Technical Papers
Mar 23, 2019

Characterizing Cold Bituminous Emulsion Mixtures Comprised of Palm Leaf Ash

Publication: Journal of Materials in Civil Engineering
Volume 31, Issue 6

Abstract

Cold bitumen emulsion mixtures (CBEMs) are a promising substitute for hot mix asphalt (HMA) due to their low environmental impact, cost effectiveness, and low energy production costs. Nevertheless, conventional CBEM has some disadvantages, mainly related to the long curing time required to reach its full strength and its higher susceptibility to moisture. This paper reports the experimental test results of research that aimed to investigate and develop a new CBEM containing a waste biomass material, palm leaf ash (PLA), a waste material produced by burning palm leaves. The new CBEM was compared with a conventional cold mix (CCM) as a control. The tests to assess the mixtures’ mechanical properties were the Marshall test, indirect tensile strength, and wheel track test. Durability was evaluated by water sensitivity and aging tests. The results revealed noticeable improvements in the mechanical properties of the CBEMs comprising ordinary portland cement (OPC), and raised the possibility of replacing some of the OPC with PLA without compromising said improvements. Results have shown that the new CBEMs with PLA achieved outstanding results in comparison with traditional CBEM, with and without the addition of OPC. There was also a significant improvement in water sensitivity when using PLA. This paper therefore opens the door for the development of new CBEMs that have outstanding mechanical characteristics when made with biomass ash materials.

Get full access to this article

View all available purchase options and get full access to this article.

Acknowledgments

The authors wish to thank the Department of Direct Implementation of the Karbala government and Karbala Cement Plant for their help and support in this research work.

References

AASHTO. 2004. Standard method of test for Hamburg wheel track testing of compacted hot mix asphalt (HMA). AASHTO T324. Washington, DC: AASHTO.
Ahmad, J., M. Yunus, K. Nizam, M. Kamaruddin, N. Hidayah, and A. Zainorabidin. 2012. “The practical use of palm oil fuel ash as a filler in asphalt pavement.” In Proc., 1 st Int. Conf. on Civil and Environmental Engineering Sustainability (IConCEES2012), 1–7. Johor Bahru, Malaysia.
Al-Busaltan, S. 2014. “Investigating filler characteristics in upgrading cold bituminous emulsion mixtures.” Int. J. Pavement Eng. Asphalt Technol. 15 (2): 54–71. https://doi.org/10.2478/ijpeat-2013-0012.
Al-Busaltan, S., H. Al Nageim, W. Atherton, and G. Sharples. 2012a. “Green bituminous asphalt relevant for highway and airfield pavement.” Constr. Build. Mater. 31: 243–250. https://doi.org/10.1016/j.conbuildmat.2011.12.065.
Al-Busaltan, S., H. Al Nageim, W. Atherton, and G. Sharples. 2012b. “Mechanical properties of an upgrading cold-mix asphalt using waste materials.” J. Mater. Civ. Eng. 24 (12): 1484–1491. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000540.
Al-Busaltan, S., H. Al-Nageim, W. Atherton, S. George, L. Seton, and N. Dempster. 2012c. “Use of SEM and XRD for characterisation the improvement in CMEM’s engineering properties.” In Proc., 34th Int. Conf. on Cement Microscopy 2012. Halle/Saale, Germany: International Cement Microscopy Association.
Al-Busaltan, S. F. S. 2012. “Development of new cold bituminous mixtures for road and highway pavements.” Ph.D. thesis, School of built environment, Liverpool John Moores Univ.
Al-Hdabi, A., H. A. Nageim, F. Ruddock, L. J. R. M. Seton, and P. Design. 2014. “Laboratory studies to investigate the properties of novel cold-rolled asphalt containing cement and waste bottom ash.” Road Mater. Pavement Des. 15 (1): 78–89. https://doi.org/10.1080/14680629.2013.852612.
Al-Mulali, M. Z., H. Awang, H. A. Khalil, and Z. S. Aljoumaily. 2015. “The incorporation of oil palm ash in concrete as a means of recycling: A review.” Cem. Concr. Compos. 55: 129–138. https://doi.org/10.1016/j.cemconcomp.2014.09.007.
Al Nageim, H., S. F. Al-Busaltan, W. Atherton, and G. Sharples. 2012. “A comparative study for improving the mechanical properties of cold bituminous emulsion mixtures with cement and waste materials.” Constr. Build. Mater. 36: 743–748. https://doi.org/10.1016/j.conbuildmat.2012.06.032.
Aprianti, E., P. Shafigh, S. Bahri, and J. N. Farahani. 2015. “Supplementary cementitious materials origin from agricultural wastes—A review.” Constr. Build. Mater. 74: 176–187. https://doi.org/10.1016/j.conbuildmat.2014.10.010.
Arum, C., C. M. Ikumapayi, and G. O. Aralepo. 2013. “Ashes of biogenic wastes—Pozzolanicity, prospects for use, and effects on some engineering properties of concrete.” Mater. Sci. Appl. 4 (9): 36665. https://doi.org/10.4236/msa.2013.49064.
Asphalt Institute. 1989. Asphalt cold mix manual. Lexington, KY: Asphalt Institute.
ASTM. 2007. Standard test method for ductility of bituminous materials. ASTM D113. West Conshohocken, PA: ASTM.
ASTM. 2008. Standard test method for residue by evaporation of emulsified asphalt. ASTM D6934. West Conshohocken, PA: ASTM.
ASTM. 2009a. Standard test method for density of semi-solid bituminous materials (pycnometer method). ASTM D70. West Conshohocken, PA: ASTM.
ASTM. 2009b. Standard test methods and practices for emulsified asphalts. ASTM D244. West Conshohocken, PA: ASTM.
ASTM. 2011. Standard practice for evaluating aggregate coating using emulsified asphalts. ASTM D6998. West Conshohocken, PA: ASTM.
ASTM. 2012. Standard test method for indirect tensile (IDT) strength of bituminous mixtures. ASTM D6931. West Conshohocken, PA: ASTM.
ASTM. 2013a. Standard specification for cationic emulsified asphalt. ASTM D2397. West Conshohocken, PA: ASTM.
ASTM. 2013b. Standard test method for determining the viscosity of emulsified asphalts using a rotational paddle viscometer. ASTM D7226. West Conshohocken, PA: ASTM.
ASTM. 2014. Standard test method for effect of moisture on asphalt concrete paving mixtures. ASTM D4867/D4867M. West Conshohocken, PA: ASTM.
ASTM. 2015a. Standard test method for Marshall stability and flow of asphalt mixtures. ASTM D6927. West Conshohocken, PA: ASTM.
ASTM. 2015b. Standard test method for penetration of bituminous materials. ASTM D5. West Conshohocken, PA: ASTM.
ASTM. 2015c. Standard test method for solubility of asphalt materials in trichloroethylene. ASTM D2042. West Conshohocken, PA: ASTM.
Basha, E., R. Hashim, H. Mahmud, and A. Muntohar. 2005. “Stabilization of residual soil with rice husk ash and cement.” Constr. Build. Mater. 19 (6): 448–453. https://doi.org/10.1016/j.conbuildmat.2004.08.001.
Bell, C. A., Y. Abwahab, M. E. Cristi, and D. Sosnovske. 1994. Selection of laboratory aging procedures for asphalt-aggregate mixtures. Washington, DC: National Cooperative Highway Research Program (NCHRP).
Bocci, M., A. Grilli, F. Cardone, and A. Graziani. 2011. “A study on the mechanical behaviour of cement–bitumen treated materials.” Constr. Build. Mater. 25 (2): 773–778. https://doi.org/10.1016/j.conbuildmat.2010.07.007.
Brown, S., and D. Needham. 2000. “A study of cement modified bitumen emulsion mixtures.” In Proc., Association of Asphalt Paving Technologists. Lino Lakes, MN: Association of Asphalt Paving Technologists.
Central Statistical Organization. 2015. Palm production report for 2015. Baghdad, Iraq: Ministry of Planning, Central Statistical Organization.
Chavez-Valencia, L., E. Alonso, A. Manzano, J. Perez, M. Contreras, and C. Signoret. 2007. “Improving the compressive strengths of cold-mix asphalt using asphalt emulsion modified by polyvinyl acetate.” Constr. Build. Mater. 21 (3): 583–589. https://doi.org/10.1016/j.conbuildmat.2005.07.017.
Dondi, G., P. Tataranni, M. Pettinari, C. Sangiorgi, A. Simone, and V. Vignali. 2014. “Crumb rubber in cold recycled bituminous mixes: Comparison between traditional crumb rubber and cryogenic crumb rubber.” Constr. Build. Mater. 68: 370–375. https://doi.org/10.1016/j.conbuildmat.2014.06.093.
Dulaimi, A., H. Al Nageim, F. Ruddock, and L. Seton. 2015. “A novel cold asphalt concrete mixture for heavily trafficked binder course.” World Acad. Sci. Eng. Technol. Int. J. Civ. Environ. Struct. Constr. Archit. Eng. 9 (8): 945–949.
Ebels, L.-J. 2008. “Characterisation of material properties and behaviour of cold bituminous mixtures for road pavements.” Ph.D. thesis, Dept. of Civil Engineering, Stellenbosch Univ.
GSRB (General Specification for Roads and Bridges). 2003. General specification for roads and bridges, Section R9. Baghdad, Iraq: Ministry of Housing and Construction.
Head, R. W. 1974. “An informal report of cold mix research using emulsified asphalt as a binder.” In Proc., Association of Asphalt Paving Technologists. Lino Lakes, MN: Washington, DC: Transportation Research Board.
Hesami, E., N. Bidewell, B. Birgisson, and N. Kringos. 2013. “Evaluation of environmental susceptibility of bituminous mastic viscosity as a function of mineral and biomass fillers.” Transp. Res. Rec. 2371: 23–31. https://doi.org/10.3141/2371-03.
Hu, S.-G., T. Wang, F.-Z. Wang, and Z.-C. Liu. 2009. “Adsorption behaviour between cement and asphalt emulsion in cement–asphalt mortar.” Adv. Cem. Res. 21 (1): 11–14. https://doi.org/10.1680/adcr.2007.00034.
Jenkins, K. J. 2000. “Mix design considerations for cold and half warm bituminous mixes with emphasis on foamed asphalt.” Ph.D. thesis, Dept. of Civil Engineering, Stellenbosch Univ.
Li, G., Y. Zhao, S. S. Pang, and W. Huang. 1998. “Experimental study of cement-asphalt emulsion composite.” Cem. Concr. Res. 28 (5): 635–641. https://doi.org/10.1016/S0008-8846(98)00038-6.
Lundberg, R., T. Jacobson, P. Redelius, and J.-A. Östlund. 2016. “Production and durability of cold mix asphalt.” In Proc., 6th Eurasphalt & Eurobitume Congress. Brussels, Belgium: European Association of Bitumen Producers.
Melotti, R., E. Santagata, M. Bassani, M. Salvo, and S. Rizzo. 2013. “A preliminary investigation into the physical and chemical properties of biomass ashes used as aggregate fillers for bituminous mixtures.” Waste Manage. 33 (9): 1906–1917. https://doi.org/10.1016/j.wasman.2013.05.015.
Miljković, M., and M. Radenberg. 2015. “Characterising the influence of bitumen emulsion on asphalt mixture performance.” Mater. Struct. 48 (7): 2195–2210. https://doi.org/10.1617/s11527-014-0302-y.
Modarres, A., and P. Ayar. 2016. “Comparing the mechanical properties of cold recycled mixture containing coal waste additive and ordinary Portland cement.” Int. J. Pavement Eng. 17 (3): 211–224. https://doi.org/10.1080/10298436.2014.979821.
Niazi, Y., and M. Jalili. 2009. “Effect of portland cement and lime additives on properties of cold in-place recycled mixtures with asphalt emulsion.” Constr. Build. Mater. 23 (3): 1338–1343. https://doi.org/10.1016/j.conbuildmat.2008.07.020.
Nordmark, D., A. Lagerkvist, J. Vestin, M. Arm, B. Lind, and P. Hallgren. 2011. “Environmental and mechanical assessment of wood fly ash used for stabilisation of gravel roads.” In Proc., 13th Int. Waste Management and Landfill Symp., 3–7. Padova, Italy: CISA Publisher.
Nunes, M. C. M. 1997. “Enabling the use of alternative materials in road construction.” Ph.D. thesis, Dept. of Civil Engineering, Univ. of Nottingham.
Oruc, S., F. Celik, and V. Akpinar. 2007. “Effect of cement on emulsified asphalt mixtures.” J. Mater. Eng. Perform. 16 (5): 578–583. https://doi.org/10.1007/s11665-007-9095-2.
Oruc, S., F. Celik, and A. Aksoy. 2006. “Performance of cement modified dense graded cold-mix asphalt and establishing mathematical model.” Indian J. Eng. Mater. Sci. 13 (6): 512–519.
Pels, J. R., D. S. de Nie, and J. H. Kiel. 2005. “Utilization of ashes from biomass combustion and gasification.” In Proc., 14th European Biomass Conf. and Exhibition. Florence, Italy: ETA-Florence.
Pettinari, M., G. Dondi, C. Sangiorgi, and O. Hededal. 2014. “The effect of cryogenic crumb rubber in cold recycled mixes for road pavements.” Constr. Build. Mater. 63: 249–256. https://doi.org/10.1016/j.conbuildmat.2014.04.060.
Sargin, Ş., M. Saltan, N. Morova, S. Serin, and S. Terzi. 2013. “Evaluation of rice husk ash as filler in hot mix asphalt concrete.” Constr. Build. Mater. 48: 390–397. https://doi.org/10.1016/j.conbuildmat.2013.06.029.
Schmidt, R. J., L. E. Santucci, and L. D. Coyne. 1973. “Performance characteristics of cement-modified asphalt emulsion mixes.” In Proc., Association of Asphalt Paving Technologists. Lino Lakes, MN: Association of Asphalt Paving Technologists.
Serfass, J. 2002. “Advantages, peculiarities and mysteries of emulsion cold mixes.” Eur. Roads Rev. Paris: Revue Générale Des Routes Et Des Aérodromes Sa.
Suleiman, N. 2002. A state-of-the-art review of cold in-place recycling of asphalt pavements in the Northern Plains region. Grand Forks, ND: Dept. of Civil Engineering, Univ. of North Dakota.
Tan, Y., J. Ouyang, J. Lv, and Y. Li. 2013. “Effect of emulsifier on cement hydration in cement asphalt mortar.” Constr. Build. Mater. 47: 159–164. https://doi.org/10.1016/j.conbuildmat.2013.04.044.
Terrell, R. L., and C. K. Wang. 1971. “Early curing behavior of cement modified asphalt emulsion mixtures.” In Proc., Association of Asphalt Paving Technologists. Lino Lakes, MN: Association of Asphalt Paving Technologists.
Thanaya, I. N. A. 2003. “Improving the performance of cold bituminous emulsion mixtures incorporating waste materials.” Ph.D. thesis, School of Civil Engineering, Univ. of Leeds.
Thanaya, I. N. A. 2007. “Review and recommendation of cold asphalt emulsion mixtures (CAEMs) design.” Civ. Eng. Dimension 9 (1): 49–55. https://doi.org/10.9744/ced.9.1.pp.%2049-56.
Thanaya, I. N. A., J. Forth, and S. Zoorob. 2006. “Utilisation of coal ashes in hot and on cold bituminous mixtures.” In Proc., Int. Coal Ash Technology Conf. AshTech 2006. Wolverhampton, UK: United Kingdom Quality Association.
Thanaya, I. N. A., S. Zoorob, and J. A. Forth. 2009. “Laboratory study on cold-mix, cold-lay emulsion mixtures.” Proc. Inst. Civ. Eng. Transp. 162 (TR1): 47–55. https://doi.org/10.1680/tran.2009.162.1.47.
Wang, Z., Q. Wang, and T. Ai. 2014. “Comparative study on effects of binders and curing ages on properties of cement emulsified asphalt mixture using gray correlation entropy analysis.” Constr. Build. Mater. 54: 615–622. https://doi.org/10.1016/j.conbuildmat.2013.12.093.
Zhang, Y., X. Kong, S. Hou, Y. Liu, and S. Han. 2012. “Study on the rheological properties of fresh cement asphalt paste.” Constr. Build. Mater. 27 (1): 534–544. https://doi.org/10.1016/j.conbuildmat.2011.07.010.

Information & Authors

Information

Published In

Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 31Issue 6June 2019

History

Received: Jul 24, 2018
Accepted: Nov 30, 2018
Published online: Mar 23, 2019
Published in print: Jun 1, 2019
Discussion open until: Aug 23, 2019

Permissions

Request permissions for this article.

Authors

Affiliations

Sajjad Al-Merzah [email protected]
Formerly, Graduate Student, Dept. of Civil Engineering, Univ. of Kerbala, Kerbala 56001, Iraq. Email: [email protected]
Shakir Al-Busaltan, Ph.D. [email protected]
Assistant Professor, Dept. of Civil Engineering, Univ. of Kerbala, Kerbala 56001, Iraq (corresponding author). Email: [email protected]; [email protected]
Hassan Al Nageim, Ph.D. [email protected]
Professor, Dept. of Civil Engineering, Liverpool John Moores Univ., Liverpool, UK. Email: [email protected]

Metrics & Citations

Metrics

Citations

Download citation

If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.

Cited by

View Options

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Media

Figures

Other

Tables

Share

Share

Copy the content Link

Share with email

Email a colleague

Share