Technical Papers
Nov 25, 2023

Self-Sensing Stress-Absorption Layer with Carbon Nanotubes Grafted onto Basalt Fibers

Publication: Journal of Materials in Civil Engineering
Volume 36, Issue 2

Abstract

Fiber-reinforced emulsified asphalt (FEA) is widely used in asphalt pavement structures as a stress-absorption layer. This study aimed at developing a multifunctional fiber-reinforced emulsified asphalt (MFEA) by empowering the FEA with the self-sensing ability. To achieve this purpose, carbon nanotubes (CNTs) were grafted onto the basalt fibers in the FEA. An optical microscope and scanning electron microscope (SEM) were respectively used to investigate the distribution of CNTs onto the fibers and the microstructure of CNT/fiber composite (CFC). The fabrication process of CFC was optimized based on the distribution homogeneity of the CNTs. The self-sensing ability of the MFEA was then evaluated in the laboratory using an electrochemical workstation. Based on the experimental and analytical results, 1.5  mg/mL was recommended as the optimal dosage of the suspension of CNTs for grafting CNTs onto the fiber. The electrical resistance of the developed MFEA was found to be isotropic and sensitive to the demulsification state, EA/CFC mass ratio, temperature, loading speed, and deformation magnitude, which confirms the potential of using developed MFEA as a self-sensing layer to monitor its response to environmental and traffic variation. Besides, the direct tension and pull-out tests indicate the positive influence of grafting CNTs onto basalt fibers on the mechanical performance of FEA.

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Data Availability Statement

Some or all data, models, or code that support the findings of this study are available from the corresponding author upon reasonable request.

Acknowledgments

The authors highly appreciate the financial support from the Guangxi Key Research and Development Program (Grant No. Guike AB20159033), the Materials Engineering Chongqing Graduate Students Joint Training Base Fund (Grant No. 202103), Natural Science Foundation of Hebei Province (Grant No. E2019203559), and the China Scholarship Council (Grant No. CSC201908080046).

References

Chen, D. 2020. “Study and application of fiber reinforced rubber asphalt sealing layer in cracking prevention of white black pavement.” M.S. thesis, School of Civil Engineering, Chongqing Jiaotong Univ.
Dai, H. 2002. “Carbon nanotubes: Opportunities and challenges.” Surf. Sci. 500 (1–3): 218–241. https://doi.org/10.1016/S0039-6028(01)01558-8.
Fan, Q., Z. Qin, S. Gao, Y. Wu, J. Pionteck, E. Mäder, and M. Zhu. 2012. “The use of a carbon nanotube layer on a polyurethane multifilament substrate for monitoring strains as large as 400%.” Carbon 50 (11): 4085–4092. https://doi.org/10.1016/j.carbon.2012.04.056.
Gao, S., and E. Mäder. 2015. “Multifunctional interphases in polymer composites.” In Multifunctionality of polymer composites: Challenges and new solutions, 338–362. Amsterdam, Netherlands: Elsevier.
Gao, S.-L., R.-C. Zhuang, J. Zhang, J.-W. Liu, and E. Mäder. 2010. “Glass fibers with carbon nanotube networks as multifunctional sensors.” Adv. Funct. Mater. 20 (12): 1885–1893. https://doi.org/10.1002/adfm.201000283.
Ji, F., C. Liu, Y. Hu, S. Xu, Y. He, J. Zhou, and Y. Zhang. 2020. “Chemically grafting carbon nanotubes onto carbon fibers for enhancing interfacial properties of fiber metal laminate.” Materials 13 (17): 3813. https://doi.org/10.3390/ma13173813.
Karger-Kocsis, J., S. Kéki, H. Mahmood, and A. Pegoretti. 2016. “Interphase engineering with nanofillers in fiber-reinforced polymer composites.” In Interface/interphase in polymer nanocomposites, 71–101. New York: Wiley.
Karimov, K. S., M. T. S. Chani, and F. A. Khalid. 2011. “Carbon nanotubes film based temperature sensors.” Phys. E: Low-Dimens. Syst. Nanostructures. 43 (9): 1701–1703. https://doi.org/10.1016/j.physe.2011.05.025.
Kongsta-Gdoutos, M. S., and C. A. Aza. 2014. “Self sensing carbon nanotube (CNT) and nanofiber (CNF) cementitious composites for real time damage assessment in smart structures.” Cem. Concr. Compos. 53 (Oct): 162–169. https://doi.org/10.1016/j.cemconcomp.2014.07.003.
Leng, Z., and I. L. Al-Qadi. 2014. “An innovative method for measuring pavement dielectric constant using the extended CMP method with two air-coupled GPR systems.” NDT and E Int. 66 (Sep): 90–98. https://doi.org/10.1016/j.ndteint.2014.05.002.
Leng, Z., Z. Zhang, Y. Zhang, Y. Wang, H. Yu, and T. Ling. 2018. “Laboratory evaluation of electromagnetic density gauges for hot-mix asphalt mixture density measurement.” Constr. Build. Mater. 158 (Jan): 1055–1064. https://doi.org/10.1016/j.conbuildmat.2017.09.186.
Li, M., M. Zu, J. Yu, H. Cheng, and Q. Li. 2017. “Stretchable fiber supercapacitors with high volumetric performance based on buckled MnO2/oxidized carbon nanotube fiber electrodes.” Small 13 (12): 1602994. https://doi.org/10.1002/smll.201602994.
Liu, Y., Z. Zhang, L. Tan, Y. Xu, C. Wang, P. Liu, H. Yu, and M. Oeser. 2020. “Laboratory evaluation of emulsified asphalt reinforced with glass fiber treated with different methods.” J. Cleaner Prod. 274 (Nov): 123116. https://doi.org/10.1016/j.jclepro.2020.123116.
Luo, S., W. Obitayo, and L. Tao. 2014. “SWCNT-thin-film-enabled fiber sensors for lifelong structural health monitoring of polymeric composites—From manufacturing to utilization to failure.” Carbon 76 (Sep): 321–329. https://doi.org/10.1016/j.carbon.2014.04.083.
Mei, L., X. He, Y. Li, R. Wang, C. Wang, and Q. Peng. 2010. “Grafting carbon nanotubes onto carbon fiber by use of dendrimers.” Mater. Lett. 64 (22): 2505–2508. https://doi.org/10.1016/j.matlet.2010.07.056.
Naghashpour, A., and S. Van Hoa. 2013. “In situ monitoring of through-thickness strain in glass fiber/epoxy composite laminates using carbon nanotube sensors.” Compos. Sci. Technol. 78 (Apr): 41–47. https://doi.org/10.1016/j.compscitech.2013.01.017.
Nofar, M., S. V. Hoa, and M. D. Pugh. 2009. “Failure detection and monitoring in polymer matrix composites subjected to static and dynamic loads using carbon nanotube networks.” Compos. Sci. Technol. 69 (10): 1599–1606. https://doi.org/10.1016/j.compscitech.2009.03.010.
Oliva-Avilés, A. I., F. Avilés, and V. Sosa. 2011. “Electrical and piezoresistive properties of multi-walled carbon nanotube/polymer composite films aligned by an electric field.” Carbon 49 (9): 2989–2997. https://doi.org/10.1016/j.carbon.2011.03.017.
Oshone, M., E. V. Dave, and J. E. Sias. 2019. “Asphalt mix fracture energy based reflective cracking performance criteria for overlay mix selection and design for pavements in cold climates.” Constr. Build. Mater. 211 (Jun): 1025–1033. https://doi.org/10.1016/j.conbuildmat.2019.03.278.
Siahkouhi, M., G. Razaqpur, N. A. Hoult, M. H. Baghban, and G. Jing. 2021. “Utilization of carbon nanotubes (CNTs) in concrete for structural health monitoring (SHM) purposes: A review.” Constr. Build. Mater. 309 (Nov): 125137. https://doi.org/10.1016/j.conbuildmat.2021.125137.
Su, S., Y. Wang, J. Qin, C. Wang, Z. Yao, R. Lu, and Q. Wang. 2019. “Continuous method for grafting CNTs on the surface of carbon fibers based on cobalt catalyst assisted by thiourea.” J. Mater. Sci. 54 (19): 12498–12508. https://doi.org/10.1007/s10853-019-03827-8.
Sun, J., S. Luo, A. Huang, M. Shi, M. Luo, L. Wei, and Y. Sui. 2020. “Double yielding behavior of in situ microfibrillar polyolefin elastomer/poly (lactic acid) composites: Effect of microfibrillar morphology.” Polym. Eng. Sci. 60 (7): 1676–1685. https://doi.org/10.1002/pen.25411.
Xin, X., M. Liang, Z. Yao, L. Su, J. Zhang, P. Li, C. Sun, and H. Jiang. 2020. “Self-sensing behavior and mechanical properties of carbon nanotubes/epoxy resin composite for asphalt pavement strain monitoring.” Constr. Build. Mater. 257 (Oct): 119404. https://doi.org/10.1016/j.conbuildmat.2020.119404.
Xu, Y. 2020. “Study on interfacial mechanical properties of fiber reinforced seal composites based on the conductivity of CNTs.” M.S. thesis, School of Civil Engineering, Chongqing Jiaotong Univ.
You, I., D.-Y. Yoo, S. Kim, M.-J. Kim, and G. Zi. 2017. “Electrical and self-sensing properties of ultra-high-performance fiber-reinforced concrete with carbon nanotubes.” Sensors 17 (11): 2481. https://doi.org/10.3390/s17112481.
Zhang, Z., J. Kohlmeier, C. Schulze, and M. Oeser. 2021. “Concept and development of an accelerated repeated rolling wheel load simulator (ARROWS) for fatigue performance characterization of asphalt mixture.” Materials 14 (24): 7838. https://doi.org/10.3390/ma14247838.
Zhang, Z., and M. Oeser. 2020. “Residual strength model and cumulative damage characterization of asphalt mixture subjected to repeated loading.” Int. J. Fatigue 135 (Jun): 105534. https://doi.org/10.1016/j.ijfatigue.2020.105534.
Zhuang, R., T. T. L. Doan, J. Liu, J. Zhang, S. Gao, and E. Mäder. 2011. “Multi-functional multi-walled carbon nanotube-jute fibres and composites.” Carbon 49 (8): 2683–2692. https://doi.org/10.1016/j.carbon.2011.02.057.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 36Issue 2February 2024

History

Received: Nov 29, 2022
Accepted: Jul 26, 2023
Published online: Nov 25, 2023
Published in print: Feb 1, 2024
Discussion open until: Apr 25, 2024

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Professor, School of Material Science and Engineering, Chongqing Jiaotong Univ., No. 69 Xuefu Ave., Nan’an, Chongqing 400074, China; Research Fellow, Guangxi Key Lab of Road Structure and Materials, Nanning 530007, China. Email: [email protected]
Professor, School of Transportation and Logistics Engineering, Wuhan Univ. of Technology, No. 1178 Heping Ave., Wuhan 430063, China; Professor, Hubei Highway Engineering Research Center, No. 1178 Heping Ave., Wuhan 400074, China (corresponding author). ORCID: https://orcid.org/0000-0003-3376-7817. Email: [email protected]
Postgraduate Research Assistant, School of Civil Engineering, Chongqing Jiaotong Univ., No. 69 Xuefu Ave., Nan’an, Chongqing 400074, China. Email: [email protected]
Postgraduate Research Assistant, School of Material Science and Engineering, Chongqing Jiaotong Univ., No. 69 Xuefu Ave., Nan’an, Chongqing 400074, China. Email: [email protected]
Postgraduate Research Assistant, School of Civil Engineering, Chongqing Jiaotong Univ., No. 69 Xuefu Ave., Nan’an, Chongqing 400074, China. Email: [email protected]
Postgraduate Research Assistant, School of Civil Engineering, Chongqing Jiaotong Univ., No. 69 Xuefu Ave., Nan’an, Chongqing 400074, China. Email: [email protected]

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