Technical Papers
Feb 16, 2023

Moisture Susceptibility of Asphalt Mixture Subjected to Chloride-Based Deicing Salt Solutions under Simulated Environmental Conditions

Publication: Journal of Materials in Civil Engineering
Volume 35, Issue 5

Abstract

Chloride-based deicing salts are considered to be cost-effective and highly efficient in ensuring safe and efficient roadway and/or aircraft operation during snowy pavement conditions. However, it brings inevitable detrimental effects on the asphalt pavement. This study seeks to elucidate the influence of deicing salt type, concentration, and exposed environment on moisture susceptibility of an asphalt mixture. Immersion Marshall stability testing and freezing-thawing splitting tensile testing were employed to evaluate the moisture susceptibility of the asphalt mixture under drying-wetting and freezing-thawing cycling. Two types of compound deicing agents and three concentrations of 3%, 10%, and 20% of each salt were used to examine and compare their degrees of deterioration on the asphalt mixture. Statistical analysis was performed to establish the relationship between key indicators of moisture susceptibility and the main factors of the asphalt mixture. Microstructure analysis was carried out to elucidate the effects of those factors on the moisture susceptibility of the asphalt mixture using x-ray diffraction (XRD) analysis and scanning electron microscope (SEM) observation. Test results indicated that the moisture susceptibility of the asphalt mixture was greatly influenced by the salt concentration and conditioned drying-wetting (D/W) or freezing-thawing (F/T) cycles. With the increase of D/W or F/T cycles, the Marshall stability, Marshall modulus, and splitting tensile strength decreased while the flow value increased. The 3% salt concentration showed a significant effect on moisture susceptibility, followed by 10% and then 20%. The proposed models can effectively predict the key indicators of moisture susceptibility with high correlation coefficients over 0.9. As confirmed by the microstructural analyses, the deterioration of the asphalt mixture under simulated environmental conditions was attributed to decreased asphalt-aggregate adhesion from water ingress, salt crystallization, and/or ice formation pressure.

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Data Availability Statement

All data, models, and code generated or used during the study appear in the published article.

Acknowledgments

The authors gratefully acknowledge the financial support from the National Science Foundation of China (No. 52008164), the National Science Foundation of Hunan Province of China (2022JJ30144), and the Fundamental Research Funds for the Central Universities (No. 531118010484).

References

ASTM. 2020. Standard practice for effect of water on asphalt-coated aggregate using boiling water. ASTM D 3625-20. West Conshohocken, PA: ASTM.
Bardal, K. G., and F. Jørgensen. 2017. “Valuing the risk and social costs of road traffic accidents—Seasonal variation and the significance of delay costs.” Transport Policy 57 (Jul): 10–19. https://doi.org/10.1016/j.tranpol.2017.03.015.
Cao, Y., A. Sha, Z. Liu, J. Li, and W. Jiang. 2021. “Energy output of piezoelectric transducers and pavements under simulated traffic load.” J. Cleaner Prod. 279 (Jan): 123508. https://doi.org/10.1016/j.jclepro.2020.123508.
Chen, Q., C. Wang, X. Sun, Y. Cao, T. Guo, and J. Chen. 2019. “Evaluation and prediction for effect of conductive gussasphalt mixture on corrosion of steel bridge deck.” Constr. Build. Mater. 228 (Dec): 116837. https://doi.org/10.1016/j.conbuildmat.2019.116837.
Coussy, O., and P. J. Monteiro. 2008. “Poroelastic model for concrete exposed to freezing temperatures.” Cem. Concr. Res. 38 (1): 40–48. https://doi.org/10.1016/j.cemconres.2007.06.006.
Curtis, C. W. 1992. “Investigation of asphalt-aggregate interactions in asphalt pavements.” Fuel 37 (Aug): 1292–1297.
Fakhri, M., S. Javadi, R. Sedghi, D. Arzjani, and Y. Zarrinpour. 2019. “Effects of deicing agents on moisture susceptibility of the WMA containing recycled crumb rubber.” Constr. Build. Mater. 227 (Aug): 116581. https://doi.org/10.1016/j.conbuildmat.2019.07.307.
Farnam, Y., A. Wiese, D. Bentz, J. Davis, and J. Weiss. 2015. “Damage development in cementitious materials exposed to magnesium chloride deicing salt.” Constr. Build. Mater. 93 (Sep): 384–392. https://doi.org/10.1016/j.conbuildmat.2015.06.004.
Feng, D., J. Yi, D. Wang, and L. Chen. 2010. “Impact of salt and freeze–thaw cycles on performance of asphalt mixtures in coastal frozen region of China.” Cold Reg. Sci. Technol. 62 (1): 34–41. https://doi.org/10.1016/j.coldregions.2010.02.002.
Gao, J., H. Guo, X. Wang, P. Wang, Y. Wei, Z. Wang, Y. Huang, and B. Yang. 2019. “Microwave deicing for asphalt mixture containing steel wool fibers.” J. Cleaner Prod. 206 (Jan): 1110–1122. https://doi.org/10.1016/j.jclepro.2018.09.223.
Goh, S., M. Akin, Z. You, and X. Shi. 2011. “Effect of deicing solutions on the tensile strength of micro- or nano-modified asphalt mixture.” Constr. Build. Mater. 25 (1): 195–200. https://doi.org/10.1016/j.conbuildmat.2010.06.038.
Guo, Q., G. Li, Y. Gao, K. Wang, Z. Dong, F. Liu, and H. Zhu. 2019. “Experimental investigation on bonding property of asphalt-aggregate interface under the actions of salt immersion and freeze-thaw cycles.” Constr. Build. Mater. 206 (Jan): 590–599. https://doi.org/10.1016/j.conbuildmat.2019.02.094.
Hassan, Y., A. O. Abd El Halim, A. G. Razaqpur, W. Bekheet, and M. H. Farha. 2002. “Effects of runway deicers on pavement materials and mixes: Comparison with road salt.” J. Transp. Eng. 128 (4): 385–391. https://doi.org/10.1061/(ASCE)0733-947X(2002)128:4(385).
Huang, B., G. Li, and L. N. Mohammad. 2003. “Analytical modeling and experimental study of tensile strength of asphalt concrete composite at low temperatures.” Composite, Part B 34 (8): 705–714. https://doi.org/10.1016/S1359-8368(03)00079-9.
Li, F., and Z. Wang. 2012. “Experiment on road performance of asphalt mixture with automatic long-term snowmelt agent.” J. Highway Transp. Res. Dev. 6 (4): 11–17. https://doi.org/10.1061/JHTRCQ.0000002.
Liu, K., Z. Wang, D. Guo, F. Wang, and H. Xie. 2018. “The interlaminar shear failure characteristics of asphalt pavement coupled heating cables.” Mater. Struct. 51 (3): 1–13. https://doi.org/10.1617/s11527-018-1193-0.
Liu, K., H. Xie, P. Xu, Z. Wang, H. Bai, and F. Wang. 2019. “The thermal and damage characteristics of an insulated-conductive composite structure for the heated bridge deck for snow-melting.” Constr. Build. Mater. 216 (Aug): 176–187. https://doi.org/10.1016/j.conbuildmat.2019.05.002.
Liu, Z., M. Xing, S. Chen, R. He, and P. Cong. 2014. “Influence of the chloride-based anti-freeze filler on the properties of asphalt mixtures.” Constr. Build. Mater. 51 (Jan): 133–140. https://doi.org/10.1016/j.conbuildmat.2013.09.057.
MOT (Ministry of Transport of the People’s Republic of China). 2000. Standard test methods of bitumen and bituminous mixtures for highway engineering. [In Chinese.] JTJ052-2000. Beijing: China Communication Press.
MOT (Ministry of Transport of the People’s Republic of China). 2011. Standard test method of bitumen and bitumen mixtures for highway engineering. JTG E20-2011. [In Chinese.] Beijing: China Communications Press.
Özgan, E., S. Serin, H. Gerengi, and İ. Arslan. 2013. “Multi-faceted investigation of the effect of de-icer chemicals on the engineering properties of asphalt concrete.” Cold Reg. Sci. Technol. 87 (Mar): 59–67. https://doi.org/10.1016/j.coldregions.2012.11.003.
Pisano, P. A., L. C. Goodwin, and M. A. Rossetti. 2008. “US highway crashes in adverse road weather conditions.” In Proc., 24th Conf. on Int. Interactive Information and Processing Systems for Meteorology. New Orleans: Oceanography and Hydrology.
Sassani, A., A. Arabzadeh, H. Ceylan, S. Kim, S. M. S. Sadati, K. Gopalakrishnan, P. C. Taylor, and H. Abdualla. 2018. “Carbon fiber-based electrically conductive concrete for salt-free deicing of pavements.” J. Cleaner Prod. 203 (Dec): 799–809. https://doi.org/10.1016/j.jclepro.2018.08.315.
Wang, C., Q. Chen, H. Fu, and J. Chen. 2018. “Heat conduction effect of steel bridge deck with conductive gussasphalt concrete pavement.” Constr. Build. Mater. 172 (Feb): 422–432. https://doi.org/10.1016/j.conbuildmat.2018.03.161.
Wang, C., H. Fu, W. Ma, Z. Zhang, X. Ji, and X. Han. 2020. “Combination design and performance evaluation of conductive bonding layer for asphalt pavement active deicing.” Constr. Build. Mater. 263 (Dec): 121037. https://doi.org/10.1016/j.conbuildmat.2020.121037.
Wang, L., N. Gong, and Y. Xing. 2016a. “Researching the influence factors of asphalt mixture performance under the damage of deicing salt and freezing-thawing cycles.” J. Funct. Mater. 47 (4): 4088–4093. https://doi.org/10.3969/j.issn.1001-9731.2016.04.018.
Wang, L., Y. Jia, D. Zhang, and J. Hu. 2016b. “Influence of salt freezing cycle on interfacial adhesion of asphalt-aggregate based on surface energy theory.” Acta Mater. Compos. Sin. 33 (10): 2380–2389. https://doi.org/10.13801/j.cnki.fhclxb.20151221.001.
Wang, Z., T. Zhang, M. Shao, T. Ai, and P. Zhao. 2017. “Investigation on snow-melting performance of asphalt mixtures incorporating with salt-storage aggregates.” Constr. Build. Mater. 142 (Jun): 187–198. https://doi.org/10.1016/j.conbuildmat.2017.03.070.
Wu, H., P. Li, T. Nian, G. Zhang, T. He, and X. Wei. 2019. “Evaluation of asphalt and asphalt mixtures’ water stability method under multiple freeze-thaw cycles.” Constr. Build. Mater. 228 (Dec): 117089. https://doi.org/10.1016/j.conbuildmat.2019.117089.
Wu, S., J. Yang, X. Sun, C. Wang, R. Yang, and J. Zhu. 2020. “Preparation and characterization of anti-freezing asphalt pavement.” Constr. Build. Mater. 236 (Mar): 117579. https://doi.org/10.1016/j.conbuildmat.2019.117579.
Wu, Z., P. Gao, D. Chen, H. Zhang, X. Chen, and Y. Lin. 2012. “Effect of chlorine deicers on performance of low temperature crack resistance of asphalt mixture.” [In Chinese.] Highway Eng. 4 (Jun): 6.
Wu, Z., C. Shi, P. Gao, D. Wang, and Z. Cao. 2014. “Effects of deicing salts on the scaling resistance of concrete.” J. Mater. Civ. Eng. 27 (5): 04014160. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001106.
Xu, H., D. Wang, Y. Tan, J. Zhou, and M. Oeser. 2018. “Investigation of design alternatives for hydronic snow melting pavement systems in China.” J. Cleaner Prod. 170 (Jan): 1413–1422. https://doi.org/10.1016/j.jclepro.2017.09.262.
Xu, O., S. Han, C. Zhang, Y. Liu, F. Xiao, and J. Xu. 2015. “Laboratory investigation of andesite and limestone asphalt mixtures containing sodium chloride-based anti-icing filler.” Constr. Build. Mater. 98 (Nov): 671–677. https://doi.org/10.1016/j.conbuildmat.2015.08.126.
Yang, H., L. Pang, Y. Zou, Q. Liu, and J. Xie. 2020. “The effect of water solution erosion on rheological, cohesion and adhesion properties of asphalt.” Constr. Build. Mater. 246 (Jun): 118465. https://doi.org/10.1016/j.conbuildmat.2020.118465.
Yang, Q. B. 2007. “Effects of NaCl concentration on ice-formation expansion and the solution absorption by concrete.” [In Chinese.] J. Build. Mater. 10 (3): 266–270.
Zhang, K., W. Li, and F. Han. 2019. “Performance deterioration mechanism and improvement techniques of asphalt mixture in salty and humid environment.” Constr. Build. Mater. 208 (May): 749–757. https://doi.org/10.1016/j.conbuildmat.2019.03.061.
Zhang, K., Y. Luo, W. Xie, and J. Wu. 2020. “Evaluation of road performance and adhesive characteristic of asphalt binder in salt erosion environment.” Mater. Today Commun. 25 (Dec): 101593. https://doi.org/10.1016/j.mtcomm.2020.101593.
Zhong, K., M. Sun, and R. Chang. 2018. “Performance evaluation of high-elastic/salt-storage asphalt mixture modified with Mafilon and rubber particles.” Constr. Build. Mater. 193 (Dec): 153–161. https://doi.org/10.1016/j.conbuildmat.2018.10.185.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 35Issue 5May 2023

History

Received: May 2, 2022
Accepted: Aug 9, 2022
Published online: Feb 16, 2023
Published in print: May 1, 2023
Discussion open until: Jul 16, 2023

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Professor, College of Civil Engineering, Hunan Univ., Changsha, Hunan 410082, China (corresponding author). ORCID: https://orcid.org/0000-0003-4921-6542. Email: [email protected]
Chair Professor, College of Civil Engineering, Hunan Univ., Changsha, Hunan 410082, China. Email: [email protected]
Professor, Dept. of Civil Engineering, Nanjing Univ. of Aeronautics and Astronautics, Nanjing 210016, China. Email: [email protected]
Henglong Zhang [email protected]
Professor, College of Civil Engineering, Hunan Univ., Changsha, Hunan 410082, China. Email: [email protected]
Associate Professor, College of Civil Engineering, Hunan Univ., Changsha, Hunan 410082, China. Email: [email protected]

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