Technical Papers
Dec 28, 2022

Investigation of the Effect of Oxidative Aging and Temperature Sensitivity on the Illinois Flexibility Index and Disc-Shaped Compact Tension Tests

Publication: Journal of Materials in Civil Engineering
Volume 35, Issue 3

Abstract

This study investigated the sensitivity of the Illinois flexibility index test (I-FIT) and the disc-shaped compact tension [DC(T)] test with respect to oxidative aging and testing temperature. For this purpose, five plant-produced surface course asphalt mixtures covering a wide range of performance-graded asphalt cement (PGAC) were utilized. As for oxidative aging sensitivity, two methods of forced-draft oven aging, at 85°C for 120 h and at 95°C for 72 h, were utilized. Furthermore, to measure the temperature sensitivity, the I-FIT test was conducted at 23°C, 24°C, 25°C and PGAC intermediate temperatures, while the DC(T) test was conducted at 18°C, 24°C, and 30°C. In this study, the analysis of the I-FIT test results from oxidative aging showed that both methods of aging caused a reduction in flexibility index values of asphalt mixtures, and the flexibility index values after two methods of aging were statistically comparable. Moreover, even though oxidative aging caused a reduction in DC(T) fracture energies of asphalt mixtures containing hard PGAC, the fracture energies before and after the two methods of aging were statistically similar for asphalt mixtures. The analysis of the I-FIT test results from testing temperature sensitivity showed that the flexibility index values of asphalt mixtures containing hard PGAC at 23°C were statistically dissimilar to those at 25°C when the testing temperature dropped from 25°C to 23°C. Consequently, regarding the I-FIT test, the comparable flexibility index values from the two methods of oxidative aging suggested utilization of forced-draft oven aging at 95°C for 72 h as a less time-consuming method compared to forced-draft oven aging at 85°C for 120 h to evaluate the effect of oxidative aging. In addition, the variability in flexibility index values due to the drop in testing temperature suggested exercising caution when conducting the test on asphalt mixtures containing hard PGAC.

Get full access to this article

View all available purchase options and get full access to this article.

Data Availability Statement

All data, models, and code generated or used during the study appear in the published article.

Acknowledgments

This research was a part of a HIIFP project funded by the Ministry of Transportation Ontario (MTO). The authors would like to acknowledge the MTO’s Bituminous Section and Laboratory Services for the supply of materials, use of their testing facilities, and their support and assistance during this project; the guidance of Imran Bashir and Seyed Tabib is especially appreciated.

References

AASHTO. 2006. Standard practice for mixture conditioning of hot mix asphalt (HMA). AASHTO R30. Washington, DC: AASHTO.
AASHTO. 2015a. Bulk specific gravity (Gmb) of compacted hot mix asphalt (HMA) using saturated surface-dry specimens. AASHTO T166. Washington, DC: AASHTO.
AASHTO. 2015b. Theoretical maximum specific gravity (GMM) and density of hot mix asphalt. AASHTO T209. Washington, DC: AASHTO.
AASHTO. 2019a. Standard method of test for determining the flexural creep stiffness of asphalt binder using the bending beam rheometer. AASHTO T313. Washington, DC: AASHTO.
AASHTO. 2019b. Standard method of test for determining the fracture potential of asphalt mixtures using flexibility index test (FIT). AASHTO TP124. Washington, DC: AASHTO.
AASHTO. 2019c. Standard method of test for determining the rheological properties of asphalt binder using a dynamic shear rheometer (DSR). AASHTO T315. Washington, DC: AASHTO.
Al Qadi, I. L., H. Ozer, Z. Zhu, P. Singhvi, U. M. Ali, M. Sawalha, A. F. Luque, and J. G. Mainieri. 2019. Development of long-term aging protocol for implementation of the Illinois flexibility index test (I-FIT). Urbana, IL: Illinois Center for Transportation, Univ. of Illinois.
Al-Qadi, I. L., H. Ozer, J. Lambros, A. El Khatib, P. Singhvi, T. Khan, J. Rivera-Perez, and B. Doll. 2015. Testing protocols to ensure performance of high asphalt binder replacement mixes using RAP and RAS. Urbana, IL: Illinois Center for Transportation, Univ. of Illinois.
ASTM. 2013. Standard test method for determining fracture energy of asphalt-aggregate mixtures using the disk-shaped compact tension geometry. ASTM D7313. West Conshohocken, PA: ASTM.
Azimi Alamdary, Y., S. Singh, and H. Baaj. 2019. “Laboratory simulation of the impact of solar radiation and moisture on long-term age conditioning of asphalt mixes.” Supplement, Road Mater. Pavement Des. 20 (S1): S521–S532. https://doi.org/10.1080/14680629.2019.1587496.
Baaj, H., H. Di Benedetto, and P. Chaverot. 2005. “Effect of binder characteristics on fatigue of asphalt pavement using an intrinsic damage approach.” J. Road Mater. Pavement Des. 6 (2): 147–174. https://doi.org/10.1080/14680629.2005.9690003.
Bashir, I., S. Salehi Ashani, D. Ahmed, S. Tabib, and G. Vasiliu. 2020. “MTO’s experience with post-production asphalt mixture performance testing.” In Proc., 65th Annual Conf. Canadian Technical Asphalt Association. 315–344. Kelowna, BC, Canada: Canadian Technical Asphalt Association.
Bazuhair, R. W., C. V. Pittman, I. L. Howard, W. S. Jordan, J. M. Hemsley, and G. L. Baumgardner. 2018. “Conditioning and testing protocol combinations to detect asphalt mixture damage.” J. Transp. Res. Rec. 2672 (28): 10–21. https://doi.org/10.1177/0361198118756631.
Braham, A., W. Buttlar, T. Clyne, M. O. Marasteanu, and M. I. Turos. 2009. “The effect of long-term laboratory aging on hot mix asphalt fracture energy.” J. Assoc. Asphalt Pavement Technol. 78: 417–445.
Braham, A. F., and B. S. Underwood. 2016. State of the art and practice in fatigue cracking and evaluation of asphalt pavements, Version 1.0. Lino Lakes, MN: Association of Asphalt Paving Technologists.
Christensen, D. W., and R. F. Bonaquist. 2009. “Analysis of HMA fatigue data using the concepts of reduced loading cycles and endurance limit.” J. Assoc. Asphalt Paving Technol. 78: 377–416.
Daniel, J. S., and R. Y. Kim. 2002. “Development of a simplified fatigue test and analysis procedure using a viscoelastic, continuum damage model.” J. Assoc. Asphalt Paving Technol. 71: 619–650.
Dave, E., B. Behnia, S. Ahmed, W. Buttlar, and H. Reis. 2011. “Low temperature fracture evaluation of asphalt mixtures using mechanical testing and acoustic emissions techniques.” J. Assoc. Asphalt Pavement Technol. 80: 193–220.
Dave, E. V., B. C. Hoplin, J. Helmer, and D. Dailey. 2016. “Effects of mix design and fracture energy on transverse cracking performance of asphalt pavements in Minnesota.” J. Transp. Res. Rec. 2576 (1): 40–50. https://doi.org/10.3141/2576-05.
Elwardany, M., F. Yousefi Rad, C. Castorena, and R. Y. Kim. 2017. “Evaluation of asphalt mixture laboratory long-term aging methods for performance testing and prediction.” J. Road Mater. Pavement Des. 18 (Sup 1): 28–61. https://doi.org/10.1080/14680629.2016.1266740.
Hanz, A., E. Dukatz, and G. Reinke. 2017. “Use of performance-based testing for high RAP mix design and production monitoring.” Supplement, Road Mater. Pavement Des. 18 (S1): 284–310. https://doi.org/10.1080/14680629.2016.1266766.
Haslett, K., E. Dave, and J. Sias. 2018. “Evaluation of cracking indices for asphalt mixtures using SCB tests at different temperatures and loading rates.” Honors thesis and capstone, Dept. of Civil and Environmental Engineering, Univ. of New Hampshire.
Hill, B., D. Oldham, B. Behnia, E. Fini, W. Buttlar, and H. Reis. 2013. “Low-temperature performance characterization of biomodified asphalt mixtures that contain reclaimed asphalt pavement.” J. Transp. Res. Rec. 2371 (1): 49–57. https://doi.org/10.3141/2371-06.
Jahangiri, B., H. Majidifard, J. Meister, and W. Buttlar. 2019. “Performance evaluation of asphalt mixtures with reclaimed asphalt pavement and recycled asphalt shingles in Missouri.” J. Transp. Res. Rec. 2673 (2): 392–403. https://doi.org/10.1177/0361198119825638.
Kim, R. Y., C. Hintz, F. Yousefi Rad, M. Elwardany, B. Underwood, M. J. Farrer, and R. R. Glaser. 2018. Long-term aging of asphalt mixtures for performance testing and prediction. Washington, DC: Transportation Research Board of the National Academies.
Ling, C., D. Swiertz, T. Manda, P. Teymourpour, and H. Bahia. 2017. “Sensitivity of the Illinois flexibility index test to mixture design factors.” J. Transp. Res. Rec. 2631 (1): 153–159. https://doi.org/10.3141/2631-17.
LS 282. 2019. “Method of test for quantitative extraction of asphalt cement and analysis of extracted aggregate from bituminous paving mixtures.” Accessed May 1, 2019. https://www.library.mto.gov.on.ca/MTOTechnicalDocuments/LabManual/LS282.
LS 284. 2020. “Method of test for recovery of asphalt from solution by rotary evaporator.” Accessed May 1, 2020. https://www.library.mto.gov.on.ca/MTOTechnicalDocuments/LabManual/LS284.
Majidifard, H., B. Jahangiri, P. Rath, and W. G. Buttlar. 2021. “Development of a balanced cracking index for asphalt mixtures tested in semi-circular bending with load-LLD measurements.” J. Meas. 173 (Mar): 108658. https://doi.org/10.1016/j.measurement.2020.108658.
Marasteanu, M., W. Buttlar, H. Bahia, and C. Williams. 2012. “Investigation of low temperature cracking in asphalt pavements.” Accessed August 1, 2012. https://www.lrrb.org./pdf/201223.pdf.
Ozer, H., I. Al-Qadi, J. Lambros, A. El-Khatib, P. Singhvi, and B. Doll. 2016. “Development of the fracture-based flexibility index for asphalt concrete cracking potential using modified semi-circle bending test parameters.” J. Constr. Build. Mater. 115 (Jul): 390–401. https://doi.org/10.1016/j.conbuildmat.2016.03.144.
Rahbar-Rastegar, R., J. Sias, and E. Dave. 2018. “Evaluation viscoelastic and fracture properties of asphalt mixture with long-term laboratory conditioning.” J. Transp. Res. Rec. 2672 (28): 503–513. https://doi.org/10.1177/0361198118795012.
Safazadeh, F., A. M. Asib, and P. Romero. 2021a. “Methods to evaluate intermediate temperature properties of asphalt mixtures by the semi-circular bending (SCB) test.” J. Road Mater. Pavement Des. 23 (7): 1694–1706. https://doi.org/10.1080/14680629.2021.1911831.
Safazadeh, F., P. Romero, A. M. Asib, and K. VanFrank. 2021b. “Practicality of driven parameters of semi-circular bending test at intermediate temperature.” J. Transp. Eng., Part B: Pavements 147 (3): 04021033. https://doi.org/10.1061/JPEODX.0000284.
Smith, B. T., and I. L. Howard. 2018. “Short- and longer-term effects of short-term aging on asphalt mixture properties.” J. Mater. Civ. Eng. 30 (3): 04018005. https://doi.org/10.1061/(ASCE)MT.1943-5533.0002170.
Yin, F., A. Epps Martin, E. Arambula-Mercado, and D. Newcomb. 2018. Short-term laboratory conditioning of asphalt mixtures. Washington, DC: Transportation Research Board of the National Academies.

Information & Authors

Information

Published In

Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 35Issue 3March 2023

History

Received: Dec 23, 2021
Accepted: Jun 28, 2022
Published online: Dec 28, 2022
Published in print: Mar 1, 2023
Discussion open until: May 28, 2023

Permissions

Request permissions for this article.

Authors

Affiliations

Saeid Salehi Ashani, Ph.D. [email protected]
Postdoctoral Research Associate, Dept. of Civil and Environmental Engineering, Univ. of Waterloo, Waterloo, ON, Canada N2L 3G1 (corresponding author). Email: [email protected]
Sina Varamini, Ph.D. [email protected]
P.Eng.
Adjunct Assistant Professor, Dept. of Civil and Environmental Engineering, Univ. of Waterloo, Waterloo, ON, Canada N2L 3G1. Email: [email protected]
Susan Tighe, Ph.D. [email protected]
P.Eng.
Provost and Vice-President Academic Dept. of Civil Engineering, McMaster Univ., Hamilton, ON, Canada L8S 4L8. Email: [email protected]

Metrics & Citations

Metrics

Citations

Download citation

If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.

Cited by

  • Performance of Cold-Mix Asphalt with Calcined Eggshell Powder–Activated GGBFS Filler, Journal of Materials in Civil Engineering, 10.1061/JMCEE7.MTENG-16982, 36, 4, (2024).

View Options

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Media

Figures

Other

Tables

Share

Share

Copy the content Link

Share with email

Email a colleague

Share