Technical Papers
Jan 6, 2021

Synthesis of Ultralight Cement Using Solid Waste Fly Ash Cenosphere for Low-Fracture Gradient Formation with Reduced Shrinkage

Publication: Journal of Hazardous, Toxic, and Radioactive Waste
Volume 25, Issue 2

Abstract

The significant generation of fly ash from coal fired thermal power plants tends to cause air pollution and health hazards. The cenospheres that are a component of fly ash are spherical in shape, light density, and particle size ranges from 100 to 400 μm. Therefore, for the effective utilization of this solid waste, in this study, an ultralight cement slurry will be prepared for low-fracture gradient formation by the incorporation of varying doses of fly ash cenospheres (FAC). The cement sheath often shrinks, which instigates fluid migration across the isolated zones. Therefore, for additional shrinkage compensation, dead burned magnesia (DBM) combined with FAC will be added to the cement slurry. The morphology of the cenospheres in the cement sheath will be observed using a scanning electron microscope (SEM). The water contact angle of 108.3° revealed that the cement sheath is hydrophobic. Moreover, the consistency test revealed that when 30% cenosphere was incorporated into the cement slurry it exhibited a consistency of 30 Bearden units of consistency (Bc) after 2 h, which resulted in better pumpability under downhole conditions. Furthermore, expansion studies will be conducted on the prepared cement slurry under permeable and impermeable conditions. In addition, the rheological properties and compressive strength of the cement slurries will be investigated. The prepared cement slurry exhibited a specific gravity of approximately 0.9 along with a compressive strength of approximately 24 MPa, which is acceptable for its application in oil well cement. Therefore, the solid waste cenosphere and DBM could provide a sustainable solution in oil well cementing for low-fracture gradient formation with improved zonal isolation.

Get full access to this article

View all available purchase options and get full access to this article.

Acknowledgments

The authors acknowledge their work to the Institute of Drilling Technology, ONGC, Dehradun, India for carrying out the experimental studies and characterization of the samples.

References

Adriano, D. C., A. L. Page, A. A. Elseewi, A. C. Chang, and I. Straughan. 1980. “Utilization and disposal of fly ash and other coal residues in terrestrial ecosystems: A review.” J. Environ. Qual. 9 (3): 333–344. https://doi.org/10.2134/jeq1980.00472425000900030001x.
Anshits, N. N., O. A. Mikhailova, A. N. Salanov, and A. G. Anshits. 2010. “Chemical composition and structure of the shell of fly ash non-perforated cenospheres produced from the combustion of the Kuznetsk coal (Russia).” Fuel 89 (8): 1849–1862. https://doi.org/10.1016/j.fuel.2010.03.049.
Ardeshirilajimi, A., and P. Mondal. 2019. “Effects of presoaked lightweight aggregate addition on drying shrinkage.” J. Mater. Civ. Eng. 31 (10): 04019211. https://doi.org/10.1061/(ASCE)MT.1943-5533.0002826.
Bora, P. J., M. Porwal, K. J. Vinoy, R. P. C. Kishore, and G. Madras. 2018. “Industrial waste fly ash cenosphere composites based broad band microwave absorber.” Composites, Part B 134: 151–163. https://doi.org/10.1016/j.compositesb.2017.09.062.
Borm, P. J. A. 1997. “Toxicity and occupational health hazards of coal fly ash (CFA). A review of data and comparison to coal mine dust.” Ann. Occup. Hyg. 41 (6): 659–676. https://doi.org/10.1016/S0003-4878(97)00026-4.
Bruton, J. R., C. D. Ivan, and T. J. Heinz. 2001. “Lost circulation control: Evolving techniques and strategies to reduce downhole mud losses.” In Vol. 1 of SPE/IADC Drilling Conf., 334–342. Richardson, TX: Society of Petroleum Engineers.
Bybee, K. 2006. “Drilling and cementing technology: New ultralightweight-cementing technology combines benefits of current leading methods.” J. Pet. Technol. 58 (2): 65–66. https://doi.org/10.2118/0206-0065-JPT.
Cavanagh, P. H., C. R. Johnson, S. Le Roy-Delage, G. G. DeBruijn, I. Cooper, D. J. Guillot, H. Bulte, and B. Dargaud. 2007. “Self-Healing cement—Novel technology to achieve leak-free wells.” In SPE/IADC Drilling Conf., 1–13. Richardson, TX: Society of Petroleum Engineers. https://doi.org/10.2118/105781-MS.
Chandane, V. S., A. P. Rathod, and K. L. Wasewar. 2017. “Coupling of in-situ pervaporation for the enhanced esterification of propionic acid with isobutyl alcohol over cenosphere based catalyst.” Chem. Eng. Process. 119: 16–24. https://doi.org/10.1016/j.cep.2017.05.015.
Chatterji, S. 1995. “Mechanism of expansion of concrete due to the presence of dead-burnt CaO and MgO.” Cem. Concr. Res. 25 (1): 51–56. https://doi.org/10.1016/0008-8846(94)00111-B.
Chu, I., S. H. Kwon, M. N. Amin, and J. K. Kim. 2012. “Estimation of temperature effects on autogenous shrinkage of concrete by a new prediction model.” Constr. Build. Mater. 35: 171–182. https://doi.org/10.1016/j.conbuildmat.2012.03.005.
Gupta, D. K., U. N. Rai, R. D. Tripathi, and M. Inouhe. 2002. “Impacts of fly-ash on soil and plant responses.” J. Plant Res. 115 (6): 401–409. https://doi.org/10.1007/s10265-002-0057-3.
Gursinsky, T., S. Ruhs, U. Friess, S. Diabaté, H. F. Krug, R. E. Silber, and A. Simm. 2006. “Air pollution-associated fly ash particles induce fibrotic mechanisms in primary fibroblasts.” Biol. Chem. 387 (10–11): 1411–1420. https://doi.org/10.1515/BC.2006.177.
Halkyard, J., M. R. Anderson, and W. C. Maurer. 2014. “Hollow glass microspheres: An option for dual gradient drilling and deep ocean mining lift.” In Annual Offshore Technology Conf., 3078–3095. Richardson, TX: Offshore Technology Conference. https://doi.org/10.4043/25044-MS.
Hanif, A., Z. Lu, and Z. Li. 2017. “Utilization of fly ash cenosphere as lightweight filler in cement-based composites—A review.” Constr. Build. Mater. 144: 373–384. https://doi.org/10.1016/j.conbuildmat.2017.03.188.
Jackson, R. B., A. Vengosh, T. H. Darrah, N. R. Warner, A. Down, R. J. Poreda, S. G. Osborn, K. Zhao, and J. D. Karr. 2013. “Increased stray gas abundance in a subset of drinking water wells near Marcellus shale gas extraction.” Proc. Natl. Acad. Sci. 110 (28): 11250–11255. https://doi.org/10.1073/pnas.1221635110.
Jahanbakhshi, R., and R. Keshavarzi. 2015. “Quantitative and qualitative analysis of lost circulation in natural and induced fractured formations: The integration of operational conditions and geomechanical parameters.” Eur. J. Environ. Civ. Eng. 19 (4): 418–444. https://doi.org/10.1080/19648189.2014.949872.
Jang, J. K., H. G. Kim, J. H. Kim, and J. S. Ryou. 2018. “The evaluation of damage effects on MgO added concrete with slag cement exposed to calcium chloride deicing salt.” Materials 11 (5): 793. https://doi.org/10.3390/ma11050793.
Kearsley, E. P., and P. J. Wainwright. 2001. “Porosity and permeability of foamed concrete.” Cem. Concr. Res. 31 (5): 805–812. https://doi.org/10.1016/S0008-8846(01)00490-2.
Kremieniewski, M. 2020. “Recipe of lightweight slurry with high early strength of the resultant cement sheath.” Energies 13 (7): 1583. https://doi.org/10.3390/en13071583.
Kucharczyková, B., P. Daněk, D. Kocáb, and P. Misák. 2017. “Experimental analysis on shrinkage and swelling in ordinary concrete.” Adv. Mater. Sci. Eng. 2017: 3027301. https://doi.org/10.1155/2017/3027301.
Liu, Z., K. Zhao, Y. Tang, and C. Hu. 2019. “Preparation of a cenosphere curing agent and its application to foam concrete.” Adv. Mater. Sci. Eng. 2019: 7523492. https://doi.org/10.1155/2019/7523492.
McBride, S. P., A. Shukla, and A. Bose. 2002. “Processing and characterization of a lightweight concrete using cenospheres.” J. Mater. Sci. 37 (19): 4217–4225. https://doi.org/10.1023/A:1020056407402.
Ngu, L. N., H. Wu, and D. K. Zhang. 2007. “Characterisation of cenospheres in fly ash from Australian power stations.” Energy Fuels 21 (6): 3437–3445. https://doi.org/10.1021/ef700340k.
Rewatkar, M. R. 2019. “Experimental investigation on cenosphere-based paper battery and electrochemical battery.” Energy Sourc., Part A 42 (16): 2018–2033. https://doi.org/10.1080/15567036.2019.1607924.
Richhariya, G., D. T. K. Dora, P. P. Kundu, N. Singal, Y. Gupta, and P. Singh. 2019. “Impregnation of novel additives in cement for preventing fluid migration through the cement sheath in oil well.” AIP Conf. Proc. 2166: 020024. https://doi.org/10.1063/1.5131611.
Richhariya, G., D. T. K. Dora, K. R. Parmar, K. K. Pant, N. Singhal, K. Lal, and P. P. Kundu. 2020. “Development of self-healing cement slurry through the incorporation of dual-encapsulated polyacrylamide for the prevention of water ingress in oil well.” Materials 13 (13): 2921–2922. https://doi.org/10.3390/ma13132921.
Roy, S., and D. S. Chapman. 2012. “Borehole temperatures and climate change : Ground temperature change in south India over the past two centuries.” J. Geophys. Res. 117: 1–12. https://doi.org/10.1029/2011JD017224.
Rugele, K., D. Lehmhus, I. Hussainova, J. Peculevica, M. Lisnanskis, and A. Shishkin. 2017. “Effect of fly-ash cenospheres on properties of clay-ceramic syntactic foams.” Materials 10 (7): 828. https://doi.org/10.3390/ma10070828.
Sarmah, P., P. Yadav, and G. Agrawal. 2015. “High-strength lightweight cement optimized for weak formations—Use of local raw material improves performance and operational latitude.” In SPE Oil & Gas India Conf. and Exhibition, 1–14. Richardson, TX: Society of Petroleum Engineers, https://doi.org/10.3390/ma10070828.
Sasaki, T., K. Soga, and M. Abuhaikal. 2018. “Water absorption and shrinkage behaviour of early-age cement in wellbore annulus.” J. Pet. Sci. Eng. 169: 205–219. https://doi.org/10.1016/j.petrol.2018.05.065.
Satpathy, H. P., S. K. Patel, and A. N. Nayak. 2019. “Development of sustainable lightweight concrete using fly ash cenosphere and sintered fly ash aggregate.” Constr. Build. Mater. 202: 636–655. https://doi.org/10.1016/j.conbuildmat.2019.01.034.
Sauki, A., M. I. Juanda, A. Azizi, M. Asadullah, T. A. Tengku Mohd, N. A. Ghazali, and N. H. Alias. 2015. “Performance evaluation of lightweight oilwell cements.” Adv. Mater. Res. 1119: 657–661. https://doi.org/10.4028/www.scientific.net/AMR.1119.657.
Shahidan, S., E. Aminuddin, K. Mohd Noor, N. I. R. Ramzi Hannan, and N. A. Saiful Bahari. 2017. “Potential of hollow glass microsphere as cement replacement for lightweight foam concrete on thermal insulation performance.” MATEC Web Conf. 103: 01014. https://doi.org/10.1051/matecconf/201710301014.
Snoeck, D., O. M. Jensen, and N. De Belie. 2015. “The influence of superabsorbent polymers on the autogenous shrinkage properties of cement pastes with supplementary cementitious materials.” Cem. Concr. Res. 74: 59–67. https://doi.org/10.1016/j.cemconres.2015.03.020.
Suppe, J. 2014. “Fluid overpressures and strength of the sedimentary upper crust.” J. Struct. Geol. 69: 481–492. https://doi.org/10.1016/j.jsg.2014.07.009.
Trezza, M. A. 2007. “Hydration study of ordinary portland cement in the presence of zinc ions.” Mater. Res. 10 (4): 331–334. https://doi.org/10.1590/S1516-14392007000400002.
Vidic, R. D., S. L. Brantley, J. M. Vandenbossche, D. Yoxtheimer, and J. D. Abad. 2013. “Impact of shale gas development on regional water quality.” Science 340 (6134): 1235009. https://doi.org/10.1126/science.1235009.
Vidick, B., J. A. Yearwood, and H. Perthuis. 1988. “How to solve lost circulation problems.” In Int. Meeting on Petroleum Engineering, 927–932. Richardson, TX: Society of Petroleum Engineers. https://doi.org/10.2118/17811-MS.

Information & Authors

Information

Published In

Go to Journal of Hazardous, Toxic, and Radioactive Waste
Journal of Hazardous, Toxic, and Radioactive Waste
Volume 25Issue 2April 2021

History

Received: May 29, 2020
Accepted: Oct 12, 2020
Published online: Jan 6, 2021
Published in print: Apr 1, 2021
Discussion open until: Jun 6, 2021

Permissions

Request permissions for this article.

Authors

Affiliations

Gaurav Richhariya [email protected]
Assistant Professor, Dept. of Petroleum and Energy Studies, DIT Univ., Dehradun 248009, India. Email: [email protected]
Assistant Professor, Dept. of Petroleum and Energy Studies, DIT Univ., Dehradun 248009, India (corresponding author). ORCID: https://orcid.org/0000-0001-5412-6360. Email: [email protected]
Naveen Singhal [email protected]
Professor, Dept. of Chemistry, DIT Univ., Dehradun 248009, India. Email: [email protected]

Metrics & Citations

Metrics

Citations

Download citation

If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.

Cited by

View Options

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Media

Figures

Other

Tables

Share

Share

Copy the content Link

Share with email

Email a colleague

Share