Effects of Capsules Containing Waste Oils on the Mechanical Properties of Hot Mix Asphalt: Experimental Approach
Publication: Journal of Materials in Civil Engineering
Volume 33, Issue 9
Abstract
Self-healing asphalt with encapsulated rejuvenators is a promising technology to improve the service life of asphalt pavements. Broken capsules reduce the viscosity of aged bitumen due to rejuvenator diffusion, sealing open microcracks at an early stage. Several waste oils have been used as low-cost rejuvenating agents in capsule production to reduce costs and enable the environmental benefits of this technology. This study aims to evaluate the effects of capsules containing waste vegetable oil (WVO) and waste mineral oil (WMO) on the mechanical properties of hot mix asphalt (HMA). Four capsule content amounts (0.25%, 0.50%, 0.70%, and 1.00% by weight) were included in HMA samples, which were evaluated through experimental standard tests such as stiffness modulus, indirect tensile strength, fatigue life, and moisture-induced damage. The results revealed that an increase in capsule content led to less rigidity and strength against permanent deformation and fatigue. It was also determined that the strength against permanent deformation of mixtures with WMO capsules increased more than that of mixtures with WVO capsules. Another finding is that the optimum capsule content ratio in asphalt mixtures is 0.50% by weight for both capsule types.
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Data Availability Statement
Some or all data, models, or code that support the findings of this study are available from the corresponding author upon reasonable request.
Acknowledgments
This study was conducted under the supervision of the Scientific and Technological Research Council of Turkey (TUBITAK). We gratefully acknowledge the financial support provided by TUBITAK to Research Project 217M570.
References
AASHTO. 2008. Standard method of test for softening point of bitumen (ring-and-ball apparatus). AASHTO T 53-06. Washington, DC: AASHTO.
AASHTO. 2014. Standard method of test for resistance of compacted hot mix asphalt (HMA) to moisture-induced damage. Washington, DC: AASHTO.
AASHTO. 2015. Method of test for penetration of bituminous materials. AASHTO T 49. Washington, DC: AASHTO.
Al-Mansoori, T., J. Norambuena-Contreras, R. Micaelo, and A. Garcia. 2018. “Self-healing of asphalt mastic by the action of polymeric capsules containing rejuvenators.” Constr. Build. Mater. 161 (Feb): 330–339. https://doi.org/10.1016/j.conbuildmat.2017.11.125.
ASTM. 2018. Standard test method for density of semi-solid asphalt binder (pycnometer method). ASTM D70-18a. West Conshohocken, PA: ASTM.
British Standards Institution. 1997. Method for determination of the fatigue characteristics of bituminous mixtures using indirect tensile fatigue. BS DD ABE. London: British Standards Institution.
British Standards Institution. 1993. Method for determination of the indirect tensile stiffness modulus of bituminous mixtures. BS DD 213. London: British Standards Institution.
Chung, K., S. Lee, W. Cho, J. Seo, and Y. Hong. 2018. “Rheological analysis of self-healing property of microcapsule-containing asphalt.” J. Ind. Eng. Chem. 64 (Aug): 284–291. https://doi.org/10.1016/j.jiec.2018.03.026.
Garcia, A., J. Jelfs, and C. J. Austin. 2015. “Internal asphalt mixture rejuvenation using capsules.” Constr. Build. Mater. 101 (Dec): 309–316. https://doi.org/10.1016/j.conbuildmat.2015.10.062.
Goh, S. W., and Z. You. 2009. “A simple stepwise method to determine and evaluate the initiation of tertiary flow for asphalt mixtures under dynamic creep test.” Constr. Build. Mater. 23 (11): 3398–3405. https://doi.org/10.1016/j.conbuildmat.2009.06.020.
Gonzalez-Torre, I., and J. Norambuena-Contreras. 2020. “Recent advances on self-healing of bituminous materials by the action of encapsulated rejuvenators.” Constr. Build. Mater. 258 (Oct): 119568. https://doi.org/10.1016/j.conbuildmat.2020.119568.
Haghshenas, H. F., R. Rea, G. Reinke, and D. F. Haghshenas. 2020. “Chemical characterization of recycling agents.” J. Mater. Civ. Eng. 32 (5): 06020005. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003167.
Leo, W. J., A. J. McLoughlin, and D. M. Malone. 1990. “Effects of sterilization treatments on some properties of alginate solutions and gels.” Biotechnol. Progr. 6 (1): 51–53. https://doi.org/10.1021/bp00001a008.
Li, B., G. Sun, D. Sun, T. Lu, J. Ma, and Y. Deng. 2020. “Survival and activation behavior of microcapsules in self-healing asphalt mixture.” Constr. Build. Mater. 260 (Nov): 119719. https://doi.org/10.1016/j.conbuildmat.2020.119719.
Micaelo, R., T. Al-Mansoori, and A. Garcia. 2016. “Study of the mechanical properties and self-healing ability of asphalt mixture containing calcium-alginate capsules.” Constr. Build. Mater. 123 (Oct): 734–744. https://doi.org/10.1016/j.conbuildmat.2016.07.095.
Norambuena-Contreras, J., L. E. Arteaga-Perez, A. Y. Guadarrama-Lezama, R. Briones, J. F. Vivanco, and I. Gonzalez-Torre. 2020. “Microencapsulated bio-based rejuvenators for the self-healing of bituminous materials.” Materials (Basel) 13 (6): 1446. https://doi.org/10.3390/ma13061446.
Norambuena-Contreras, J., Q. Liu, L. Zhang, S. Wu, E. Yalcin, and A. Garcia. 2019. “Influence of encapsulated sunflower oil on the mechanical and self-healing properties of dense-graded asphalt mixtures.” Mater. Struct. 52 (4): 78. https://doi.org/10.1617/s11527-019-1376-3.
Norambuena-Contreras, J., E. Yalcin, A. Garcia, T. Al-Mansoori, M. Yilmaz, and R. Hudson-Griffiths. 2018. “Effect of mixing and ageing on the mechanical and self-healing properties of asphalt mixtures containing polymeric capsules.” Constr. Build. Mater. 175 (Jun): 254–266. https://doi.org/10.1016/j.conbuildmat.2018.04.153.
Read, J., and D. Whiteoak. 2003. The shell bitumen handbook. London: Thomas Telford.
Sengöz, B., and A. Topal. 2005. “Use of asphalt roofing shingle waste in HMA.” Constr. Build. Mater. 19 (5): 1890–1894. https://doi.org/10.1016/j.conbuildmat.2004.08.005.
Shirzad, S., M. M. Hassan, M. A. Aguirre, L. N. Mohammad, S. Cooper, and I. I. Negulescu. 2017. “Microencapsulated sunflower oil for rejuvenation and healing of asphalt mixtures.” J. Mater. Civ. Eng. 29 (9): 04017147. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001988.
Shirzad, S., M. M. Hassan, M. A. Aguirre, L. N. Mohammad, and W. H. Daly. 2016. “Evaluation of sunflower oil as a rejuvenator and its microencapsulation as a healing agent.” J. Mater. Civ. Eng. 28 (11): 04016116. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001625.
Su, J. F., J. Qiu, and H. Schlangen. 2013. “Self-healing bitumen by microcapsules containing rejuvenator.” In Proc., 4th Int. Conf. on Self-Healing Materials. Delft, Netherlands: Delft Univ. of Technology.
Su, J.-F., and E. Schlangen. 2012. “Synthesis and physicochemical properties of high compact microcapsules containing rejuvenator applied in asphalt.” Chem. Eng. J. 198–199 (Aug): 289–300. https://doi.org/10.1016/j.cej.2012.05.094.
Sun, D., B. Li, F. Ye, X. Zhu, T. Lu, and Y. Tian. 2018a. “Fatigue behavior of microcapsule-induced self-healing asphalt concrete.” J. Cleaner Prod. 188 (Jul): 466–476. https://doi.org/10.1016/j.jclepro.2018.03.281.
Sun, D., G. Sun, X. Zhu, A. Guarin, B. Li, Z. Dai, and J. Ling. 2018b. “A comprehensive review on self-healing of asphalt materials: Mechanism, model, characterization and enhancement.” Adv. Colloid Interface Sci. 256 (Jun): 65–93. https://doi.org/10.1016/j.cis.2018.05.003.
Tabaković, A., and E. Schlangen. 2016. “Self-healing technology for asphalt pavements.” Adv. Polymer Sci. 1–22. https://doi.org/10.1007%2F12_2015_335.
TSE (Turkish Standards Institution). 2008. Determination of flash point—Pensky-Martens closed cup method. TS EN ISO 2719. Ankara, Turkey: Turkish Standards Institution.
TSE (Turkish Standards Institution). 2014. Bitumen and bituminous binders—Determination of solubility. TS EN 12592. Ankara, Turkey: Turkish Standards Institution.
Wu, S., L. Pang, L. Mo, J. Qiu, G. Zhu, and Y. Xiao. 2008. “UV and thermal aging of pure bitumen—Comparison between laboratory simulation and natural exposure aging.” Road Mater. Pavement Des. 9 (1): 103–113. https://doi.org/10.1080/14680629.2008.9690161.
Xu, S., A. Tabaković, X. Liu, and E. Schlangen. 2018. “Calcium alginate capsules encapsulating rejuvenator as healing system for asphalt mastic.” Constr. Build. Mater. 169 (Apr): 379–387. https://doi.org/10.1016/j.conbuildmat.2018.01.046.
Yamaç, Ö. E., M. Yilmaz, E. Yalçın, B. V. Kök, J. Norambuena-Contreras, and A. Garcia. 2020. “Self-healing of asphalt mastic using capsules containing waste oils.” Constr. Build. Mater. 270 (Feb): 121417. https://doi.org/10.1016/j.conbuildmat.2020.121417.
Zaremotekhases, F., I. I. Idris, M. M. Hassan, L. N. Mohammad, and I. I. Negulescu. 2020. “Effect of sodium alginate fibers encapsulating rejuvenators on the self-healing capability and cracking resistance of asphalt mixtures.” J. Mater. Civ. Eng. 32 (12): 04020355. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003440.
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Received: Oct 7, 2020
Accepted: Mar 1, 2021
Published online: Jul 13, 2021
Published in print: Sep 1, 2021
Discussion open until: Dec 13, 2021
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