Technical Papers
Nov 20, 2018

Self-Healing of SMA and Steel-Reinforced Mortar with Microcapsules

Publication: Journal of Materials in Civil Engineering
Volume 31, Issue 2

Abstract

Healing capabilities of shape-memory alloys (SMAs) and steel-reinforced mortar with self-healing microcapsules were investigated. Small cracks ranging from 13 to 152 μm were induced by three-point bending, and specimens were subjected to a 14-day healing period under water-submerged conditions at 55°C±5°C to induce shape-memory effect activation. Light microscopy investigation was performed at 3, 7, and 14 days of the healing period. Moreover, healing products were investigated using scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS). Healing efficiency improvements with the increase in microcapsule content were reported at 3 and 7 days for steel-reinforced specimens. Furthermore, for all mortar mixes evaluated, SMA-reinforced specimens exhibited a superior healing performance than steel-reinforced specimens at 3 days of healing due the crack-closing action of SMA. The overwhelming majority of healing products were identified as likely calcite crystals, and the limited gellike products also present were presumably calcium silicate hydrate (C─ S─ H).

Get full access to this article

View all available purchase options and get full access to this article.

Acknowledgments

The authors would like to acknowledge the financial support through a grant from Qatar National Research Foundation (QNRF)/National Priorities Research Program (NPRP) as well as the laboratory support from Louisiana Transportation Research Center (LTRC).

References

Edvardsen, C. 1999. “Water permeability and autogenous healing of cracks in concrete.” ACI Mater. J. 96 (4): 448–454.
Gilford, J., III, et al. 2014. “Dicyclopentadiene and sodium silicate microencapsulation for self-healing of concrete.” J. Mater. Civ. Eng. 26 (5): 886–896. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000892.
Hassan, M. M., J. Milla, T. Rupnow, M. Al-Ansari, and W. H. Daly. 2016. “Microencapsulation of calcium nitrate for concrete applications.” Transp. Res. Rec. 2577: 8–16. https://doi.org/10.3141/2577-02.
Huang, H., and G. Ye. 2011. “Application of sodium silicate solution as self-healing agent in cementitious materials.” In Proc., Int. RILEM Conf. on Advances in Construction Materials through Science and Engineering, 530–536. Hong Kong, China: RILEM.
Kan, L., H. Shi, A. R. Sakulich, and V. C. Li. 2010. “Self-healing characterization of engineered cementitious composite materials.” ACI Mater. J. 107 (6): 617–624.
Karagöl, F., R. Demirboğa, M. A. Kaygusuz, M. M. Yadollahi, and R. Polat. 2013. “The influence of calcium nitrate as antifreeze admixture on the compressive strength of concrete exposed to low temperatures.” Cold Reg. Sci. Technol. 89: 30–35. https://doi.org/10.1016/j.coldregions.2013.02.001.
Kuang, Y., and J. Ou. 2008. “Self-repairing performance of concrete beams strengthened using superelastic SMA wires in combination with adhesives released from hollow fibers.” Smart Mater. Struct. 17 (2): 25020. https://doi.org/10.1088/0964-1726/17/2/025020.
Li, V., and E.-H. Yang. 2008. “Self healing in concrete materials.” In Self healing materials, 161–193. New York: Springer.
Li, V. C., E. Herbert, S. Senot, E. Schlangen, V. C. Li, and E. Herbert. 2012. “Robust self-healing concrete for sustainable infrastructure robust self-healing concrete for sustainable infrastructure.” J. Adv. Concr. Technol. 10 (6): 207–218. https://doi.org/10.3151/jact.10.207.
Li, W., Z. Jiang, Z. Yang, N. Zhao, and W. Yuan. 2013. “Self-healing efficiency of cementitious materials containing microcapsules filled with healing adhesive: Mechanical restoration and healing process monitored by water absorption.” PLoS One 8 (11): e81616.
Maes, M., K. Van Tittelboom, and N. De Belie. 2014. “The efficiency of self-healing cementitious materials by means of encapsulated polyurethane in chloride containing environments.” Constr. Build. Mater. 71: 528–537. https://doi.org/10.1016/j.conbuildmat.2014.08.053.
Milla, J., M. Hassan, T. Rupnow, M. Al-Ansari, and G. Arce. 2016. “Effect of self-healing calcium nitrate microcapsules on concrete properties.” Transp. Res. Rec. 2577: 69–77. https://doi.org/10.3141/2577-09.
Pelletier, M. M., R. Brown, A. Shukla, and A. Bose. 2010. Self-healing concrete with a microencapsulated healing agent. Kingston, RI: Univ. of Rhode Island.
Ramachandran, V. S. 1995. Concrete admixtures handbook: Properties, science, and technology. Park Ridge, NJ: Noyes.
Song, G., N. Ma, and H. N. Li. 2006. “Applications of shape memory alloys in civil structures.” Eng. Struct. 28 (9): 1266–1274. https://doi.org/10.1016/j.engstruct.2005.12.010.
Sun, L., D. Liang, Q. Gao, and J. Zhou. 2013. “Analysis on factors affecting the self-repair capability of SMA wire concrete beam.” Math. Prob. Eng. 2013: 1–6.
Van Tittelboom, K., and N. De Belie. 2013. “Self-healing in cementitious materials: A review.” Materials 6 (6): 2182–2217. https://doi.org/10.3390/ma6062182.
Van Tittelboom, K., N. De Belie, D. Van Loo, and P. Jacobs. 2011. “Self-healing efficiency of cementitious materials containing tubular capsules filled with healing agent.” Cem. Concr. Compos. 33 (4): 497–505. https://doi.org/10.1016/j.cemconcomp.2011.01.004.
Wang, J. Y., H. Soens, W. Verstraete, and N. De Belie. 2014. “Self-healing concrete by use of microencapsulated bacterial spores.” Cem. Concr. Res. 56: 139–152. https://doi.org/10.1016/j.cemconres.2013.11.009.
White, S. R., N. R. Sottos, P. H. Geubelle, J. S. Moore, M. R. Kessler, S. R. Sriram, E. N. Brown, and S. Viswanathan. 2001. “Autonomic healing of polymer composites.” Nature 409 (6822): 794–797. https://doi.org/10.1038/35057232.
Winter, N. B. 2012. Scanning electron microscopy of cement and concrete. Rendlesham, UK: WHD Microanalysis Consultants Ltd.
Wu, M., B. Johannesson, and M. Geiker. 2012. “A review: Self-healing in cementitious materials and engineered cementitious composite as a self-healing material.” Constr. Build. Mater. 28 (1): 571–583. https://doi.org/10.1016/j.conbuildmat.2011.08.086.
Yang, Z., J. Hollar, X. He, and X. Shi. 2011. “A self-healing cementitious composite using oil core/silica gel shell microcapsules.” Cem. Concr. Compos. 33 (4): 506–512. https://doi.org/10.1016/j.cemconcomp.2011.01.010.

Information & Authors

Information

Published In

Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 31Issue 2February 2019

History

Received: Nov 15, 2017
Accepted: Jul 17, 2018
Published online: Nov 20, 2018
Published in print: Feb 1, 2019
Discussion open until: Apr 20, 2019

Permissions

Request permissions for this article.

Authors

Affiliations

Gabriel A. Arce, A.M.ASCE
Postdoctoral Fellow, Dept. of Construction Management, Louisiana State Univ., Baton Rouge, LA 70803.
Marwa M. Hassan, M.ASCE [email protected]
CETF Distinguished Professor, Dept. of Construction Management, Louisiana State Univ., Baton Rouge, LA 70803 (corresponding author). Email: [email protected]
Louay N. Mohammad, M.ASCE
Irma Louise Rush Stewart Distinguished Professor, Dept. of Civil and Environmental Engineering, Louisiana State Univ., Baton Rouge, LA 70803; Director, Engineering Materials Characterization Research Facility, Louisiana Transportation Research Center, 4101 Gourrier Ave., Baton Rouge, LA 70808.
Tyson Rupnow, M.ASCE
Research and Development Associate Director, Louisiana Transportation Research Center, 4101 Gourrier Ave., Baton Rouge, LA 70808.

Metrics & Citations

Metrics

Citations

Download citation

If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.

Cited by

View Options

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Media

Figures

Other

Tables

Share

Share

Copy the content Link

Share with email

Email a colleague

Share