Influence of Iron-Containing Components on the Curing and Hardening Properties of Magnesium Oxychloride Binders
Publication: Journal of Materials in Civil Engineering
Volume 36, Issue 12
Abstract
The article presents the results of studies of composite magnesium oxychloride iron-containing binders. The research is aimed at solving the problem of increasing operational durability and expanding the scope of application of magnesium materials. The purpose of the work is to study hydrate formation, hardening, and properties of composite magnesium binders with varying contents of iron compounds. Compositions of caustic magnesite (magnesium oxide) with iron oxides, with ferruginous minerals (andradite and pyrite), and with waste from the enrichment of magnetite ores have been studied. The scientific novelty of the research results lies in the identification of patterns of hydration of magnesium oxychloride binder with a high content (at least 50%) of iron compounds. The mutual influence of magnesium and ferruginous components during hydration and formation of the binder structure has been established. Schemes for the formation of hydrates involving andradite and pyrite have been proposed. The qualitative composition of the main hydrates of composite binders was determined by diffractometric and differential thermal analysis methods. The microstructure of the materials was studied by electron microscopy. The structure of magnesium paste made from a composite binder is formed by crystals of magnesium pentahydroxychloride and amorphous gel-like iron-containing hydrates. In composite binders containing iron oxide or andradite, magnesium hydroxychlorocarbonate is formed. The dependence of the stability of magnesium hydroxychlorocarbonate on the content of magnesium oxide and chloride was revealed. The patterns of the influence of iron compounds on the hydration and hardening of magnesium oxide form the basis for the development of a composite binder containing 50%–70% magnetite ore enrichment waste. A composite binder containing a ferrous man-made component is not inferior in strength properties to caustic magnesite and is characterized by high structural resistance to long-term operational impacts.
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Data Availability Statement
All data, models, and code generated or used during the study appear in the published article.
Acknowledgments
This research is funded by the Science Committee of the Ministry of Science and Higher Education of the Republic of Kazakhstan (Grant No. AP 23487805).
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Information
Published In
Journal of Materials in Civil Engineering
Volume 36 • Issue 12 • December 2024
Copyright
© 2024 American Society of Civil Engineers.
History
Received: Oct 9, 2023
Accepted: May 2, 2024
Published online: Sep 26, 2024
Published in print: Dec 1, 2024
Discussion open until: Feb 26, 2025
ASCE Technical Topics:
- Binders (material)
- Chemical compounds
- Chemical elements
- Chemicals
- Chemistry
- Composite materials
- Continuum mechanics
- Dynamics (solid mechanics)
- Engineering materials (by type)
- Engineering mechanics
- Environmental engineering
- Forces (type)
- Hydration
- Iron compounds
- Laminating
- Magnesium
- Magnetic fields
- Material durability
- Material mechanics
- Material properties
- Materials engineering
- Materials processing
- Pollutants
- Solid mechanics
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