Moisture Damage of Asphalt Based on Adhesion, Microsurface Energy, and Nanosurface Roughness
Publication: Journal of Materials in Civil Engineering
Volume 34, Issue 10
Abstract
To explore the influence of water on the multiscale adhesive behavior between asphalt binder and aggregate, the nanosurface morphology and microsurface energy of asphalt binder and the macrobonding force between the asphalt binder and aggregate over different soaking times were examined using atomic force microscopy (AFM) and the pull-off test. Relationships between the macrobonding and the nanosurface roughness as well as the microsurface energy were analyzed. The results demonstrated that the effect of water on the surface morphology of asphalt binder was important. After immersion in water, water-induced bulges occurred on the asphalt binder surface, which further changed the nanosurface roughness and the surface energy of asphalt. As per the sensitivity results, it can be concluded that the surface energy of asphalt and the effective contact area between asphalt and aggregate were reduced because of moisture, thus resulting in the failure of adhesion.
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Data Availability Statement
All data, models, and code generated or used during the study appear in the published article.
Acknowledgments
This work was supported in part by the National Natural Science Foundation of China under Project No. 51908460, by the Open Fund of Key Laboratory for Special Area Highway Engineering of Ministry of Education (Chang’an University) under Project No. 300102219516, and by the Open Fund of Key Laboratory of Road Structure & Materials of Ministry of Transport (Chang’an University) under Project No. 300102219520.
References
Allen, R. G. 2010. “Properties in asphalt using atomic force microscopy.” Ph.D. thesis, Dept. of Civil Engineering, Texas A&M Univ.
Al-Rawashdeh, A. S., and S. Sargand. 2014. “Performance assessment of a warm asphalt binder in the presence of water by using surface free energy concepts and nanoscale techniques.” J. Mater. Civ. Eng. 26 (5): 803–811. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000866.
Arifuzzaman, M., M. S. Islam, and M. I. Hossain. 2017. “Moisture damage evaluation in SBS and lime modified asphalt using AFM and artificial intelligence.” Neural Comput. Appl. 28 (1): 125–134. https://doi.org/10.1007/s00521-015-2041-6.
ASTM. 1995. Standard test method for pull-off strength of coatings using portable adhesion testers. ASTM D4541. West Conshohocken, PA: ASTM.
Caro, S., E. Masad, A. Bhasin, and D. N. Little. 2008a. “Moisture susceptibility of asphalt mixtures, part 1: Mechanisms.” Int. J. Pavement Eng. 9 (2): 81–98. https://doi.org/10.1080/10298430701792128.
Caro, S., E. Masad, A. Bhasin, and D. N. Little. 2008b. “Moisture susceptibility of asphalt mixtures, part 2: Characterisation and modelling.” Int. J. Pavement Eng. 9 (2): 99–114. https://doi.org/10.1080/10298430701792144.
Chen, Q., C. Wang, Z. Qiao, and T. Guo. 2020. “Graphene/tourmaline composites as a filler of hot mix asphalt mixture: Preparation and properties.” Constr. Build. Mater. 239 (Apr): 117859. https://doi.org/10.1016/j.conbuildmat.2019.117859.
Cheng, Z., X. Zhang, and F. Kong. 2020. “Investigation on moisture diffusion property into asphalt film.” [In Chinese.] J. Build. Mater. 24 (2): 1–13.
Copeland, A. R. 2007. “Influence of moisture on bond strength of asphalt-aggregate systems.” Ph.D. thesis, Dept. of Civil Engineering, Vanderbilt Univ.
Dos Santos, S., M. N. Partl, and L. D. Poulikakos. 2014. “Newly observed effects of water on the microstructures of bitumen surface.” Constr. Build. Mater. 71 (Nov): 618–627. https://doi.org/10.1016/j.conbuildmat.2014.08.076.
Fang, J., and J. Tu. 2019. “Effect of ultraviolet (UV) aging on rheology properties and microstructure of polyurethane (PU) modified asphalt.” Mater. Res. Express 6 (12): 125318. https://doi.org/10.1088/2053-1591/ab558f.
Fowkes, F. M. 1964. “Attractive forces at interfaces.” Ind. Eng. Chem. Res. 56 (12): 40–52. https://doi.org/10.1021/ie50660a008.
Gong, Y., J. Xu, R. Chang, and E. H. Yan. 2021. “Effect of water diffusion and thermal coupling condition on SBS modified asphalts’ surface micro properties.” Constr. Build. Mater. 273 (Mar): 121758. https://doi.org/10.1016/j.conbuildmat.2020.121758.
Hamedi, G. H., and F. M. Nejad. 2017. “Evaluating the effect of mix design and thermodynamics parameters on moisture sensitivity of hot mix design.” J. Mater. Civ. Eng. 29 (2): 04016207. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001734.
Han, X., X. Chen, X. Yang, and H. Bai. 2007. “Nanometer scale surface roughness measurement based on AFM.” [In Chinese.] J. Chongqing Univ. 1 (2): 5–8.
Ji, X., Y. Hou, H. Zou, B. Chen, and Y. Jiang. 2020a. “Study of surface microscopic properties of asphalt based on atomic force microscopy.” Constr. Build. Mater. 242 (May): 118025. https://doi.org/10.1016/j.conbuildmat.2020.118025.
Ji, X., J. Li, X. Zhai, H. Zou, and B. Chen. 2020b. “Application of atomic force microscope to investigate the surface micro-adhesion properties of asphalt.” Materials (Basel) 13 (7): 1736. https://doi.org/10.3390/ma13071736.
Ji, X., E. Sun, H. Zou, Y. Hou, and B. Chen. 2020c. “Study on the multiscale adhesive properties between asphalt and aggregate.” Constr. Build. Mater. 249 (Jul): 118693. https://doi.org/10.1016/j.conbuildmat.2020.118693.
Johnson, K. L., K. Kendall, and A. D. Roberts. 1971. “Surface energy and the contact of elastic solids.” Proc. R. Soc. London, Ser. A 324 (1558): 301–313. https://doi.org/10.1098/rspa.1971.0141.
Li, C., J. Zheng, Z. Zhang, A. Sha, and J. Li. 2020. “Morphology-based indices and recommended sampling sizes for using image-based methods to quantify degradations of compacted aggregate materials.” Constr. Build. Mater. 230 (Jan): 116970. https://doi.org/10.1016/j.conbuildmat.2019.116970.
Liu, K., L. Deng, J. Zheng, and K. Jiang. 2016. “Moisture induced damage of various asphalt binders.” [In Chinese.] Chin. J. Mater. Res. 30 (10): 773–780.
Liu, L., C. Xin, and M. Wang. 2018. “A method of determination of micro scale properties of asphalt components in mixtures based on atomic force microscopy.” J. Tongji Univ. (Nat. Sci.) 46 (9): 1218–1224. https://doi.org/10.11908/j.issn.0253-374x.2018.09.009.
Liu, X., A. Sha, C. Li, Z. Zhang, and H. Li. 2020. “Influence of water on warm-modified asphalt: Views from adhesion, morphology and chemical characteristics.” Constr. Build. Mater. 264 (Dec): 120159. https://doi.org/10.1016/j.conbuildmat.2020.120159.
Macedo, T. F., G. A. Badilla-Vargas, P. H. Osmari, A. D. de Oliveira, R. A. Simao, L. F. M. Leite, and F. T. S. Aragao. 2020. “An experimental testing and analysis procedure to determine linear viscoelastic properties of asphalt binder microstructural components.” Constr. Build. Mater. 230 (Jan): 116999. https://doi.org/10.1016/j.conbuildmat.2019.116999.
Ministry of Transport of the People’s Republic of China. 2011. Standard test methods of bitumen and bituminous mixtures for highway engineering. JTG E20-2011. Beijing: China Communication Press.
Nguyen, T., W. E. Byrd, D. P. Bentz, and J. F. Seiler. 1992. Development of a technique for in-situ measurement of water at the asphalt/model siliceous aggregate interface. Washington, DC: Strategic Highway Research Program, National Research Council.
Sengoz, B., and E. Agar. 2007. “Effect of asphalt film thickness on the moisture sensitivity characteristics of hot-mix asphalt.” Build. Environ. 42 (10): 3621–3628. https://doi.org/10.1016/j.buildenv.2006.10.006.
Sheng, Y., L. Li, J. Geng, and Z. Zhang. 2018. “Influence of humidity on aging of SBS modified asphalt.” [In Chinese.] J. China Foreign Highway 38 (4): 283–286.
Song, Y., X. Wang, and Y. Zhang. 2011. “Moisture damage-component of road asphalt and its influencing factors.” [In Chinese.] J. China Univ. Pet. (Ed. Nat. Sci.) 35 (4): 172–176.
Tomanovic, A., and C. Maksimovic. 1996. “Improved modelling of suspended solids discharge from asphalt surface during storm event.” Water Sci. Technol. 33 (4–5): 363–369. https://doi.org/10.1016/0273-1223(96)00253-3.
Vasconcelos, K. L., A. Bhasin, and D. N. Little. 2011. “History dependence of water diffusion in asphalt binders.” Int. J. Pavement Eng. 12 (5): 497–506. https://doi.org/10.1080/10298436.2010.535536.
Wang, C., Q. Chen, T. Guo, and Q. Li. 2020a. “Environmental effects and enhancement mechanism of graphene/tourmaline composites.” J. Cleaner Prod. 262 (Jul): 121313. https://doi.org/10.1016/j.jclepro.2020.121313.
Wang, H., Y. Guo, A. Shen, X. Yang, and P. Li. 2020b. “Effect of nanoclays on moisture susceptibility of SBS-modified asphalt binder.” [In Chinese.] Adv. Mater. Sci. Eng. 2020 (1): 1–15.
Wang, X., X. Gu, X. Hu, Q. Zhang, and Q. Dong. 2020c. “Three-stage evolution of air voids and deformation of porous-asphalt mixtures in high-temperature permanent deformation.” J. Mater. Civ. Eng. 32 (9): 04020233. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003300.
Wei, J. 2008. “Study on surface free energy of asphalt, aggregate and moisture diffusion in asphalt.” Ph.D. thesis, College of Chemistry & Chemical Engineering, China Univ. of Petroleum (East China).
Wei, W. 2012. “Research on the hot-bonding technique in waterproof of asphalt concrete bridge deck.” Master’s thesis, School of Transportation Science and Engineering, Harbin Institute of Technology.
Xu, M., J. Yi, D. Feng, Y. Huang, and D. Wang. 2016. “Analysis of adhesive characteristics of asphalt based on atomic force microscopy and molecular dynamics simulation.” ACS Appl. Mater. Interfaces 8 (19): 12393–12403. https://doi.org/10.1021/acsami.6b01598.
Yang, J., X. Zhu, Y. Yuan, and L. Li. 2020. “Effects of aging on micromechanical properties of asphalt binder using AFM.” J. Mater. Civ. Eng. 32 (5): 04020081. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003030.
Yi, J., X. Pang, D. Feng, Z. Pei, M. Xu, S. Xie, and Y. Huang. 2017a. “Studies on surface energy of asphalt and aggregate at different scales and bonding property of asphalt–aggregate system.” Road Mater. Pavement Des. 19 (5): 1102–1125. https://doi.org/10.1080/14680629.2017.1300597.
Yi, J., X. Pang, and D. Yao. 2017b. “Characterization of surface roughness and adhesive mechanism of asphalt and mineral aggregate based on atomic force microscopy method.” [In Chinese.] Acta Mater. Compos. Sin. 34 (5): 1111–1121.
Zhang, H., Y. Wang, T. Yu, and Z. Liu. 2020. “Microstructural characteristics of differently aged asphalt samples based on atomic force microscopy (AFM).” Constr. Build. Mater. 255 (Sep): 119388. https://doi.org/10.1016/j.conbuildmat.2020.119388.
Zhu, J., K. Zhang, K. Liu, and X. Shi. 2020. “Adhesion characteristics of graphene oxide modified asphalt unveiled by surface free energy and AFM-scanned micro-morphology.” Constr. Build. Mater. 244 (May): 118404. https://doi.org/10.1016/j.conbuildmat.2020.118404.
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Received: Aug 13, 2021
Accepted: Jan 27, 2022
Published online: Jul 20, 2022
Published in print: Oct 1, 2022
Discussion open until: Dec 20, 2022
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