudo-strain energy analysis approach in the LAS test.” Constr. Build. Mater. 266 (Part A): 120911. https://doi.org/10.1016/j.conbuildmat.2020.120911.
Diab, A., and Z. You. 2017. “Small and large strain rheological characterizations of polymer-and crumb rubber-modified asphalt binders.” Constr. Build. Mater. 144 (Jul): 168–177. https://doi.org/10.1016/j.conbuildmat.2017.03.175.
Ding, J., J. Jiang, F. Ni, Q. Dong, and Z. Zhao. 2020. “Correlation investigation of fatigue indices of fine aggregate matrix (FAM) and asphalt mixture containing reclaimed asphalt pavement materials.” Constr. Build. Mater. 262 (Nov): 120646. https://doi.org/10.1016/j.conbuildmat.2020.120646.
Elwardany, M. D., F. Yousefi Rad, C. Castorena, and Y. R. Kim. 2017. “Evaluation of asphalt mixture laboratory long-term ageing methods for performance testing and prediction.” Supplement, Road Mater. Pavement Des. 18 (S1): 28–61. https://doi.org/10.1080/14680629.2016.1266740.
Farrar, M. J., T. F. Turner, J.-P. Planche, J. F. Schabron, and P. M. Harnsberger. 2013. “Evolution of the crossover modulus with oxidative aging: Method to estimate change in viscoelastic properties of asphalt binder with time and depth on the road.” Transp. Res. Rec. 2370 (1): 76–83. https://doi.org/10.3141/2370-10.
Glaser, R. R., J. F. Schabron, T. F. Turner, J.-P. Planche, S. L. Salmans, and J. L. Loveridge. 2013. “Low-and intermediate-temperature behaviour of polymer-modified asphalt binders, mastics, fine aggregate matrices, and mixtures with reclaimed asphalt pavement material.” Transp. Res. Rec. 2370 (1): 63–68. https://doi.org/10.3141/2370-08.
Gong, X., P. Romero, Z. Dong, and Y. Li. 2017. “Investigation on the low temperature property of asphalt fine aggregate matrix and asphalt mixture including the environmental factors.” Constr. Build. Mater. 156 (Dec): 56–62. https://doi.org/10.1016/j.conbuildmat.2017.08.142.
Gudipudi, P., and B. S. Underwood. 2015. “Testing and modeling of fine aggregate matrix and its relationship to asphalt concrete mix.” Transp. Res. Rec. 2507 (1): 120–127. https://doi.org/10.3141/2507-13.
He, Y., M. Z. Alavi, D. Jones, and J. Harvey. 2016. “Proposing a solvent-free approach to evaluate the properties of blended binders in asphalt mixes containing high quantities of reclaimed asphalt pavement and recycled asphalt shingles.” Constr. Build. Mater. 114 (Jul): 172–180. https://doi.org/10.1016/j.conbuildmat.2016.03.074.
Hintz, C., and H. Bahia. 2013. “Simplification of linear amplitude sweep test and specification parameter.” Transp. Res. Rec. 2370 (1): 10–16. https://doi.org/10.3141/2370-02.
Jing, R., A. Varveri, X. Liu, A. Scarpas, and S. Erkens. 2020. “Rheological, fatigue and relaxation properties of aged bitumen.” Int. J. Pavement Eng. 21 (8): 1024–1033. https://doi.org/10.1080/10298436.2019.1654609.
Kim, Y. R., C. Castorena, N. F. Saleh, E. Braswell, M. Elwardany, and F. Y. Rad. 2020. Long-term aging of asphalt mixtures for performance testing and prediction: Phase III results. NCHRP Research Rep. No. 871. Washington, DC: TRB Publications. https://doi.org/10.17226/26133.
Kim, Y. R., C. Castorena, N. F. Saleh, E. Braswell, M. Elwardany, and F. Y. Rad. 2021. Long-term aging of asphalt mixtures for performance testing and prediction: Phase III results. Washington, DC: Transportation Research Board.
Lenz, R. W. 1967. Organic chemistry of synthetic high polymers. New York: Interscience Publ.
Liu, F., Z. Zhou, and Y. Wang. 2019. “Predict the rheological properties of aged asphalt binders using a universal kinetic model.” Constr. Build. Mater. 195 (Jan): 283–291. https://doi.org/10.1016/j.conbuildmat.2018.11.025.
Liu, F., Z. Zhou, and X. Zhang. 2021. “Linking chemical to rheological properties of asphalt binder with oxidative aging effect.” Road Mater. Pavement Des. 22 (9): 2014–2028. https://doi.org/10.1080/14680629.2020.1740770.
Liu, M., K. Lunsford, R. Davison, C. Glover, and J. Bullin. 1996. “The kinetics of carbonyl formation in asphalt.” AIChE J. 42 (4): 1069–1076. https://doi.org/10.1002/aic.690420417.
Ningappa, A., and S. Suresha. 2020. “Laboratory evaluation of long-term aging effect on linear viscoelastic and fatigue properties of FAM mixtures.” Constr. Build. Mater. 241 (Apr): 118087. https://doi.org/10.1016/j.conbuildmat.2020.118087.
Petersen, J. C. 2000. “Chemical composition of asphalt as related to asphalt durability.” In Developments in petroleum science, 363–399. Amsterdam, Netherlands: Elsevier.
Petersen, J. C. 2009. “A review of the fundamentals of asphalt oxidation: Chemical, physicochemical, physical property, and durability relationships.” Transp. Res. Circular (Oct): 01141704. https://doi.org/10.17226/23002.
Petersen, J. C., and R. Glaser. 2011. “Asphalt oxidation mechanisms and the role of oxidation products on age hardening revisited.” Road Mater. Pavement Des. 12 (4): 795–819. https://doi.org/10.1080/14680629.2011.9713895.
Petersen, J. C., P. M. Harnsberger, and R. E. Robertson. 1996. “Factors affecting the kinetics and mechanisms of asphalt oxidation and the relative effects of oxidation products on age hardening.” In Vol. 41 of American chemical society, division of fuel chemistry. Washington, DC: American Chemical Society.
Poulikakos, L., D. Wang, L. Porot, and B. Hofko. 2019. “Impact of asphalt aging temperature on chemo-mechanics.” RSC Adv. 9 (21): 11602–11613. https://doi.org/10.1039/C9RA00645A.
Qin, Q., J. F. Schabron, R. B. Boysen, and M. J. Farrar. 2014. “Field aging effect on chemistry and rheology of asphalt binders and rheological predictions for field aging.” Fuel 121 (Apr): 86–94. https://doi.org/10.1016/j.fuel.2013.12.040.
Rad, F. Y., M. D. Elwardany, C. Castorena, and Y. R. Kim. 2017. “Investigation of proper long-term laboratory aging temperature for performance testing of asphalt concrete.” Constr. Build. Mater. 147 (Aug): 616–629. https://doi.org/10.1016/j.conbuildmat.2017.04.197.
Rahbar-Rastegar, R., R. Zhang, J. E. Sias, and E. V. Dave. 2019. “Evaluation of laboratory ageing procedures on cracking performance of asphalt mixtures.” Supplement, Road Mater. Pavement Des. 20 (S2): S647–S662. https://doi.org/10.1080/14680629.2019.1633782.
Sabouri, M., D. Mirzaiyan, and A. Moniri. 2018. “Effectiveness of linear amplitude sweep (LAS) asphalt binder test in predicting asphalt mixtures fatigue performance.” Constr. Build. Mater. 171 (May): 281–290. https://doi.org/10.1016/j.conbuildmat.2018.03.146.
Safaei, F., and C. Castorena. 2016. “Temperature effects of linear amplitude sweep testing and analysis.” Transp. Res. Rec. 2574 (1): 92–100. https://doi.org/10.3141/2574-10.
Safaei, F., C. Castorena, and Y. R. Kim. 2016. “Linking asphalt binder fatigue to asphalt mixture fatigue performance using viscoelastic continuum damage modeling.” Mech. Time-Depend. Mater. 20 (3): 299–323. https://doi.org/10.1007/s11043-016-9304-1.
Safaei, F., J.-S. Lee, L. A. H. D. Nascimento, C. Hintz, and Y. R. Kim. 2014. “Implications of warm-mix asphalt on long-term oxidative ageing and fatigue performance of asphalt binders and mixtures.” Supplement, Road Mater. Pavement Des. 15 (S1): 45–61. https://doi.org/10.1080/14680629.2014.927050.
Schapery, R. 1987. “Deformation and fracture characterization of inelastic composite materials using potentials.” Polym. Eng. Sci. 27 (1): 63–76. https://doi.org/10.1002/pen.760270110.
Shu, X., B. Huang, and D. Vukosavljevic. 2008. “Laboratory evaluation of fatigue characteristics of recycled asphalt mixture.” Constr. Build. Mater. 22 (7): 1323–1330. https://doi.org/10.1016/j.conbuildmat.2007.04.019.
Sirin, O., M. Ohiduzzaman, E. Kassem, and D. K. Paul. 2020. “Comprehensive evaluation of long-term aging of asphalt mixtures in hot climatic condition.” Road Mater. Pavement Des. 21 (4): 927–949. https://doi.org/10.1080/14680629.2018.1531777.
Sreeram, A., Z. Leng, Y. Zhang, and R. K. Padhan. 2018. “Evaluation of RAP binder mobilisation and blending efficiency in bituminous mixtures: An approach using ATR-FTIR and artificial aggregate.” Constr. Build. Mater. 179 (Aug): 245–253. https://doi.org/10.1016/j.conbuildmat.2018.05.154.
Underwood, B. S., and Y. R. Kim. 2013. “Microstructural investigation of asphalt concrete for performing multiscale experimental studies.” Int. J. Pavement Eng. 14 (5): 498–516. https://doi.org/10.1080/10298436.2012.746689.
Wang, C., C. Castorena, J. Zhang, and Y. Richard Kim. 2015. “Unified failure criterion for asphalt binder under cyclic fatigue loading.” Supplement, Road Mater. Pavement Des. 16 (S2): 125–148. https://doi.org/10.1080/14680629.2015.1077010.
Wang, D., D. Li, J. Yan, Z. Leng, Y. Wu, J. Yu, and H. Yu. 2018. “Rheological and chemical characteristic of warm asphalt rubber binders and their liquid phases.” Constr. Build. Mater. 193 (Dec): 547–556. https://doi.org/10.1016/j.conbuildmat.2018.10.199.
Wang, Y., and Y. Richard Kim. 2017. “Development of a pseudo strain energy-based fatigue failure criterion for asphalt mixtures.” Int. J. Pavement Eng. 20 (10): 1182–1192. https://doi.org/10.1080/10298436.2017.1394100.
Wen, H., and H. Bahia. 2009. “Characterizing fatigue of asphalt binders with viscoelastic continuum damage mechanics.” Transp. Res. Rec. 2126 (1): 55–62. https://doi.org/10.3141/2126-07.
Yan, C., W. Huang, P. Lin, Y. Zhang, and Q. Lv. 2019. “Chemical and rheological evaluation of aging properties of high content SBS polymer modified asphalt.” Fuel 252 (Sep): 417–426. https://doi.org/10.1016/j.fuel.2019.04.022.
Zhang, H., Z. Chen, G. Xu, and C. Shi. 2018. “Evaluation of aging behaviors of asphalt binders through different rheological indices.” Fuel 221 (Jun): 78–88. https://doi.org/10.1016/j.fuel.2018.02.087.
Zhang, R., J. E. Sias, and E. V. Dave. 2021. “Development of a rheology-based mixture aging model for asphalt material cracking performance evaluation.” Mater. Struct. 54 (4): 150. https://doi.org/10.1617/s11527-021-01743-5.
Zhang, R., J. E. Sias, E. V. Dave, and R. Rahbar-Rastegar. 2019. “Impact of aging on the viscoelastic properties and cracking behavior of asphalt mixtures.” Transp. Res. Rec. 2673 (6): 406–415. https://doi.org/10.1177/0361198119846473.
Zhou, Z., X. Gu, Q. Dong, F. Ni, and Y. Jiang. 2020. “Low-and intermediate-temperature behaviour of polymer-modified asphalt binders, mastics, fine aggregate matrices, and mixtures with reclaimed asphalt pavement material.” Road Mater. Pavement Des. 21 (7): 1872–1901. https://doi.org/10.1080/14680629.2019.1574233.

Information & Authors

Information

Published In

Go to Journal of Transportation Engineering, Part B: Pavements
Journal of Transportation Engineering, Part B: Pavements
Volume 149Issue 1March 2023

History

Received: Oct 28, 2021
Accepted: Jul 10, 2022
Published online: Oct 31, 2022
Published in print: Mar 1, 2023
Discussion open until: Mar 31, 2023

Permissions

Request permissions for this article.

Authors

Affiliations

Jitong Ding, Ph.D. [email protected]
Candidate, 422 School of Transportation, Southeast Univ., 2 Southeast University Rd., Jiangning District, Nanjing, Jiangsu 211189, China. Email: [email protected]
Yajin Han, Ph.D. [email protected]
Candidate, 422 School of Transportation, Southeast Univ., 2 Southeast University Rd., Jiangning District, Nanjing, Jiangsu 211189, China. Email: [email protected]
Qipeng Zhang, Ph.D. [email protected]
Candidate, 422 School of Transportation, Southeast Univ., 2 Southeast University Rd., Jiangning District, Nanjing, Jiangsu 211189, China. Email: [email protected]
Jiwang Jiang, Ph.D. [email protected]
Postdoctoral Research Fellow, 422 School of Transportation, Southeast Univ., 2 Southeast University Rd., Jiangning District, Nanjing, Jiangsu 211189, China. Email: [email protected]
Fujian Ni, Ph.D. [email protected]
Professor, 406 School of Transportation, Southeast Univ., 2 Southeast University Rd., Jiangning District, Nanjing, Jiangsu 211189, China (corresponding author). Email: [email protected]
Xiang Ma, Ph.D. [email protected]
Associate Professor, College of Civil Engineering, Nanjing Forestry Univ., 159# Longpan, Nanjing 210037, China. Email: [email protected]

Metrics & Citations

Metrics

Citations

Download citation

If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.

View Options

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Media

Figures

Other

Tables

Share

Share

Copy the content Link

Share with email

Email a colleague

Share