TECHNICAL NOTES
May 1, 2007

Change in Microporosity of Granitic Building Stones upon Consolidation Treatments

Publication: Journal of Materials in Civil Engineering
Volume 19, Issue 5

Abstract

The microporosity of granite stones has been studied in both the untreated condition as well as after being treated with a consolidation treatment using two commercial products. A decrease in the specific surface area and pore size distribution (especially micropores) has been found in samples treated with an organic silicate consolidant. Treatment with a consolidant containing polysiloxane (a water repellent agent) leads to variable results, depending on the precise pore structure of the untreated stone. The use of consolidation treatments may restrict flow of fluids (e.g., water, saline solutions, etc.) through the pores of the stones, which may decrease degradation.

Get full access to this article

View all available purchase options and get full access to this article.

Acknowledgments

The writers thank the financial support from Junta de Castilla y León (CSI08/03) and MEC (MAT2004-04498 and CGL2004-07066-CO2-02/BTE). This work is dedicated to the beloved memory of Dr. M. Angeles Vicente.

References

Davidson, A. T. (1985). “WH Committee: Report of 9th Session, Paris 1985.” ⟨http://whc.unesco.org/archive/repcom85.htm#348⟩ (June 14, 2001).
Hammecker, C., Esbert, R. M., and Jeannette, D. (1992). “Geometry modifications of porous network in carbonate rocks by ethyl silicate treatment.” Proc., 7th Int. Congress on Deterioration and Conservation of Stone, Laboratório Nacional de Engenharia Civil, Lisbon, Portugal, Vol. 3, 1053–1062.
Iñigo, A. C., García-Talegón, J., Molina, E., Perez-Rodriguez, J. L., Vargas, M., and Vicente, M. A. (1994). “Granites employed in Avila (Spain): II—Petrophysical characteristics.” Mater. Constr., 44(233), 28–37.
Iñigo, A. C., García-Talegón, J., Trulillano, R., and Vicente-Tavera, S. (1996). “Influence of consolidation and hydrofugation treatments on the physical properties of Avila natural and artificially aged granite: A statistical approach.” Proc., EC Worshop on Degradation and Conservation of Granitic Rocks in Monuments, Protection, and Conservation of European Cultural Heritage, Research Rep. No. 5, Santiago de Compostela, Spain, 145–151.
Iñigo, A. C., Vicente, M. A., and Rives, V. (2000). “Weathering and decay of granitic rocks: its relation to their pore network.” Mech. Mater., 32(9), 555–560.
Iñigo, A. C., Vicente-Tavera, S., Vicente, M. A., and Rives, V. (2001). “Effect of treatments on pore network of granites.” J. Mater. Civ. Eng., 13(3), 166–168.
Lowell, S., and Shields, J. E. (1984). Powder surface area and porosity, Chapman and Hall, London.
Meng, B. (1993). “Characterization of pore structure for the interpretation of moisture transport.” Proc., Int. RILEM/UNESCO Congress on Conservation of Stone and Other Materials, RILEM/UNESCO, Paris, Vol. 1, 155–162.
Norme Française (NF). (1973a). “Mesures de la porosité, de la masse volumique réelle et de la masse volumique apparente.” B10-503, AFNOR, Paris La Defense, France (in French).
Norme Française (NF). (1973b). “Mesure du coeficient de absortion déau.” B10-504, AFNOR, Paris La Défense, France (in French).
NORMAL. (1981) “Assorbimento d’acqua per immersione totale, capacita’ di imbibizione.” CNR-ICR 7/81, Comas grafica s. r. l., Rome (in Italian).
NORMAL. (1986a). “Interventi conservativi: Progettazione esecuzione e valutazione Preventiva.” CNR-ICR 20/85, Comas Grafica s.r.l., Rome (in Italian).
NORMAL. (1986b). “Assorbimento d’acqua per capillaritá, coefficiente di assorbimento capillare.” CNR-ICR 11/85, Comas Grafica s.r.l., Rome (in Italian).
RILEM. (1980). “Coefficient de conductivité de vapeur d’eau.” Mater. Struct., 13(75), 196–198 (in French).
Rives, V. (1991). “A computer program for analyzing nitrogen adsorption isotherms on porous solids.” Adsorpt. Sci. Technol., 8(2), 95–103.
Sing, K. S. W., Everett, D. H., Haul, R. A. W., Moscou, L., Pierotti, R. A, Rouquerol, J., and Siemieniewska, T. (1985). “Reporting physisorption data for gas solid systems with special reference to the determination of surface-area and porosity (recommendations 1984).” Pure Appl. Chem., 57(4), 603–619.
Valdeón, L., Grossi, C. M., Marcos, R. M., and Esbert, R. M. (1992). “Effect of conservation treatments on hydric properties of stones.” Proc., 7th Int. Congress on Deterioration and Conservation of Stone, Laboratório Nacional de Engenharia Civil, Lisbon, Portugal, 3, 1073–1081.

Information & Authors

Information

Published In

Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 19Issue 5May 2007
Pages: 437 - 440

History

Accepted: May 22, 2006
Received: Aug 26, 2006
Published online: May 1, 2007
Published in print: May 2007

Permissions

Request permissions for this article.

Notes

Note. Associate Editor: Jason Weiss

Authors

Affiliations

A. C. Iñigo, Ph.D. [email protected]
Scientist, IRNA/CSIC of Salamanca, Cordel de Merinas 40-52, 37008 Salamanca, Spain. E-mail: [email protected]
J. F. Supit, Ph.D. [email protected]
Postdoctoral Grant IRNA/CSIC of Salamanca, Cordel de Merinas 40-52, 37008 Salamanca, Spain. E-mail: [email protected]
O. Prieto, Ph.D. [email protected]
Postdoctoral Grant, Univ. of Salamanca, Plaza de Los Caídos, s/n, 37008 Salamanca, Spain. E-mail: [email protected]
V. Rives, Ph.D. [email protected]
Full Professor, Dept. of Inorganic Chemistry, Univ. of Salamanca, Plaza de los Caídos, s/n, 37008 Salamanca, Spain. E-mail: [email protected]

Metrics & Citations

Metrics

Citations

Download citation

If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.

Cited by

View Options

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Media

Figures

Other

Tables

Share

Share

Copy the content Link

Share with email

Email a colleague

Share