Application of Maturity to Estimate the Strength Development of High-Early-Strength Concrete Mixtures Using Isothermal Calorimetry
Publication: Journal of Materials in Civil Engineering
Volume 36, Issue 5
Abstract
Repair materials for concrete infrastructure applications are designed to minimize closure time and subsequent effect on traffic. Available material choices are typically limited to expensive prepackaged materials or high-early-strength (HES) concrete mixtures. HES concrete mixtures are often designed with high paste content and limited inclusion of supplementary cementitious materials so to promote higher early-age strengths. The traditional approval for HES concrete mixtures has relied on testing the strength of concrete cylinders cured at room temperature. This practice has often resulted in the overdesign of these HES mixtures, primarily because it fails to consider the higher temperatures that typically develop during the in situ curing. Moreover, as highlighted in several reports by state agencies, the high cement content and the near absence of proper curing practices have likely contributed to the premature failure of some of these mixtures. In this study, isothermal calorimetry was explored as a potential tool to quickly evaluate HES concrete formulations in terms of early-age mechanical performance. It was found that this test method, when combined with maturity, can provide reasonable estimations of the concrete strength development for isothermal and nonisothermal curing conditions up to 8 h after the initial mix. The proposed test method can be used as a first step in the optimization of HES concrete mixtures and can help predicting the time to reopening for in situ conditions.
Get full access to this article
View all available purchase options and get full access to this article.
Data Availability Statement
Some or all data, models, or code that support the findings of this study are available from the corresponding author upon reasonable request.
Acknowledgments
The authors acknowledge Sika for providing the accelerating admixtures used in the study. The authors also acknowledge the work performed by Mr. John Leavitt and Mr. Thomas Russo at the Concrete Laboratory at Turner-Fairbank Highway Research Center.
Disclaimer
Certain commercial products are identified in this paper to specify the materials used and procedures employed. In no case does such identification imply endorsement or recommendation by the Federal Highway Administration, nor does it indicate that the products are necessarily the best available for the purpose.
References
ASTM. 2015. Standard practice for use of unbonded caps in determination of compressive strength of hardened cylindrical concrete specimens. ASTM C1231/C1231M-15.West Conshohocken, PA: ASTM.
ASTM. 2017a. Standard practice for density (unit weight), yield, and air content (gravimetric) of concrete. ASTM C138/C138M-17. West Conshohocken, PA: ASTM.
ASTM. 2017b. Standard test method for measurement of heat of hydration of hydraulic cementitious materials using isothermal conduction. ASTM C1702-17. West Conshohocken, PA: ASTM.
ASTM. 2017c. Standard test method for temperature of freshly mixed hydraulic-cement concrete. ASTM C1064/C1064M-17. West Conshohocken, PA: ASTM.
ASTM. 2018. Standard specification for concrete aggregates. ASTM C33. West Conshohocken, PA: ASTM.
ASTM. 2019a. Standard practice for making and curing concrete test specimens in the laboratory. ASTM C192. West Conshohocken, PA: ASTM.
ASTM. 2019b. Standard specification for chemical admixtures for concrete. ASTM C494/C494M. West Conshohocken, PA: ASTM.
ASTM. 2020a. Standard test methods for measuring the reactivity of supplementary cementitious materials by isothermal calorimetry and bound water measurements. ASTM C1897-20. West Conshohocken, PA: ASTM.
ASTM. 2020b. Standard test method for slump of hydraulic-cement concrete. ASTM C143/C143M-20. West Conshohocken, PA: ASTM.
ASTM. 2021a. Standard specification for Portland cement. ASTM C150/C150M. West Conshohocken, PA: ASTM.
ASTM. 2021b. Standard test method for compressive strength of cylindrical concrete specimens. ASTM C39/C39M. West Conshohocken, PA: ASTM.
ASTM. 2022a. Standard practice for measuring hydration kinetics of hydraulic cementitious mixtures using isothermal calorimetry. ASTM C1679-22. West Conshohocken, PA: ASTM.
ASTM. 2022b. Standard specification for slag cement for use in concrete and mortars. ASTM C989. West Conshohocken, PA: ASTM.
ASTM. 2022c. Standard test method for air content of freshly mixed concrete by the pressure method. ASTM C231/C231M-22. West Conshohocken, PA: ASTM.
ASTM. 2023. Standard specification for coal fly ash and raw or calcined natural pozzolan for use in concrete. ASTM C618. West Conshohocken, PA: ASTM.
Barde, A., S. Parameswaran, T. Chariton, J. Weiss, M. D. Cohen, and S. Newbolds. 2006. Evaluation of rapid setting cement-based materials for patching and repair. West Lafayette, IN: Joint Transportation Research Program, Indiana DOT and Purdue Univ.
Bentz, D. P., T. Barrett, I. De La Varga, and W. J. Weiss. 2012. “Relating compressive strength to heat release in mortars.” Adv. Civ. Eng. Mater. 1 (1): 14. https://doi.org/10.1520/ACEM20120002.
Chang, C., D. Saenz, S. Nazarian, I. N. Abdallah, A. Wimsatt, T. Freeman, and E. G. Fernando. 2014. TxDOT guidelines to assign PMIS treatment levels. Austin, TX: Texas DOT.
Cheung, J., A. Jeknavorian, L. Roberts, and D. Silva. 2011. “Impact of admixtures on the hydration kinetics of portland cement.” Cem. Concr. Res. 41 (12): 1289–1309. https://doi.org/10.1016/j.cemconres.2011.03.005.
Cook, M. D., J. N. Seader, M. T. Ley, and B. W. Russell. 2015. Investigation of optimized graded concrete for Oklahoma: Phase 2. Oklahoma City, OK: Oklahoma DOT.
Delatte, N. J. 2021. Optimizing concrete pavement opening to traffic. Ames, IA: National Concrete Pavement Technology Center.
FHWA (Federal Highway Administration). 2023. Source: FHWA 2023. Washington, DC: FHWA.
Freiesleben Hansen, P., and E. J. Pedersen. 1977. “Maleinstrument Til Kontrol Af Betons Haerdning.” Nord Betong 1 (1): 21–25.
Frølich, L., L. Wadsö, and P. Sandberg. 2016. “Using isothermal calorimetry to predict one day mortar strengths.” Cem. Concr. Res. 88 (Oct): 108–113. https://doi.org/10.1016/j.cemconres.2016.06.009.
Ghafoori, N., M. Najimi, and M. Maler. 2017. High-early-strength high-performance concrete for rapid pavement repair. Carson City, NV: Univ. of Nevada Las Vegas.
Gholami, S., J. Hu, Y. R. Kim, and M. Mamirov. 2019. “Performance of portland cement-based rapid-patching materials with different cement and accelerator types, and cement contents.” Transp. Res. Rec. 2673 (11): 172–184. https://doi.org/10.1177/0361198119852330.
Kuryłowicz-Cudowska, A. 2022. “Correlation between compressive strength and heat of hydration of cement mortars with siliceous fly ash.” Minerals 12 (11): 1471. https://doi.org/10.3390/min12111471.
Kuryłowicz-Cudowska, A., and E. Haustein. 2021. “Isothermal calorimetry and compressive strength tests of mortar specimens for determination of apparent activation energy.” J. Mater. Civ. Eng. 33 (4): 04021035. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003634.
Mapa, D. G., A. Markandeya, A. Sedaghat, K. A. Riding, and A. Zayed. 2021. “Effect of different cracking mitigation measures on high early-strength concrete performance.” J. Mater. Civ. Eng. 33 (8): 04021205. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003852.
McDaniel, R. S., J. Olek, A. Behnood, B. Magee, and R. Pollock. 2014. Pavement patching practices. Washington, DC: Transportation Research Board.
Olson, H., K. Tutu, J. Lashley, M. Oman, J. Geib, and B. Worel. 2021. Effective long-lasting partial depth joint repairs for challenging conditions. St. Paul, MN: Minnesota DOT, Office of Policy Analysis, Research & Innovation.
Pane, I., and W. Hansen. 2002. “Concrete hydration and mechanical properties under nonisothermal conditions.” ACI Mater. J. 99 (6): 534–542. https://doi.org/10.14359/12362.
Pane, I., and W. Hansen. 2005. “Investigation of blended cement hydration by isothermal calorimetry and thermal analysis.” Cem. Concr. Res. 35 (6): 1155–1164. https://doi.org/10.1016/j.cemconres.2004.10.027.
Pang, X., L. Sun, M. Chen, M. Xian, G. Cheng, Y. Liu, and J. Qin. 2022. “Influence of curing temperature on the hydration and strength development of Class G portland cement.” Cem. Concr. Res. 156 (Jun): 106776. https://doi.org/10.1016/j.cemconres.2022.106776.
Poole, J. L. 2007. Modeling temperature sensitivity and heat evolution of concrete. Austin, TX: Univ. of Texas at Austin.
Poole, J. L., K. A. Riding, K. J. Folliard, M. C. G. Juenger, and A. K. Schindler. 2007. “Methods for calculating activation energy for portland cement.” ACI Mater J. 10 (1): 303–311. https://doi.org/10.14359/18499.
Poole, J. L., K. A. Riding, M. C. G. Juenger, K. J. Folliard, and A. K. Schindler. 2011. “Effect of chemical admixtures on apparent activation energy of cementitious systems.” J. Mater. Civ. Eng. 23 (12): 1654–1661. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000345.
Popovics, S. 1985. “New formulas for the prediction of the effect of porosity on concrete strength.” J. Am. Concr. Inst. 82 (2): 136–146. https://doi.org/10.14359/10321.
Riding, K., A. Schindler, P. Pesek, T. Drimalas, and K. Folliard. 2013. ConcreteWorks V3 training/user manual. Austin, TX: Univ. of Texas at Austin Center for Transportation Research.
Riding, K. A., J. L. Poole, K. J. Folliard, M. C. G. Juenger, and A. K. Schindler. 2012. “Modeling hydration of cementitious systems.” ACI Mater. J. 109 (2): 225–234. https://doi.org/10.14359/51683709.
Smith, K., D. Harrington, L. Pierce, P. Ram, and K. Smith. 2014. Concrete pavement preservation guide. 2nd Ed. Concrete producer. Washington, DC: Federal Highway Administration.
Snelson, D. G., S. Wild, and M. O’Farrell. 2008. “Heat of hydration of portland cement-metakaolin-fly ash (PC-MK-PFA) blends.” Cem. Concr. Res. 38 (6): 832–840. https://doi.org/10.1016/j.cemconres.2008.01.004.
Soliman, H., J. L. Lambert, A. Shalaby, T. Liske, S. Kass, and L. Deane. 2011. “Characterizing field and laboratory performance of cementitious partial depth repair materials.” In Proc., 2011 Conf. and Exhibition of the Transportation Association of Canada—Transportation Successes: Let’s Build on Them, TAC/ATC 2011. Ottawa: Transportation Association of Canada.
Sprinkel, M. M., M. S. Hossain, and C. Ozyildirim. 2019. Premature failure of concrete patching: Reasons and resolutions. Charlottesville, VA: Virginia Transportation Research Council.
Sun, L. J., X. Y. Pang, S. Ghabezloo, and H. B. Yan. 2023. “Modeling the hydration, viscosity and ultrasonic property evolution of class G cement up to 90°C and 200 MPa by a scale factor method.” Pet. Sci. 20 (4): 2372–2385. https://doi.org/10.1016/j.petsci.2023.01.014.
Todd, N. T. 2015. Assessing risk reduction of high early strength concrete mixtures. West Lafayette, IN: Purdue Univ.
Van Dam, T. J., K. R. Peterson, L. L. Sutter, A. Panguluri, N. Sytsma, N. Buch, R. Kowli, and P. Desaraju. 2005. Guidelines for early-opening-to-traffic portland cement concrete for pavement rehabilitation. Washington, DC: Transportation Research Board.
Zayed, A., K. A. Riding, A. Sedaghat, D. Mapa, A. Markandeya, N. Shanahan, F. Nosouhian, and A. Williams. 2018. Performance improvement of high early strength (HES) concrete for pavement replacement slabs. Tallahassee, FL: Florida DOT Research Center.
Information & Authors
Information
Published In
Copyright
© 2024 Published by American Society of Civil Engineers.
History
Received: Jun 20, 2023
Accepted: Oct 24, 2023
Published online: Feb 26, 2024
Published in print: May 1, 2024
Discussion open until: Jul 26, 2024
Authors
Metrics & Citations
Metrics
Citations
Download citation
If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.