Technical Notes
May 7, 2020

Suppressing Ettringite-Induced Swelling of Gypseous Soil by Using Magnesia-Activated Ground Granulated Blast-Furnace Slag

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Publication: Journal of Geotechnical and Geoenvironmental Engineering
Volume 146, Issue 7

Abstract

Ettringite usually is formed in lime- and cement-stabilized gypseous soils, resulting in significant swelling upon wetting and thereby causing damage to pavements and foundation systems. To reduce the ettringite formation and the associated swelling, magnesia (MgO)-activated ground granulated blast-furnace slag (GGBS) was investigated for stabilizing gypseous soil. Experimental tests, including swelling, unconfined compression strength, X-ray diffraction (XRD), and scanning electron microscopy (SEM) studies, were conducted to examine properties of MgO-GGBS-treated gypseous soil. Test results illustrated that the swelling of MgO-GGBS-stabilized soils (0.4%–2%) was much lower than that of cement-stabilized soil (6.1%), whereas the strength of MgO-GGBS-stabilized soils after soaking (1.2–2.8 MPa) was significantly higher than that of cement-stabilized soil (0.3 MPa). XRD and SEM results showed that no ettringite was formed in MgO-GGBS-stabilized soils, which primarily was responsible for the lesser swelling and higher strength compared with that of the cement-stabilized soil after soaking. Overall, test results indicated the potential of MgO-GGBS for effective stabilization of gypseous soils.

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Data Availability Statement

All data, models, and code generated or used during the study appear in the published article.

Acknowledgments

The authors appreciate the grant (M4081914) from Nanyang Technological University, Singapore, and the assistance of Ong Yi Jie with the laboratory testing.

References

ASTM. 2012. Standard test methods for laboratory compaction characteristics of soil using standard effort (12 400 ft-lbf/ft3 (600 kN-m/m3)). ASTM D698-12e2. West Conshohocken, PA: ASTM.
ASTM. 2017. Standard method for compressive strength of molded soil-cement cylinders. ASTM D1633. West Conshohocken, PA: ASTM.
BSI (British Standards Institution). 1990. Methods of test for soils for civil engineering purposes. Part 2: Classification tests. BS 1377-2. London: BSI.
Cheshomi, A., A. Eshaghi, and J. Hassanpour. 2017. “Effect of lime and fly ash on swelling percentage and Atterberg limits of sulfate-bearing clay.” Appl. Clay Sci. 135 (Jan): 190–198. https://doi.org/10.1016/j.clay.2016.09.019.
Chrysochoou, M., D. G. Grubb, and N. E. Malasavage. 2012. “Assessment of sulfate-induced swell in stabilized dredged material: Is ettringite always a problem?” J. Geotech. Geoenviron. Eng. 138 (3): 407–414. https://doi.org/10.1061/(ASCE)GT.1943-5606.0000584.
Congress, S. S. C., and A. J. Puppala. 2019. “Evaluation of UAV–CRP data for monitoring transportation infrastructure constructed over expansive soils.” Indian Geotech. J. 49 (4): 1–13. https://doi.org/10.1007/s40098-019-00384-4.
Grubb, D. G., N. E. Malasavage, C. J. Smith, and M. Chrysochoou. 2010. “Stabilized dredged material. II: Geomechanical behavior.” J. Geotech. Geoenviron. Eng. 136 (8): 1025–1036. https://doi.org/10.1061/(ASCE)GT.1943-5606.0000290.
Haha, M. B., B. Lothenbach, G. Le Saout, and F. Winnefeld. 2011. “Influence of slag chemistry on the hydration of alkali-activated blast-furnace slag. Part I: Effect of MgO.” Cem. Concr. Res. 41 (9): 955–963. https://doi.org/10.1016/j.cemconres.2011.05.002.
Hekal, E. E., E. Kishar, and H. Mostafa. 2002. “Magnesium sulfate attack on hardened blended cement pastes under different circumstances.” Cem. Concr. Res. 32 (9): 1421–1427. https://doi.org/10.1016/S0008-8846(02)00801-3.
Higgins, D. D. 2005. Soil stabilisation with ground granulated blast-furnace slag, 1–15. London: UK Cementitious Slag Makers Association.
Hoyos, L. R., A. J. Puppala, and P. Chainuwat. 2004. “Dynamic properties of chemically stabilized sulfate rich clay.” J. Geotech. Geoenviron. Eng. 130 (2): 153–162. https://doi.org/10.1061/(ASCE)1090-0241(2004)130:2(153).
Hunter, D. 1988. “Lime-induced heave in sulfate-bearing clay soils.” J. Geotech. Eng. 114 (2): 150–167. https://doi.org/10.1061/(ASCE)0733-9410(1988)114:2(150).
Jha, A. K., and P. V. Sivapullaiah. 2016. “Volume change behavior of lime treated gypseous soil—Influence of mineralogy and microstructure.” Appl. Clay Sci. 119 (Jan): 202–212. https://doi.org/10.1016/j.clay.2015.09.017.
Jha, A. K., and P. V. Sivapullaiah. 2017a. “Physical and strength development in lime treated gypseous soil with fly ash—Micro-analyses.” Appl. Clay Sci. 145 (Sep): 17–27. https://doi.org/10.1016/j.clay.2017.05.016.
Jha, A. K., and P. V. Sivapullaiah. 2017b. “Volume change behavior of gypseous soil.” J. Mater. Civ. Eng. 29 (10): 06017010. https://doi.org/10.1061/(ASCE)MT.1943-5533.0002015.
Jha, A. K., and P. V. Sivapullaiah. 2018. “Potential of fly ash to suppress the susceptible behavior of lime-treated gypseous soil.” Soils Found. 58 (3): 654–665. https://doi.org/10.1016/j.sandf.2018.02.024.
Jin, F., and A. Al-Tabbaa. 2013. “Thermogravimetric study on the hydration of reactive magnesia and silica mixture at room temperature.” Thermochim. Acta 566 (Aug): 162–168. https://doi.org/10.1016/j.tca.2013.05.036.
Jin, F., and A. Al-Tabbaa. 2014. “Characterisation of different commercial reactive magnesia.” Adv. Cem. Res. 26 (2): 101–113. https://doi.org/10.1680/adcr.13.00004.
Jin, F., K. Gu, A. Abdollahzadeh, and A. Al-Tabbaa. 2015. “Effects of different reactive MgOs on the hydration of MgO-activated GGBS paste.” J. Mater. Civ. Eng. 27 (7): B4014001. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001009.
Lee, W. F., and S. C. Lee. 2006. “Effect of hydrotalcite on the swelling and mechanical behaviors for the hybrid nanocomposite hydrogels based on gelatin and hydrotalcite.” J. Appl. Polym. Sci. 100 (1): 500–507. https://doi.org/10.1002/app.23219.
Li, W., Y. Yi, and A. J. Puppala. 2019. “Utilization of carbide slag-activated ground granulated blastfurnace slag to treat gypseous soil.” Soils Found. 59 (5): 1496–1507. https://doi.org/10.1016/j.sandf.2019.06.002.
Little, D. N., S. Nair, and B. Herbert. 2009. “Addressing sulfate-induced heave in lime treated soils.” J. Geotech. Geoenviron. Eng. 136 (1): 110–118. https://doi.org/10.1061/(ASCE)GT.1943-5606.0000185.
Mitchell, J. K. 1986. “Practical problems from surprising soil behavior.” J. Geotech. Eng. Div. 112 (3): 259–289.
Nidzam, R. M., and J. M. Kinuthia. 2010. “Sustainable soil stabilisation with blastfurnace slag—A review.” Proc. Inst. Civ. Eng. Constr. Mater. 163 (3): 157–165. https://doi.org/10.1680/coma.2010.163.3.157.
Puppala, A. J., S. S. C. Congress, N. Talluri, and E. Wattanasanthicharoen. 2019. “Sulfate-heaving studies on chemically treated sulfate-rich geomaterials.” J. Mater. Civ. Eng. 31 (6): 04019076. https://doi.org/10.1061/(ASCE)MT.1943-5533.0002729.
Puppala, A. J., J. A. Griffin, L. R. Hoyos, and S. Chomtid. 2004. “Studies on sulfate-resistant cement stabilization methods to address sulfate-induced soil heave.” J. Geotech. Geoenviron. Eng. 130 (4): 391–402. https://doi.org/10.1061/(ASCE)1090-0241(2004)130:4(391).
Puppala, A. J., N. Intharasombat, and R. K. Vempati. 2005. “Experimental studies on ettringite-induced heaving in soils.” J. Geotech. Geoenviron. Eng. 131 (3): 325–337. https://doi.org/10.1061/(ASCE)1090-0241(2005)131:3(325).
Puppala, A. J., N. Talluri, S. S. C. Congress, and A. Gaily. 2018. “Ettringite induced heaving in stabilized high sulfate soils.” Innovative Infrastruct. Solutions 3 (1): 72. https://doi.org/10.1007/s41062-018-0179-7.
Rajasekaran, G. 2005. “Sulphate attack and ettringite formation in the lime and cement stabilized marine clays.” Ocean Eng. 32 (1): 1133–1159.
Santhanam, M., M. D. Cohen, and J. Olek. 2001. “Sulfate attack research—Whither now?” Cem. Concr. Res. 31 (6): 845–851. https://doi.org/10.1016/S0008-8846(01)00510-5.
Shand, M. A. 2006. The chemistry and technology of magnesia. Hoboken, NJ: Wiley.
Snedker, E. A., and J. Temporal. 1990. “M40 Motorway Banbury IV contract - Lime stabilisation.” Highways Transp. 37 (12): 7–8.
Tasong, W. A., S. Wild, and R. J. D. Tilley. 1999. “Mechanisms by which ground granulated blastfurnace slag prevents sulphate attack of lime-stabilised kaolinite.” Cem. Concr. Res. 29 (7): 975–982. https://doi.org/10.1016/S0008-8846(99)00007-1.
TxDOT (Texas Department of Transportation). 2005. Guidelines for treatment of sulfate-rich soils and bases in pavement structures. Austin, TX: TxDOT.
Vandeperre, L. J., M. Liska, and A. Al-Tabbaa. 2008. “Microstructures of reactive magnesia cement blends.” Cem. Concr. Compos. 30 (8): 706–714. https://doi.org/10.1016/j.cemconcomp.2008.05.002.
Wild, S., J. M. Kinuthia, G. I. Jones, and D. D. Higgins. 1998. “Effects of partial substitution of lime with ground granulated blast furnace slag (GGBS) on the strength properties of lime-stabilised sulphate-bearing clay soils.” Eng. Geol. 51 (1): 37–53. https://doi.org/10.1016/S0013-7952(98)00039-8.
Wild, S., J. M. Kinuthia, G. I. Jones, and D. D. Higgins. 1999. “Suppression of swelling associated with ettringite formation in lime stabilized sulphate bearing clay soils by partial substitution of lime with ground granulated blastfurnace slag (GGBS).” Eng. Geol. 51 (4): 257–277. https://doi.org/10.1016/S0013-7952(98)00069-6.
Xeidakis, G. S. 1996a. “Stabilization of swelling clays by Mg (OH)2. Changes in clay properties after addition of Mg-hydroxide.” Eng. Geol. 44 (1–4): 107–120. https://doi.org/10.1016/S0013-7952(96)00047-6.
Xeidakis, G. S. 1996b. “Stabilization of swelling clays by Mg (OH)2. Factors affecting hydroxy-Mg-interlayering in swelling clays.” Eng. Geol. 44 (1–4): 93–106. https://doi.org/10.1016/S0013-7952(96)00046-4.
Yi, Y., L. Gu, S. Liu, and F. Jin. 2016a. “Magnesia reactivity on activating efficacy for ground granulated blastfurnace slag for soft clay stabilisation.” Appl. Clay Sci. 126 (Jun): 57–62. https://doi.org/10.1016/j.clay.2016.02.033.
Yi, Y., C. Li, S. Liu, and A. Al-Tabbaa. 2014a. “Resistance of MgO–GGBS and CS–GGBS stabilised marine soft clays to sodium sulfate attack.” Géotechnique 64 (8): 673–679. https://doi.org/10.1680/geot.14.T.012.
Yi, Y., C. Li, S. Liu, and F. Jin. 2015a. “Magnesium sulfate attack on clays stabilised by carbide slag and magnesia-ground granulated blast furnace slag.” Géotechnique Lett. 5 (4): 306–312. https://doi.org/10.1680/jgele.15.00129.
Yi, Y., M. Liska, and A. Al-Tabba. 2014b. “Properties and microstructure of GGBS–magnesia pastes.” Adv. Cem. Res. 26 (2): 114–122. https://doi.org/10.1680/adcr.13.00005.
Yi, Y., M. Liska, and A. Al-Tabbaa. 2014c. “Properties of two model soils stabilized with different blends and contents of GGBS, MgO, lime and PC.” J. Mater. Civ. Eng. 26 (2): 267–274. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000806.
Yi, Y., M. Liska, F. Jin, and A. Al-Tabbaa. 2016b. “Mechanism of reactive magnesia–ground granulated blast-furnace slag (GGBS) soil stabilization.” Can. Geotech. J. 53 (5): 773–782. https://doi.org/10.1139/cgj-2015-0183.
Yi, Y., X. Zheng, S. Liu, and A. Al-Tabbaa. 2015b. “Comparison of reactive magnesia-and carbide slag-activated ground granulated blastfurnace slag and Portland cement for stabilisation of a natural soil.” Appl. Clay Sci. 111 (Jul): 21–26. https://doi.org/10.1016/j.clay.2015.03.023.
Zhang, T., L. J. Vandeperre, and C. R. Cheeseman. 2014. “Formation of magnesium silicate hydrate (M-S-H) cement pastes using sodium hexametaphosphate.” Cem. Concr. Res. 65 (Nov): 8–14. https://doi.org/10.1016/j.cemconres.2014.07.001.

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Journal of Geotechnical and Geoenvironmental Engineering
Volume 146Issue 7July 2020

History

Received: Jul 22, 2019
Accepted: Feb 11, 2020
Published online: May 7, 2020
Published in print: Jul 1, 2020
Discussion open until: Oct 7, 2020

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Wentao Li, Ph.D. [email protected]
Research Fellow, School of Civil and Environmental Engineering, Nanyang Technological Univ., 50 Nanyang Ave., Singapore 639798. Email: [email protected]
Assistant Professor, School of Civil and Environmental Engineering, Nanyang Technological Univ., 50 Nanyang Ave., Singapore 639798 (corresponding author). ORCID: https://orcid.org/0000-0002-1188-3799. Email: [email protected]
Anand J. Puppala, Ph.D., F.ASCE [email protected]
P.E.
A.P. Florence Wiley Chair Professor, Zachry Dept. of Civil and Environmental Engineering, Texas A&M Univ., College Station, TX 77843. Email: [email protected]

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