Technical Papers
Sep 22, 2022

Investigation of Curing and Strength Characteristics of Cold-Mix Asphalt with Rice Husk Ash–Activated Fillers

Publication: Journal of Transportation Engineering, Part B: Pavements
Volume 148, Issue 4

Abstract

Presently, the application of cold-mix asphalt (CMA) in structural layers of pavement is limited due to the slow curing rate and low early-life strength. This study attempts to achieve the reduction in curing period and improvement in strength development of CMA by using nonconventional fillers (NCFs) such as fly ash, ground granulated blast-furnace slag (GGBS), rice husk ash (RHA), and fly ash and GGBS activated with RHA. Curing rate was evaluated using moisture loss monitoring of mixture and compacted specimens of CMA. Strength development was evaluated using indirect tensile strength testing and wheel tracking testing. Laboratory investigations revealed that curing period and temperature have a significant impact on the rate of moisture loss and strength gain. Mechanical strength increased with the increase in curing period and temperature for cold mixes with NCFs. CMA with GGBS activated using RHA exhibited higher curing rates than conventional CMA and substantially higher early-strength development among all the mixes considered. This is due to the combined effect of moisture loss and accelerated hydration process. Statistical analysis also indicated that the improvement was significant. Thus, the use of GGBS with RHA as activator by partial replacement of mineral filler is a potential solution to prolonged curing period and weak early-life strength of CMA.

Practical Applications

Cold-mix asphalt is a sustainable paving mix with economic and environmental advantages. All the steps involved in the construction of the road using a cold mix are done at ambient temperature. Increasing the application of cold-mix asphalt is highly essential. The long time required for curing and the low early strength deter the extensive use of cold mixing in the field. This study suggests that the use of cold mixes in which ground granulated blast-furnace slag with rice husk ash are incorporated as filler helps in resolving these issues by increasing the curing rate and early strength of cold mixes. The study recommends using 25% stone dust, 50% ground granulated blast-furnace slag, and 25% rice husk ash as filler. Because ground granulated blast-furnace slag and rice husk ash are industrial and agricultural waste materials, respectively, using these materials is a sustainable way of resolving the problems of cold mixing. Also, as these materials are easily available, and the modified mix can be easily produced; this can be conveniently implemented in the field. This can pave the way to the use of cold mixing in the top layer of heavily trafficked roads as well.

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Data Availability Statement

All data, models, or code that support the findings of this study are available from the corresponding author upon reasonable request.

Acknowledgments

The authors thank the Centre for Transportation Research, Department of Civil Engineering, National Institute of Technology Calicut, Kerala, India, for its support for this research.

References

AASHTO. 2019. Standard method of test for Hamburg wheel-track testing of compacted asphalt mixtures. AASHTO T 324. Washington, DC: AASHTO.
Al-Busaltan, S., H. Al Nageim, W. Atherton, and G. Sharples. 2012. “Mechanical properties of an upgrading cold-mix asphalt using waste materials.” J. Mater. Civ. Eng. 24 (12): 1484–1491. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000540.
Al-Hdabi, A., and H. Al Nageim. 2017. “Improving asphalt emulsion mixtures properties containing cementitious filler by adding GGBS.” J. Mater. Civ. Eng. 29 (5): 04016297. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001859.
ASTM. 2015a. Standard test method for relative density (specific gravity) and absorption of coarse aggregate. ASTM C127-15. West Conshohocken, PA: ASTM.
ASTM. 2015b. Standard test method for relative density (specific gravity) and absorption of fine aggregate. ASTM C128-15. West Conshohocken, PA: ASTM.
ASTM. 2016. Standard test method for residue by evaporation of emulsified asphalt. ASTM D6934-08. West Conshohocken, PA: ASTM.
ASTM. 2017a. Standard test method for ductility of asphalt materials. ASTM D113-17. West Conshohocken, PA: ASTM.
ASTM. 2017b. Standard test method for indirect tensile (IDT) strength of asphalt mixtures. ASTM D6931–17. West Conshohocken, PA: ASTM.
ASTM. 2017c. Standard test methods and practices for emulsified asphalts. ASTM D244-09. West Conshohocken, PA: ASTM.
ASTM. 2017d. Standard test methods for uncompacted void content of fine aggregate (as influenced by particle shape, surface texture, and grading). ASTM C1252-17. West Conshohocken, PA: ASTM.
ASTM. 2018a. Standard test method for oversized particles in emulsified asphalts (Sieve Test). ASTM D6933-18. West Conshohocken, PA: ASTM.
ASTM. 2018b. Standard test method for viscosity of emulsified asphalt by Saybolt Furol viscometer. ASTM D7496-18. West Conshohocken, PA: ASTM.
ASTM. 2019a. Standard test method for flat particles, elongated particles, or flat and elongated particles in coarse aggregate. ASTM D4791-19. West Conshohocken, PA: ASTM.
ASTM. 2019b. Standard test method for settlement and storage stability of emulsified asphalts. ASTM D6930-19. West Conshohocken, PA: ASTM.
ASTM. 2020a. Standard test method for penetration of bituminous materials. ASTM D5/D5M-20. West Conshohocken, PA: ASTM.
ASTM. 2020b. Standard test method for resistance to degradation of small-size coarse aggregate by abrasion and impact in the Los Angeles machine. ASTM C131/C131M-20. West Conshohocken, PA: ASTM.
ASTM. 2021. Standard practice for evaluating the effect of freezing on emulsified asphalts. ASTM D6929-21. West Conshohocken, PA: ASTM.
BIS (Bureau of Indian Standards). 1963a. Methods of test for aggregates for concrete (P-I): Particle size and shape. BIS: 2386 (Part 1). New Delhi, India: BIS.
BIS (Bureau of Indian Standards). 1963b. Methods of test for aggregates for concrete (P-III): Specific gravity, density, voids, absorption, bulking. BIS: 2386 (Part 3). New Delhi, India: BIS.
BIS (Bureau of Indian Standards). 1963c. Methods of test for aggregates for concrete (P-IV): Mechanical properties. BIS: 2386 (Part 4). New Delhi, India: BIS.
BIS (Bureau of Indian Standards). 1967. Methods of test for pozzolanic materials. BIS: 1727. New Delhi, India: BIS.
BIS (Bureau of Indian Standards). 1978a. Methods for testing tar and bituminous materials: Determination of penetration. BIS: 1203. New Delhi, India: BIS.
BIS (Bureau of Indian Standards). 1978b. Methods for testing tar and bituminous materials: Determination of ductility. BIS: 1208. New Delhi, India: BIS.
BIS (Bureau of Indian Standards). 2004a. Bitumen emulsion for roads (cationic type). BIS: 8887. New Delhi, India: BIS.
BIS (Bureau of Indian Standards). 2004b. Bitumen emulsion for roads and allied applications (anionic type). BIS: 3117. New Delhi, India: BIS.
Bocci, M., A. Grilli, F. Cardone, and A. Graziani. 2011. “A study on the mechanical behaviour of cement-bitumen treated materials.” Constr. Build. Mater. 25 (2): 773–778. https://doi.org/10.1016/j.conbuildmat.2010.07.007.
Cardone, F., A. Grilli, M. Bocci, and A. Graziani. 2014. “Curing and temperature sensitivity of cement-bitumen treated materials.” Int. J. Pavement Eng. 16 (10): 868–880. https://doi.org/10.1080/10298436.2014.966710.
Casillas, S., and A. Braham. 2021. “Quantifying effects of laboratory curing conditions on workability, compactability, and cohesion gain of cold in-place recycling.” Road Mater. Pavement Des. 22 (10): 2329–2351. https://doi.org/10.1080/14680629.2020.1753101.
Chelelgo, K., Z. C. A. Gariy, and S. M. Shitote. 2019. “Modeling of fatigue-strength development in cold-emulsion asphalt mixtures using maturity method.” Appl. Sci. 9 (13): 2694. https://doi.org/10.3390/app9132694.
Du, S. 2018. “Effect of curing conditions on properties of cement asphalt emulsion mixture.” Constr. Build. Mater. 164 (Mar): 84–93. https://doi.org/10.1016/j.conbuildmat.2017.12.179.
Dulaimi, A., H. Al Nageim, F. Ruddock, and L. Seton. 2017a. “Laboratory studies to examine the properties of a novel cold-asphalt concrete binder course mixture containing binary blended cementitious filler.” J. Mater. Civ. Eng. 29 (9): 04017139. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001975.
Dulaimi, A., H. Al Nageim, F. Ruddock, and L. Seton. 2017b. “Performance analysis of a cold asphalt concrete binder course containing high-calcium fly ash utilizing waste material.” J. Mater. Civ. Eng. 29 (7): 04017048. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001883.
Feng, Q., H. Yamamichi, M. Shoya, and S. Sugita. 2004. “Study on the pozzolanic properties of rice husk ash by hydrochloric acid pretreatment.” Cem. Concr. Res. 34 (3): 521–526. https://doi.org/10.1016/j.cemconres.2003.09.005.
Ferrotti, G., A. Grilli, C. Mignini, and A. Graziani. 2020. “Comparing the field and laboratory curing behaviour of cold recycled asphalt mixtures for binder courses.” Material 13 (21): 4697. https://doi.org/10.3390/ma13214697.
Fu, P., D. Jones, J. T. Harvey, and F. A. Halles. 2010. “Investigation of the curing mechanism of foamed asphalt mixes based on micromechanics principles.” J. Mater. Civ. Eng. 22 (1): 29–38. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000009.
García, A., P. Lura, M. N. Partl, and I. Jerjen. 2013. “Influence of cement content and environmental humidity on asphalt emulsion and cement composites performance.” Mater. Struct. 46: 1275–1289. https://doi.org/10.1617/s11527-012-9971-6.
Graziani, A., C. Godenzoni, F. Cardone, and M. Bocci. 2016. “Effect of curing on the physical and mechanical properties of cold-recycled bituminous mixtures.” Mater. Des. 95 (Apr): 358–369. https://doi.org/10.1016/j.matdes.2016.01.094.
Graziani, A., C. Iafelice, S. Raschia, D. Perraton, and A. Carter. 2018. “A procedure for characterizing the curing process of cold recycled bitumen emulsion mixtures.” Constr. Build. Mater. 173 (Jun): 754–762. https://doi.org/10.1016/j.conbuildmat.2018.04.091.
IRC (Indian Roads Congress). 2013. Specifications for road and bridge works (5th Revision), Ministry of Road Transport and Highways MoRTH. New Delhi, India: IRC.
IRC (Indian Roads Congress). 2014. Use of cold mix technology in construction and maintenance of roads using bitumen emulsion. IRC:SP:100. New Delhi, India: IRC.
Khweir, K., D. Fordyce, D. Strickland, and J. Read. 2004. “Effect of curing time on the performance of cold asphalt mixtures.” In Proc., 3rd Eurasphalt and Eurobitume Congress. Breukelen, Netherlands: Foundation Eurasphalt.
Kim, Y., S. Im, and H. “David” Lee. 2011. “Impacts of curing time and moisture content on engineering properties of cold in-place recycling mixtures using foamed or emulsified asphalt.” J. Mater. Civ. Eng. 23 (5): 542–553. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000209.
Muthadhi, A., and S. Kothandaraman. 2013. “Experimental investigations of performance characteristics of rice husk ash: Blended concrete.” J. Mater. Civ. Eng. 25 (8): 1115–1118. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000656.
Nassar, A. I. 2016. “Enhancing the performance of cold bitumen emulsion mixture using supplementary cementitious materials.” Ph.D. dissertation, Dept. of Civil Engineering, Univ. of Nottingham.
Needham, D. 1996. “Developments in bitumen emulsion mixtures for roads.” Ph.D. dissertation, Dept. of Civil Engineering, Univ. of Nottingham.
Ojum, C., K. Kuna, N. H. Thom, and G. Airey. 2014. “An investigation into the effects of accelerated curing on cold recycled bituminous mixes.” In Proc., 12th Int. Conf. on Asphalt Pavements, ISAP. Nottingham, UK: Univ. of Nottingham.
Omrani, M. A., and A. Modarres. 2019. “Stiffness and fatigue behavior of emulsified cold recycled mixture containing waste powder additives: Mechanical and microstructural analysis.” J. Mater. Civ. Eng. 31 (6): 04019061. https://doi.org/10.1061/(ASCE)MT.1943-5533.0002704.
Otieno, M. N., J. W. Kaluli, and C. Kabubo. 2020. “Strength prediction of cold asphalt emulsion mixtures using the maturity method.” J. Mater. Civ. Eng. 32 (5): 04020096. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003166.
SABITA (South African Bitumen Association). 2020. Technical guideline: Bitumen stabilised materials: A guideline for design and construction of bitumen emulsion and foamed bitumen stabilised materials. SABITA TG2. Cape Town, South Africa: SABITA.
Sadique, M., H. Al Nageim, W. Atherton, L. Seton, and N. Dempster. 2012. “A new composite cementitious material for construction.” Constr. Build. Mater. 35 (Oct): 846–855. https://doi.org/10.1016/j.conbuildmat.2012.04.107.
Sufian, Z., N. A. Aziz, M. Y. Matori, M. Z. Hussain, M. R. Hainin, and E. A. Oluwasola. 2014. “Influence of active filler, curing time and moisture content on the strength properties of emulsion and foamed bitumen stabilized mix.” J. Teknologi (Sci. Eng) 70 (4): 135–141. https://doi.org/10.11113/jt.v70.3502.
Thanaya, I. N. A. 2003. “Improving the performance of cold bituminous emulsion mixtures (CBEMs) incorporating waste materials.” Ph.D. dissertation, School of Civil Engineering, Univ. of Leeds.
Thiriet, V. G., E. Chailleux, J.-M. Piau, F. Delfosse, and C. Leroy. 2021. “Effects of curing on emulsion cold mix asphalts and their extracted binder.” Funct. Compos. Mater. 2 (12): 1–14. https://doi.org/10.1186/s42252-021-00024-2.
Yang, W., J. Ouyang, Y. Meng, B. Han, and Y. Sha. 2021. “Effect of curing and compaction on volumetric and mechanical properties of cold-recycled mixture with asphalt emulsion under different cement contents.” Constr. Build. Mater. 297 (Aug): 123699. https://doi.org/10.1016/j.conbuildmat.2021.123699.

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Go to Journal of Transportation Engineering, Part B: Pavements
Journal of Transportation Engineering, Part B: Pavements
Volume 148Issue 4December 2022

History

Received: Dec 22, 2021
Accepted: Jul 13, 2022
Published online: Sep 22, 2022
Published in print: Dec 1, 2022
Discussion open until: Feb 22, 2023

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Ph.D. Research Scholar, Dept. of Civil Engineering, National Institute of Technology Calicut, Calicut, Kerala 673601, India (corresponding author). ORCID: https://orcid.org/0000-0002-9550-031X. Email: [email protected]
Assistant Professor, Dept. of Civil Engineering, National Institute of Technology Calicut, Calicut, Kerala 673601, India. ORCID: https://orcid.org/0000-0002-4747-3070. Email: [email protected]
Professor, Dept. of Civil Engineering, National Institute of Technology Calicut, Calicut, Kerala 673601, India. ORCID: https://orcid.org/0000-0001-8107-4455. Email: [email protected]

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