Technical Papers
Mar 28, 2023

Failure of Frozen Sandstone under Uniaxial Compression with Interpretation of Pressure Melting of Pore Ice from Electrical Resistance

Publication: Journal of Geotechnical and Geoenvironmental Engineering
Volume 149, Issue 6

Abstract

Understanding the failure process in frozen porous rock is of great importance to both geomorphology research and engineering design in cold regions. The mechanical behavior of frozen porous rock has its own particularity due to the existence of ice and unfrozen water in pores. To investigate the failure process in frozen rocks, uniaxial compression tests on oven-dried, air-dried, and water-saturated sandstones at 15°C and 20°C were conducted, and the electrical resistances of rock samples were monitored during compression, with which the pressure-melting effect of pore ice can be interpreted. Moreover, the phase composition of pores in sandstone before and after freezing was measured through the nuclear magnetic resonance (NMR) method. The results show that the initial water content of frozen rock changes the variation trend of electrical resistance, that is, the starting point of increasing stage in electrical resistance is shifted from the microcrack propagation stage in frozen oven-dried and air-dried samples to the stress peak in the frozen water-saturated sample. Also, the electrical resistance of frozen water-saturated rock decreases by 29.4% in the microcrack compaction stage, which is 7.4 times higher than that of frozen oven-dried rock and 4.3 times higher than that of frozen air-dried rock. Finally, 96% of pore water (free water, capillary water, and amounts of adsorbed water) is frozen in the saturated rock. The freezing point of water in microcracks is severely depressed by the strong capillary pressure, while the stress concentration effect in microcracks enlarges the applied pressure greatly and eventually induces pressure melting of pore ice. Based on the results and analysis, we suggest that the pressure-melting effect works primarily in the microcrack compaction stage and microcrack propagation stage and remolds the failure process of frozen saturated sandstone by altering the interaction between ice and pore (or microcrack).

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Data Availability Statement

The data sets generated and/or analyzed during the current study are available from the corresponding author upon reasonable request.

Acknowledgments

This work was supported by the National Natural Science Foundation of China (Grant Nos. 42271148 and 42077274).

References

Bai, Y., R. L. Shan, Y. Ju, Y. X. Wu, P. F. Sun, and Z. E. Wang. 2020. “Study on the mechanical properties and damage constitutive model of frozen weakly cemented red sandstone.” Cold Reg. Sci. Technol. 171 (Sep): 102980. https://doi.org/10.1016/j.coldregions.2019.102980.
Carr, H. Y., and E. M. Purcell. 1954. “Effects of diffusion on free precession in nuclear magnetic resonance experiments.” Phys. Rev. 94 (3): 630. https://doi.org/10.1103/PhysRev.94.630.
Dash, J. G., A. W. Rempel, and J. S. Wettlaufer. 2006. “The physics of premelted ice and its geophysical consequences.” Rev. Mod. Phys. 78 (3): 695–741. https://doi.org/10.1103/RevModPhys.78.695.
Dastidar, R. 2007. “Nuclear magnetic resonance (NMR) study of freezing and thawing of saturated porous media and application to shale and pore volume compressibility estimation.” Ph.D. thesis, School of Petroleum and Geological Engineering, Univ. of Oklahoma Graduate College.
Emmert, A., and C. Kneisel. 2017. “Internal structure of two alpine rock glaciers investigated by quasi-3-D electrical resistivity imaging.” Cryosphere 11 (2): 841–855. https://doi.org/10.5194/tc-11-841-2017.
Han, Y. C., H. L. Jia, T. Wang, L. Wang, Q. Li, and Y. B. Wang. 2022. “Fracture toughness and cracking behavior of frozen sandstone at different freezing temperatures.” Eng. Fract. Mech. 271 (5): 108664. https://doi.org/10.1016/j.engfracmech.2022.108664.
Hansen-Goos, H., and J. S. Wettlaufer. 2010. “Theory of ice premelting in porous media.” Phys. Rev. E 81 (3): 031604. https://doi.org/10.1103/PhysRevE.81.031604.
Herring, T., E. Cey, and A. Pidlisecky. 2019. “Electrical resistivity of a partially saturated porous medium at subzero temperatures.” Vadose Zone J. 18 (1): 1–11. https://doi.org/10.2136/vzj2019.02.0019.
Hertzberg, R. W. 1996. Deformation and fracture mechanics of engineering materials. New York: Wiley.
Jia, H. L., S. Ding, Y. Wang, F. Zi, Q. Sun, and G. S. Yang. 2019. “An NMR-based investigation of pore water freezing process in sandstone.” Cold Reg. Sci. Technol. 168 (9): 102893. https://doi.org/10.1016/j.coldregions.2019.102893.
Jia, H. L., S. Ding, F. Zi, Y. H. Dong, and Y. J. Shen. 2020a. “Evolution in sandstone pore structures with freeze-thaw cycling and interpretation of damage mechanisms in saturated porous rocks.” Catena 195: 104915. https://doi.org/10.1016/j.catena.2020.104915.
Jia, H. L., F. Zi, G. S. Yang, G. Li, Y. J. Shen, Q. Sun, and P. Yang. 2020b. “Influence of pore water (ice) content on the strength and deformability of frozen argillaceous siltstone.” Rock Mech. Rock Eng. 53 (2): 967–974. https://doi.org/10.1007/s00603-019-01943-0.
Keuschnig, M., M. Krautblatter, I. Hartmeyer, C. Fuss, and L. Schrott. 2017. “Automated electrical resistivity tomography testing for early warning in unstable permafrost rock walls around alpine infrastructure.” Permafrost Periglacial Processes 28 (1): 158–171. https://doi.org/10.1002/ppp.1916.
Khairy, H., and Z. Z. T. Harith. 2011. “Influence of pore geometry, pressure and partial water saturation to electrical properties of reservoir rock: Measurement and model development.” J. Pet. Sci. Eng. 78 (3–4): 687–704. https://doi.org/10.1016/j.petrol.2011.07.018.
Kim, Y., K. Kim, S. S. Hong, and W. Cho. 2014. “The variation of physical properties in frozen soils at various freezing temperatures.” In Proc., ASME 2014 33rd Int. Conf. on Ocean, Offshore and Arctic Engineering. San Francisco: Polar and Arctic Science and Technology.
Kittel, C., and H. Kroemer. 1980. Thermal physics. London: Macmillan.
Kodama, J., T. Goto, Y. Fujii, and P. Hagan. 2013. “The effects of water content, temperature and loading rate on strength and failure process of frozen rocks.” Int. J. Rock Mech. Min. Sci. 62 (6): 1–13. https://doi.org/10.1016/j.ijrmms.2013.03.006.
Liu, B., Y. Sun, B. Wang, Y. Han, R. Zhang, and J. Wang. 2020. “Effect of water content on mechanical and electrical characteristics of the water-rich sandstone during freezing.” Environ. Earth Sci. 79 (10): 1–14. https://doi.org/10.1007/s12665-020-08991-8.
Liu, Z., K. Muldrew, R. G. Wan, and J. A. Elliott. 2003. “Measurement of freezing point depression of water in glass capillaries and the associated ice front shape.” Phys. Rev. E 67 (6): 061602. https://doi.org/10.1103/PhysRevE.67.061602.
Ma, W., Z. Wu, L. Zhang, and X. Chang. 1999. “Analyses of process on the strength decrease in frozen soils under high confining pressures.” Cold Reg. Sci. Technol. 29 (1): 1–7. https://doi.org/10.1016/S0165-232X(98)00020-2.
Martinez, G. A., and L. A. Davis. 2000. “Petrophysical measurements on shales using NMR.” In Proc., SPE/AAPG Western Regional Meeting. Houston: Society of Petroleum Engineers.
Matteson, A., J. P. Tomanic, M. M. Herron, D. F. Allen, and W. E. Kenyon. 1998. “NMR relaxation of clay-brine mixtures.” In SPE Annual Technical Conf. and Exhibition, 205–211. Houston: Society of Petroleum Engineers. https://doi.org/10.2118/49008-ms.
Meiboom, S., and D. Gill. 1958. “Modified spin-echo method for measuring nuclear relaxation times.” Rev. Sci. Instrum. 29 (Apr): 688–691. https://doi.org/10.1063/1.1716296.
Meng, W., and Y. Guo. 2015. “Experimental study on mechanical properties of ice.” In Proc., AASRI Int. Conf. on Industrial Electronics and Applications, 192–196. Dordrecht, Netherlands: Atlantis Press.
Morrow, N. R. 1970. “Physics and thermodynamics of capillary action in porous media.” Ind. Eng. Chem. 62 (6): 32–56. https://doi.org/10.1021/ie50726a006.
Nguyen, S. T. 2014. “Micromechanical approach for electrical resistivity and conductivity of sandstone.” J. Appl. Geophys. 111 (Jun): 135–140. https://doi.org/10.1016/j.jappgeo.2014.10.001.
Parkhomenko, E. I. 1967. Electrical properties of rocks. New York: Plenum Press.
Rempel, A. W. 2007. “Formation of ice lenses and frost heave.” J. Geophys. Res. Earth Surf. 112 (5): F02S21. https://doi.org/10.1029/2006JF000525.
Saltas, V., I. Fitilis, and F. Vallianatos. 2014. “A combined complex electrical impedance and acoustic emission study in limestone samples under uniaxial loading.” Tectonophysics 637 (6): 198–206. https://doi.org/10.1016/j.tecto.2014.10.011.
Shen, Y. J., Y. Z. Wang, X. Wei, H. L. Jia, and R. Yan. 2020. “Investigation on meso-debonding process of the sandstone–concrete interface induced by freeze–thaw cycles using NMR technology.” Constr. Build. Mater. 252 (11): 118962. https://doi.org/10.1016/j.conbuildmat.2020.118962.
Siegesmund, S., and H. Dürrast. 2014. “Physical and mechanical properties of rocks.” In Stone in architecture, 97–225. Berlin: Springer.
Sondergeld, C. H., and C. S. Rai. 2007. “Velocity and resistivity changes during freeze-thaw cycles in Berea sandstone.” Geophysics 72 (2): 99–105. https://doi.org/10.1190/1.2435198.
Sun, Q., S. Zhu, and L. Xue. 2015. “Electrical resistivity variation in uniaxial rock compression.” Arabian J. Geosci. 8 (4): 1869–1880. https://doi.org/10.1007/s12517-014-1381-3.
Sun, W., K. P. Hou, Z. Q. Yang, and Y. M. Wen. 2017. “X-ray CT three-dimensional reconstruction and discrete element analysis of the cement paste backfill pore structure under uniaxial compression.” Constr. Build. Mater. 138 (Jan): 69–78. https://doi.org/10.1016/j.conbuildmat.2017.01.088.
Teng, J. D., J. Liu, S. Zhang, and D. Sheng. 2022. “Frost heave in coarse-grained soils: Experimental evidence and numerical modelling.” Géotechnique 2022 (Jun): 1–43. https://doi.org/10.1680/jgeot.21.00182.
Tice, A. R., D. M. Anderson, and K. F. Sterrett. 1982. “Unfrozen water contents of submarine permafrost determined by nuclear magnetic resonance.” Dev. Geotech. Eng. 28 (9): 35–146. https://doi.org/10.1016/B978-0-444-42010-7.50017-7.
Verwer, K., G. P. Eberli, and R. J. Weger. 2011. “Effect of pore structure on electrical resistivity in carbonates.” AAPG Bull. 95 (2): 175–190. https://doi.org/10.1306/06301010047.
Wang, T., Q. Sun, H. L. Jia, J. T. Ren, and T. Luo. 2021. “Linking the mechanical properties of frozen sandstone to phase composition of pore water measured by LF-NMR at subzero temperatures.” Bull. Eng. Geol. Environ. 80 (6): 4501–4513. https://doi.org/10.1007/s10064-021-02224-3.
Wang, T., Q. Sun, H. L. Jia, Y. J. Shen, and G. Y. Li. 2022. “Fracture mechanical properties of frozen sandstone at different initial saturation degrees.” Rock Mech. Rock Eng. 2022 (1): 1–18. https://doi.org/10.1007/s00603-022-02830-x.
Wang, Y. H., Y. F. Liu, and H. T. Ma. 2012. “Changing regularity of rock damage variable and resistivity under loading condition.” Saf. Sci. 50 (4): 718–722. https://doi.org/10.1016/j.ssci.2011.08.046.
Wark, K. 1988. Thermodynamics. 5th ed. New York: McGraw-Hill.
Watanabe, K., and T. Wake. 2009. “Measurement of unfrozen water content and relative permittivity of frozen unsaturated soil using NMR and TDR.” Cold Reg. Sci. Technol. 59 (1): 34–41. https://doi.org/10.1016/j.coldregions.2009.05.011.
Watanabe, T., and A. Higuchi. 2015. “Simultaneous measurements of elastic wave velocities and electrical conductivity in a brine-saturated granitic rock under confining pressures and their implication for interpretation of geophysical observations.” Prog. Earth Planet Sci. 2 (15): 37. https://doi.org/10.1186/s40645-015-0067-0.
Watanabe, T., M. Makimura, Y. Kaiwa, G. Desbois, K. Yoshida, and K. Michibayashi. 2019. “Elastic wave velocity and electrical conductivity in a brine-saturated rock and microstructure of pores.” Earth Planets Space 71 (1): 1–12. https://doi.org/10.1186/s40623-019-1112-9.
Wu, G., K. Wang, M. Zhao, Z. Nie, and Z. Huang. 2019. “Analysis of damage evolution of sandstone under uniaxial loading and unloading conditions based on resistivity characteristics.” Adv. Civ. Eng. 2019 (1): 1–12. https://doi.org/10.1016/j.jappgeo.2014.10.001.
Yamabe, T., and K. M. Neaupane. 2001. “Determination of some thermomechanical properties of Sirahama sandstone under subzero temperature condition.” Int. J. Rock Mech. Min. Sci. 38 (7): 1029–1034. https://doi.org/10.1016/S1365-1609(01)00067-3.
Yang, X., A. Jiang, and M. Li. 2019. “Experimental investigation of the time-dependent behavior of quartz sandstone and quartzite under the combined effects of chemical erosion and freeze–thaw cycles.” Cold Reg. Sci. Technol. 161 (3): 51–62. https://doi.org/10.1016/j.coldregions.2019.03.008.
Yin, D., and Q. Xu. 2021. “Investigating the damage evolution of sandstone using electrical impedance spectroscopy.” Int. J. Rock Mech. Min. Sci. 144 (Apr): 104817. https://doi.org/10.1016/j.ijrmms.2021.104817.
Zeng, X., H. Liu, H. Zhu, C. Ling, K. Liang, H. A. Umar, and C. Ma. 2020. “Study on damage of concrete under uniaxial compression based on electrical resistivity method.” Constr. Build. Mater. 254 (20): 119270. https://doi.org/10.1016/j.conbuildmat.2020.119270.
Zhang, L., C. Yang, D. Wang, P. Zhang, and Y. Zhang. 2022. “Freezing point depression of soil water depending on its non-uniform nature in pore water pressure.” Geoderma 412 (Apr): 115724. https://doi.org/10.1016/j.geoderma.2022.115724.
Zhang, Y., S. Niu, Z. Du, J. Hao, and J. Yang. 2020. “Dynamic fracture evolution of tight sandstone under uniaxial compression in high resolution 3D X-ray microscopy.” J. Pet. Sci. Eng. 195 (10): 107585. https://doi.org/10.1016/j.petrol.2020.107585.
Zhao, Y., Y. Sun, S. Liu, K. Wang, and Y. Jiang. 2017. “Pore structure characterization of coal by NMR cryoporometry.” Fuel 190 (Feb): 359–369. https://doi.org/10.1016/j.fuel.2016.10.121.

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Go to Journal of Geotechnical and Geoenvironmental Engineering
Journal of Geotechnical and Geoenvironmental Engineering
Volume 149Issue 6June 2023

History

Received: May 10, 2022
Accepted: Jan 27, 2023
Published online: Mar 28, 2023
Published in print: Jun 1, 2023
Discussion open until: Aug 28, 2023

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Ph.D. Candidate, College of Geology and Environment, Xi’an Univ. of Science and Technology, Xi’an 710000, China. ORCID: https://orcid.org/0000-0002-5930-7555. Email: [email protected]
Hailiang Jia [email protected]
Associate Professor, College of Architecture and Civil Engineering, Xi’an Univ. of Science and Technology, Xi’an 710000, China (corresponding author). Email: [email protected]
Professor, College of Geology and Environment, Xi’an Univ. of Science and Technology, Xi’an 710000, China. ORCID: https://orcid.org/0000-0002-6321-4773. Email: [email protected]
Lecturer, College of Geology and Environment, Xi’an Univ. of Science and Technology, Xi’an 710000, China. Email: [email protected]
Associate Professor, Key Laboratory of Safety and Durability of Concrete Structures of Shaanxi, Xijing Univ., Xi’an 710123, China. ORCID: https://orcid.org/0000-0002-7905-5973. Email: [email protected]
Yanjun Shen [email protected]
Professor, College of Geology and Environment, Xi’an Univ. of Science and Technology, Xi’an 710000, China. Email: [email protected]

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