Effect of Laboratory Aging Levels on Asphalt Binder Chemical/Rheological Properties and Fracture Resistance of Asphalt Mixtures
Publication: Journal of Materials in Civil Engineering
Volume 34, Issue 3
Abstract
This study aimed to evaluate the effect of laboratory aging levels on chemical and rheological properties of asphalt binder as well as fracture performance of asphalt mixture. Compacted asphalt mixtures were laboratory aged at 85°C for 0, 2, 5, 7, and 10 days and then subjected to the semicircular bending (SCB) test. Asphalt binders were extracted from the aged samples for further chemical and rheological characterization. Chemical characterization included Fourier transform spectroscopy (FTIR) and gel permeation chromatography (GPC). Rheological tests included bending beam rheometer (BBR) and linear amplitude sweep (LAS) tests. Asphalt binder rheological characterization showed that the cracking resistance of asphalt binders decreased with an increase of aging level. Statistical analysis of SCB test results indicated that there is no significant drop in the critical strain energy release rate, , between 2- and 5-day aging, but 10-day aging resulted in a significant decrease in . It was observed that the aging susceptibility of asphalt mixtures in terms of SCB results was consistent with FTIR and LAS test results.
Get full access to this article
View all available purchase options and get full access to this article.
Data Availability Statement
All data, models, and code generated or used during the study appear in the published article.
Acknowledgments
This study was a part of Louisiana DOTD project 19-4B, implementation of semicircular bend test for quality control (QC)/quality assurance(QA) of asphalt mixtures. The authors would like to express their gratitude to the Louisiana Transportation Research Center for their support.
References
AASHTO. 2012. Standard method of test for determining the flexural creep stiffness of asphalt binder using the bending beam rheometer (BBR). AASHTO T 313. Washington, DC: AASHTO.
AASHTO. 2015. Standard method for test for estimating fatigue resistance of asphalt binders using the linear amplitude sweep. AASHTO TP 101-12. Washington, DC: AASHTO.
Anderson, R. M., G. N. King, D. I. Hanson, and P. B. Blankenship. 2011. “Evaluation of the relationship between asphalt binder properties and non-load related cracking.” Assoc. Asphalt Paving Technol. 80: 615–664.
ASTM. 2011. Standard practice for molecular weight averages and molecular weight distribution of hydrocarbon, rosin, and terpene resins by size-exclusion chromatography. ASTM D6579. West Conshohocken, PA: ASTM.
ASTM. 2012. Standard practice for general techniques for obtaining infrared spectra for qualitative analysis. ASTM E1252. West Conshohocken, PA: ASTM.
ASTM. 2016a. Standard practice for determining the continuous grading temperatures and continuous grades for PG graded asphalt binders. ASTM D7643. West Conshohocken, PA: ASTM.
ASTM. 2016b. Standard test method for evaluation of asphalt mixture cracking resistance using the semi-circular bend test (SCB) at intermediate temperatures. ASTM D8044. West Conshohocken, PA: ASTM.
Baek, C., S. B. Underwood, and R. Y. Kim. 2012. “Effects of oxidative aging on asphalt mixture properties.” Transp. Res. Rec. 2296 (1): 77–85. https://doi.org/10.3141/2296-08.
Bell, C. A., Y. AbWahab, M. E. Cristi, and D. Sosnovske. 1994a. Selection of laboratory aging procedures for asphalt-aggregate asphalt mixtures. Washington, DC: Strategic Highway Research Program, National Research Council.
Bell, C. A., A. Wieder, and M. J. Fellin. 1994b. Laboratory aging of asphalt-aggregate asphalt mixtures: Field validation. Washington, DC: National Research Council.
Cao, W., P. Barghabany, L. Mohammad, S. B. Cooper III, and S. Balamurugan. 2019a. “Chemical and rheological evaluation of asphalts incorporating RAP/RAS binders and warm-mix technologies in relation to crack resistance.” J. Constr. Build. Mater. 198 (Feb): 256–268. https://doi.org/10.1016/j.conbuildmat.2018.11.122.
Cao, W., L. Mohammad, and P. Barghabany. 2018. “Use of viscoelastic continuum damage theory to correlate fatigue resistance of asphalt binders and mixtures.” Int. J. Geomech. 18 (11): 04018151. https://doi.org/10.1061/(ASCE)GM.1943-5622.0001306.
Cao, W., Y. Wang, and C. Wang. 2019b. “Fatigue characterization of bio-modified asphalt binders under various laboratory aging conditions.” Constr. Build. Mater. 208 (May): 686–696. https://doi.org/10.1016/j.conbuildmat.2019.03.069.
Cooper, B. S., L. Negulescu, S. S. Balamurugan, L. N. Mohammad, and H. W. Daly. 2015. “Binder composition and intermediate temperature cracking performance of asphalt mixtures containing RAS.” Supplement, Road Mater. Pavement Des. 16 (S2): 275–295. https://doi.org/10.1080/14680629.2015.1077013.
Cortizo, M. S., D. O. Larsen, H. Bianchetto, and J. L. Alessandrini. 2004. “Effect of the thermal degradation of SBS copolymers during the ageing of modified asphalts.” Polym. Degrad. Stab. 86 (2): 275–282. https://doi.org/10.1016/j.polymdegradstab.2004.05.006.
Daly, W. H., I. I. Negulescu, and S. Balamurugan. 2013. Implementation of GPC characterization of asphalt binders at Louisiana materials laboratory. Baton Rouge, LA: Louisiana DOT and Development.
Diab, A., M. Enieb, and D. Singh. 2018. “Influence of aging on properties of polymer-modified asphalt.” Constr. Build. Mater. 196 (Jan): 54–65. https://doi.org/10.1016/j.conbuildmat.2018.11.105.
Glover, C. J., R. R. Davison, C. H. Domke, Y. Ruan, P. Juristyarini, D. B. Knorr, and S. H. Jung. 2005. Development of a new method for assessing asphalt binder durability with field validation. Austin, TX: Texas State Dept. of Highways and Public Transportation.
Hao, G., W. Huang, J. Yuan, N. Tang, and F. Xiao. 2017. “Effect of aging on chemical and rheological properties of SBS modified asphalt with different compositions.” Constr. Build. Mater. 156 (Dec): 902–910. https://doi.org/10.1016/j.conbuildmat.2017.06.146.
Johnson, C. M. 2010. “Estimating asphalt binder fatigue resistance using an accelerated test method.” Ph.D. dissertation, Dept. of Civil and Environmental Engineering, Univ. of Wisconsin-Madison.
Kim, R. K., C. Castorena, M. Elwardany, F. Yousefi Rad, S. B. Underwood, A. Gundla, P. Gudipundi, J. Farra, and R. Glaser. 2018. Long-term aging of asphalt mixtures for performance testing and prediction. Washington, DC: National Cooperative Highway Research Program.
LADOTD (Louisiana DOT and Development). 2016. Louisiana Specifications for Roads and Bridges. Baton Rouge, LA: LADOTD.
Mansourkhaki, A., M. Ameri, M. Habibpour, and B. S. Underwood. 2020. “Chemical composition and rheological characteristics of binders containing RAP and rejuvenator.” J. Mater. Civ. Eng. 32 (4): 04020026. https://doi.org/10.1061/(ASCE)MT.1943-5533.0003016.
Mogawer, W., T. Bennert, J. S. Daniel, R. Bonaquist, A. Austerman, and A. Booshehrian. 2012. “Performance characteristics of plant produced high RAP mixtures.” Supplement, Road Mater. Pavement Des. 13 (S1): 183–208. https://doi.org/10.1080/14680629.2012.657070.
Molenaar, A., E. Hagos, and M. van de Ven. 2010. “Effects of aging on the mechanical characteristics of bituminous binders in PAC.” J. Mater. Civ. Eng. 22 (8): 779–787. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000021.
Mukala, M. M. 2012. “Statistics corner: A guide to appropriate use of correlation coefficient in medical research.” Malawi Med. J. 24 (3): 69–71.
Mull, M. A., A. Othman, and L. Mohammad. 2005. “Fatigue crack propagation analysis of chemically modified crumb rubber-asphalt mixtures.” J. Elastomers Plast. 37 (1): 73–87. https://doi.org/10.1177/0095244305049898.
Nabizadeh, H., H. F. Haghshenas, Y. R. Kim, and F. T. Aragao. 2017. “Effects of rejuvenators on high-RAP mixtures based on laboratory tests of asphalt concrete (AC) mixtures and fine aggregate matrix (FAM) mixtures.” Constr. Build. Mater. J. 152 (Oct): 65–73. https://doi.org/10.1016/j.conbuildmat.2017.06.101.
Negulesco, L., L. N. Mohammad, W. Daly, and C. Abadie. 2006. “Chemical and rheological characterization of wet and dry aging of SBS copolymer modified asphalt cements: Laboratory and field evaluation.” J. Assoc. Asphalt Paving Technol. 75: 267–296.
Newcomb, D., A. E. Martin, F. Yin, E. Arambula, E. S. Park, A. Chowdhury, R. Brown, C. Rodezno, N. Tran, and E. Coleri. 2015. Short-term laboratory conditioning of asphalt mixtures. Washington, DC: National Cooperative Highway Research Program.
Overholser, B. R., and K. M. Sowinski. 2008. “Biostatistics primer: Part 2.” Nutr. Clin. Pract. 23 (1): 76–84. https://doi.org/10.1177/011542650802300176.
Petersen, J. C., and R. Glaser. 2011. “Asphalt oxidation mechanisms and the role of oxidation products on age hardening revisited.” Road Mater. Pavement Des. 12 (4): 795–819. https://doi.org/10.1080/14680629.2011.9713895.
Rowe, G. M. 2011. “Prepared discussion for the AAPT paper by Anderson et al.: Evaluation of the relationship between asphalt binder properties and non-load related cracking.” J. Assoc. Asphalt Paving Technol. 80: 649–662.
Ruan, Y., R. R. Davison, and C. J. Glover. 2003. “The effect of long-term oxidation on the rheological properties of polymer modified asphalts.” Fuel 82 (14): 1763–1773. https://doi.org/10.1016/S0016-2361(03)00144-3.
Schober, P., C. Boer, and L. Schwarte. 2018. “Correlation coefficients: Appropriate use and interpretation.” Anesth. Analg. 126 (5): 1763–1768. https://doi.org/10.1213/ANE.0000000000002864.
Tarbox, S., and J. S. Daniel. 2012. “Effects of long-term oven aging on reclaimed asphalt pavement mixtures.” Transp. Res. Rec. 2294 (1): 1–15. https://doi.org/10.3141/2294-01.
Tarefder, R., and S. Yousefi. 2015. “Rheological examination of aging in polymer-modified asphalt.” J. Mater. Civ. Eng. 28 (2): 1–12. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001370.
Van den Bergh, W. 2011. “The effect of ageing on the fatigue and healing properties of bituminous mortars.” Ph.D. dissertation, Dept. of Design and Construction, Delft Univ. of Technology.
Wackerly, D. D., W. Mendenhall III, and R. L. Scheaffer. 2008. Multivariate probability distributions. Mathematical statistics with applications. 7th ed., 223–295. Belmont, CA: Brooks/Cole.
Wu, Z., N. L. Mohammad, L. B. Wang, and M. A. Mull. 2005. “Fracture resistance characterization of Superpave asphalt mixtures using the semi-circular bending test.” J. ASTM Int. 2 (3): 12264. https://doi.org/10.1520/JAI12264.
Zhang, H., Z. Chen, G. Xu, and C. Shi. 2018. “Evaluation of aging behaviors of asphalt binders through different rheological indices.” Fuel 221 (Jun): 78–88. https://doi.org/10.1016/j.fuel.2018.02.087.
Zhou, F., D. Newcomb, C. Gurganus, S. Banihashemrad, S. E. Par, M. Sakhaeifar, and L. R. Lytton. 2016. Experimental design for field validation of laboratory tests to assess cracking resistance of asphalt mixtures. Washington, DC: National Cooperative Highway Research Program.
Information & Authors
Information
Published In
Copyright
© 2021 American Society of Civil Engineers.
History
Received: Apr 27, 2021
Accepted: Jul 22, 2021
Published online: Dec 29, 2021
Published in print: Mar 1, 2022
Discussion open until: May 29, 2022
Authors
Metrics & Citations
Metrics
Citations
Download citation
If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.
Cited by
- Chi-Su Lim, Dae-Sung Jang, Sang-Min Yu, Jae-Jun Lee, Analysis of the Properties of Modified Asphalt Binder by FTIR Method, Materials, 10.3390/ma15165743, 15, 16, (5743), (2022).