Technical Papers
Jul 20, 2022

Laboratory Study to Evaluate the In-Situ Use of Rejuvenator Seal Material to Restore In-Service Asphalt Pavement

Publication: Journal of Materials in Civil Engineering
Volume 34, Issue 10

Abstract

Rejuvenator seal material (RSM) is designed to revitalize an aged asphalt binder by spraying it on the surface of roads. It restores the mechanical properties of the existing pavement. This paper studied the effectiveness of RSMs containing cooking oil residue, motor oil residue, coal oil, solvent, and virgin or styrene-butadiene-styrene (SBS) modified 60/70 bitumen to improve the behavior of an in-service pavement. Three stages were followed to formulate RSMs. To achieve the effective oil, the penetration grade and softening point changes of rolling thin-film oven (RTFO) + pressure aging vessel (PAV) aged 60/70 bitumen mixing with different percentages of oils were studied. Then, the penetration depth of benzene, toluene, and xylene in hot mix asphalt (HMA) samples were measured to choose the most efficient solvent. Finally, the penetration depth of RSMs with various mixing ratios in HMA mixes was measured to determine the mix design and application values (g/m2). RSM-A (5%COR+5%MOR and 60/70 bitumen), RSM-B (5%COR+5%CO and 60/70 bitumen), and RSM-C (5%COR+5%CO and SBS modified 60/70 bitumen) were selected for further assessments. Other than the aforesaid RSMs, RejuvaSeal was used as a generic commercial substance. A British Pendulum Test was used to ensure sufficient skid resistance to reopen the traffic soon after distributing the RSMs. Dynamic shear rheometer and bending beam rheometer tests were used to investigate the rheological properties of extracted bitumen from the upper 1.5 cm layer of the pavement with and without RSMs. Moreover, the fatigue behavior of rejuvenated asphalt mixtures was studied by the 4-point bending test. Based on the results, all RSMs had a positive effect on the softening of the aged bitumen. All RSMs regained the fatigue performance of the aged binder. However, they showed the reverse effect on the rutting resistance. RSM-C containing 5%COR+5%CO and SBS modified 60/70 bitumen considerably modified the rheological properties of the aged binder even better than those mixtures rejuvenated by RejuvaSeal.

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Data Availability Statement

All data, models, and code generated or used during the study appear in the published article.

References

Ahmed, R. B., and K. Hossain. 2020. “Waste cooking oil as an asphalt rejuvenator: A state-of-the-art review.” Constr. Build. Mater. 230 (Jan): 116985. https://doi.org/10.1016/j.conbuildmat.2019.116985.
Ali, M. F., and M. N. Siddiqui. 2001. “Changes in asphalt chemistry and durability during oxidation and polymer modification.” Pet. Sci. Technol. 19 (9–10): 1229–1249. https://doi.org/10.1081/LFT-100108305.
Asli, H., E. Ahmadinia, M. Zargar, and M. R. Karim. 2012. “Investigation on physical properties of waste cooking oil—Rejuvenated bitumen binder.” Constr. Build. Mater. 37 (Dec): 398–405. https://doi.org/10.1016/j.conbuildmat.2012.07.042.
ASTM. 2015. Standard test method for determining the rheological properties of asphalt binder using a dynamic shear rheometer. ASTM D7175-15. West Conshohocken, PA: ASTM.
ASTM. 2016a. Standard specification for road tar. ASTM D490-92(2016). West Conshohocken, PA: ASTM.
ASTM. 2016b. Standard test method for determining the flexural creep stiffness of asphalt binder using the bending beam rheometer (BBR). ASTM D6648-08(2016). West Conshohocken, PA: ASTM.
ASTM. 2017a. Standard practice for recovery of asphalt from solution using the rotary evaporator. ASTM D5404/D5404M-12. West Conshohocken, PA: ASTM.
ASTM. 2017b. Standard test methods for quantitative extraction of asphalt binder from asphalt mixtures. ASTM D2172/D2172M-17e1. West Conshohocken, PA: ASTM.
ASTM. 2019a. Practice for accelerated aging of asphalt binder using a pressurized aging vessel (PAV). ASTM D6521-19a. West Conshohocken, PA: ASTM.
ASTM. 2019b. Standard test method for measuring paved surface frictional properties using the dynamic friction tester. ASTM E1911-19. West Conshohocken, PA: ASTM.
ASTM. 2019c. Test method for effect of heat and air on a moving film of asphalt (rolling thin-film oven test). ASTM D2872-19. West Conshohocken, PA: ASTM.
ASTM. 2021. Standard test method for recovery of asphalt from solution by Abson method. ASTM D1856-21. West Conshohocken, PA: ASTM.
Baghaee Moghaddam, T., and H. Baaj. 2016. “The use of rejuvenating agents in production of recycled hot mix asphalt: A systematic review.” Constr. Build. Mater. 114 (Jul): 805–816. https://doi.org/10.1016/j.conbuildmat.2016.04.015.
Baghaee Moghaddam, T., M. R. Karim, and T. Syammaun. 2012. “Dynamic properties of stone mastic asphalt mixtures containing waste plastic bottles.” Constr. Build. Mater. 34 (Sep): 236–242. https://doi.org/10.1016/j.conbuildmat.2012.02.054.
Behnood, A. 2019. “Application of rejuvenators to improve the rheological and mechanical properties of asphalt binders and mixtures: A review.” J. Cleaner Prod. 231 (Sep): 171–182. https://doi.org/10.1016/j.jclepro.2019.05.209.
Blanchette, A., S. T. Lee, and T. Wood. 2020. Spray on rejuvenators synthesis. St. Paul, MN: Minnesota DOT.
Blomberg, T., M. Makowska, and T. Pellinen. 2016. “Laboratory simulation of bitumen aging and rejuvenation to mimic multiple cycles of reuse.” Transp. Res. Procedia 14 (Jan): 694–703. https://doi.org/10.1016/j.trpro.2016.05.335.
Brownridge, J. 2010. “The role of an asphalt rejuvenator in pavement preservation: Use and need for asphalt rejuvenation.” In Proc., Compendium of Papers from the First Int. Conf. on Pavement Preservation, 351–364. Newport Beach, CA: California DOT.
Bullas, J. C. 1969. “HMSO, instructions for using the portable skid-resistance tester.” Accessed May 16, 1996. https://www.academia.edu/2628616/HMSO_Instructions_for_using_the_portable_skid_resistance_tester_2nd_edition_1969.
Canestrari, F., and L. P. Ingrassia. 2020. “A review of top-down cracking in asphalt pavements: Causes, models, experimental tools and future challenges.” J. Traffic Transp. Eng. 7 (5): 541–572. https://doi.org/10.1016/j.jtte.2020.08.002.
Cao, Z., M. Chen, J. Yu, and X. Han. 2020. “Preparation and characterization of active rejuvenated SBS modified bitumen for the sustainable development of high-grade asphalt pavement.” J. Cleaner Prod. 273 (Nov): 123012. https://doi.org/10.1016/j.jclepro.2020.123012.
CEN (European Committee for Standardization). 2012. Bituminous mixtures—Test methods for hot mix asphalt—Part 24: Resistance to fatigue. EN 12697-24:2012. Brussels, Belgium: CEN.
Chu, L., W. Guo, and T. F. Fwa. 2022. “Theoretical and practical engineering significance of British pendulum test.” Int. J. Pavement Eng. 23 (1): 1–8. https://doi.org/10.1080/10298436.2020.1726351.
Cong, P., X. Guo, and L. Mei. 2020. “Investigation on rejuvenation methods of aged SBS modified asphalt binder.” Fuel 279 (Nov): 118556. https://doi.org/10.1016/j.fuel.2020.118556.
Daryaee, D., M. Ameri, and A. Mansourkhaki. 2020. “Utilizing of waste polymer modified bitumen in combination with rejuvenator in high reclaimed asphalt pavement mixtures.” Constr. Build. Mater. 235 (Feb): 117516. https://doi.org/10.1016/j.conbuildmat.2019.117516.
Daryaee, D., M. Habibpour, S. Gulzar, and B. S. Underwood. 2021. “Combined effect of waste polymer and rejuvenator on performance properties of reclaimed asphalt binder.” Constr. Build. Mater. 268 (Jan): 121059. https://doi.org/10.1016/j.conbuildmat.2020.121059.
Dehghan, Z., and A. Modarres. 2017. “Evaluating the fatigue properties of hot mix asphalt reinforced by recycled PET fibers using 4-point bending test.” Constr. Build. Mater. 139 (May): 384–393. https://doi.org/10.1016/j.conbuildmat.2017.02.082.
Ding, Y., B. Huang, W. Hu, B. Tang, and M. Yu. 2019. “Utilizing recycled asphalt shingle into pavement by extraction method.” J. Cleaner Prod. 236 (Nov): 117656. https://doi.org/10.1016/j.jclepro.2019.117656.
Hesp, S., and S. K. Subramani. 2009. “Another look at the bending beam rheometer for specification grading of asphalt cements.” In Proc., 6th Int. Conf. on Maintenance and Rehabilitation of Pavements and Technological Control, MAIREPAV 2009. Torino, Italy: Politecnico di Torino.
Ishaq, M. A., and F. Giustozzi. 2020. “Rejuvenator effectiveness in reducing moisture and freeze/thaw damage on long-term performance of 20% RAP asphalt mixes: An Australian case study.” Case Stud. Constr. Mater. 13 (Dec): e00454. https://doi.org/10.1016/j.cscm.2020.e00454.
Ismail, A. I., A. M. Atta, M. El-Newehy, and M. E. El-Hefnawy. 2020. “Synthesis and application of new amphiphilic asphaltene ionic liquid polymers to demulsify Arabic heavy petroleum crude oil emulsions.” Polymers (Basel) 12 (6): 1273. https://doi.org/10.3390/polym12061273.
Khasawneh, M. A., and M. A. Alsheyab. 2020. “Effect of nominal maximum aggregate size and aggregate gradation on the surface frictional properties of hot mix asphalt mixtures.” Constr. Build. Mater. 244 (May): 118355. https://doi.org/10.1016/j.conbuildmat.2020.118355.
Kommidi, S. R., and Y.-R. Kim. 2021. “Dynamic shear rheometer testing and mechanistic conversion to predict bending beam rheometer low temperature behavior of bituminous binder.” Constr. Build. Mater. 267 (Jan): 120563. https://doi.org/10.1016/j.conbuildmat.2020.120563.
Lin, J., P. Guo, J. Xie, S. Wu, and M. Chen. 2013. “Effect of rejuvenator sealer materials on the properties of aged asphalt binder.” J. Mater. Civ. Eng. 25 (7): 829–835. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000702.
Lin, J., J. Hong, C. Huang, J. Liu, and S. Wu. 2014. “Effectiveness of rejuvenator seal materials on performance of asphalt pavement.” Constr. Build. Mater. 55 (Mar): 63–68. https://doi.org/10.1016/j.conbuildmat.2014.01.018.
Lu, X., and U. Isacsson. 2002. “Effect of ageing on bitumen chemistry and rheology.” Constr. Build. Mater. 16 (1): 15–22. https://doi.org/10.1016/S0950-0618(01)00033-2.
Mansourkhaki, A., M. Ameri, M. Habibpour, and B. Shane Underwood. 2020. “Chemical composition and rheological characteristics of binders containing RAP and rejuvenator.” J. Mater. Civ. Eng. 32 (4): 04020026. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003016.
Mohd Hasan, M. R., Z. You, H. Yin, L. You, and R. Zhang. 2019. “Characterizations of foamed asphalt binders prepared using combinations of physical and chemical foaming agents.” Constr. Build. Mater. 204 (Apr): 94–104. https://doi.org/10.1016/j.conbuildmat.2019.01.156.
Mubaraki, M. 2020. “Comparison of laboratory performance of two superpave binders mixed with two modifiers.” Road Mater. Pavement Des. 21 (4): 1155–1169. https://doi.org/10.1080/14680629.2018.1541138.
Nejad, F. M., P. Aghajani, A. Modarres, and H. Firoozifar. 2012. “Investigating the properties of crumb rubber modified bitumen using classic and SHRP testing methods.” Constr. Build. Mater. 26 (1): 481–489. https://doi.org/10.1016/j.conbuildmat.2011.06.048.
Newcomb, D. E., P. Arabali, H. Al-Khayat, and F. Zhou. 2021. Test methods to quantify cracking resistance of asphalt binders and mixtures. St. Paul, MN: Minnesota DOT.
Nogueira, R. L., J. B. Soares, and S. de Aguiar Soares. 2019. “Rheological evaluation of cotton seed oil fatty amides as a rejuvenating agent for RAP oxidized asphalts.” Constr. Build. Mater. 223 (Oct): 1145–1153. https://doi.org/10.1016/j.conbuildmat.2019.06.128.
Pradhan, S. K., and U. C. Sahoo. 2020. “Influence of softer binder and rejuvenator on bituminous mixtures containing reclaimed asphalt pavement (RAP) material.” Int. J. Transp. Sci. Technol. 11 (1): 46–59. https://doi.org/10.1016/j.ijtst.2020.12.001.
Ržek, L., M. Ravnikar Turk, and M. Tušar. 2020. “Increasing the rate of reclaimed asphalt in asphalt mixture by using alternative rejuvenator produced by tire pyrolysis.” Constr. Build. Mater. 232 (Jan): 117177. https://doi.org/10.1016/j.conbuildmat.2019.117177.
Safaei, F., and C. Castorena. 2020. “Improved interpretation of asphalt binder parallel plate dynamic shear rheometer fatigue tests.” Int. J. Pavement Eng. 21 (1): 74–87. https://doi.org/10.1080/10298436.2018.1438611.
Salih, J., F. Edum-Fotwe, and A. Price. 2016. “Investigating the road maintenance performance in developing countries.” Int. J. Civ. Environ. Eng. 10 (4): 433–437. https://doi.org/10.5281/zenodo.1123648.
Shen, J., S. Amirkhanian, and B. Tang. 2007. “Effects of rejuvenator on performance-based properties of rejuvenated asphalt binder and mixtures.” Constr. Build. Mater. 21 (5): 958–964. https://doi.org/10.1016/j.conbuildmat.2006.03.006.
Speight, J. G. 2004. “Petroleum asphaltenes—Part 1: Asphaltenes, resins and the structure of petroleum.” Oil Gas Sci. Technol. 59 (5): 467–477. https://doi.org/10.2516/ogst:2004032.
Sun, Z., J. Yi, Y. Huang, D. Feng, and C. Guo. 2016. “Investigation of the potential application of biodiesel by-product as asphalt modifier.” Road Mater. Pavement Des. 17 (3): 737–752. https://doi.org/10.1080/14680629.2015.1096819.
Svasdisant, T., M. Schorsch, G. Y. Baladi, and S. Pinyosunun. 2002. “Mechanistic analysis of top-down cracks in asphalt pavements.” Transp. Res. Rec. 1809 (1): 126–136. https://doi.org/10.3141/1809-15.
Tayebali, A. A., G. M. Rowe, and J. B. Sousa. 1992. “Fatigue response of asphalt-aggregate mixtures (with discussion).” J. Assoc. Asphalt Paving Technol. 61: 333–360.
Wang, Z., J. Li, Z. Zhang, M. Jia, and J. Yang. 2020. “Formulation of a new warm-mix recycling agent and its rejuvenating effect on aged asphalt.” Constr. Build. Mater. 262 (Nov): 120804. https://doi.org/10.1016/j.conbuildmat.2020.120804.
Wróbel, M., A. Woszuk, M. Ratajczak, and W. Franus. 2021. “Properties of reclaimed asphalt pavement mixture with organic rejuvenator.” Constr. Build. Mater. 271 (Feb): 121514. https://doi.org/10.1016/j.conbuildmat.2020.121514.
Yang, X., and Z. You. 2015. “High temperature performance evaluation of bio-oil modified asphalt binders using the DSR and MSCR tests.” Constr. Build. Mater. 76 (Feb): 380–387. https://doi.org/10.1016/j.conbuildmat.2014.11.063.
Yu, M., Z. You, G. Wu, L. Kong, C. Liu, and J. Gao. 2020. “Measurement and modeling of skid resistance of asphalt pavement: A review.” Constr. Build. Mater. 260 (Nov): 119878. https://doi.org/10.1016/j.conbuildmat.2020.119878.
Zaumanis, M., R. B. Mallick, L. Poulikakos, and R. Frank. 2014. “Influence of six rejuvenators on the performance properties of reclaimed asphalt pavement (RAP) binder and 100% recycled asphalt mixtures.” Constr. Build. Mater. 71 (Nov): 538–550. https://doi.org/10.1016/j.conbuildmat.2014.08.073.
Zeng, Z. A., B. S. Underwood, and C. Castorena. 2020. “Low-temperature performance grade characterisation of asphalt binder using the dynamic shear rheometer.” Int. J. Pavement Eng. 23 (3): 811–823. https://doi.org/10.1080/10298436.2020.1774766.
Zhang, J., C. Guo, T. Chen, W. Zhang, K. Yao, C. Fan, M. Liang, C. Guo, and Z. Yao. 2021. “Evaluation on the mechanical performance of recycled asphalt mixtures incorporated with high percentage of RAP and self-developed rejuvenators.” Constr. Build. Mater. 269 (Feb): 121337. https://doi.org/10.1016/j.conbuildmat.2020.121337.
Zhang, J., X. Zhang, M. Liang, H. Jiang, J. Wei, and Z. Yao. 2020a. “Influence of different rejuvenating agents on rheological behavior and dynamic response of recycled asphalt mixtures incorporating 60% RAP dosage.” Constr. Build. Mater. 238 (Mar): 117778. https://doi.org/10.1016/j.conbuildmat.2019.117778.
Zhang, X., K. Zhang, C. Wu, K. Liu, and K. Jiang. 2020b. “Preparation of bio-oil and its application in asphalt modification and rejuvenation: A review of the properties, practical application and life cycle assessment.” Constr. Build. Mater. 262 (Nov): 120528. https://doi.org/10.1016/j.conbuildmat.2020.120528.
Zhou, T., L. Cao, E. H. Fini, L. Li, Z. Liu, and Z. Dong. 2020. “Behaviors of asphalt under certain aging levels and effects of rejuvenation.” Constr. Build. Mater. 249 (Jul): 118748. https://doi.org/10.1016/j.conbuildmat.2020.118748.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 34Issue 10October 2022

History

Received: Sep 3, 2021
Accepted: Jan 27, 2022
Published online: Jul 20, 2022
Published in print: Oct 1, 2022
Discussion open until: Dec 20, 2022

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Masoud Taghavi [email protected]
Master’s Student, Highway and Transportation Engineering, Dept. of Civil Engineering, Babol Noshirvani Univ. of Technology, Babol 91847-95678, Iran. Email: [email protected]
Saeid Hesami [email protected]
Associate Professor and Doctor of Philosophy in Highway and Transportation Engineering, Dept. of Civil Engineering, Babol Noshirvani Univ. of Technology, Babol 47148-7116, Iran (corresponding author). Email: [email protected]
Ebrahim Hesami [email protected]
Doctor of Philosophy in Civil Engineering, Researcher, Dept. of Civil & Architectural Engineering, KTH Royal Institute of Technology, Stock, Stockholm 114 28, Sweden. Email: [email protected]
Seyedalireza Mohammadirad [email protected]
Master’s Student, Highway and Transportation Engineering, Dept. of Civil Engineering, Babol Noshirvani Univ. of Technology, Babol 47148-87863, Iran. Email: [email protected]

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