Technical Papers
Sep 29, 2017

Experimental Study on Pore Structure and Mechanical Properties of Stratified Coal

Publication: International Journal of Geomechanics
Volume 17, Issue 12

Abstract

The most striking feature of liquid nitrogen (LN2) fracturing is to drastically reduce the temperature around the rock when LN2 is injected into the reservoir. The strong thermal gradient can significantly induce the internal thermal stress of the rock, which results in severe damage. In this study, the permeability, ultrasonic wave, and triaxial compression test were performed to investigate the influence of LN2 treatment on pore structure and mechanical properties of stratified coal. In the pore structure tests, the increasing range of permeability of LN2-treated samples is 100.3–149.6%, and the P-wave velocity decreases by 3.1–4.6%. In the triaxial compression tests, the compressive strength and elastic modulus of LN2-treated samples decrease by 11–39.6% and 18.2–32.1%, respectively. The experimental results indicate that LN2 treatment increases the connectivity of coal pores, improving its flow conductivity and permeability, which can effectively enhance the fracturing effect. Meanwhile, it also reduces the ability of coal to resist deformation and rupture, which contributes to the reduction of initiation pressure in the reservoir simulation. In addition, the analysis further suggests that the super low temperature thermal stress can greatly promote the generation of secondary cracks and the formation of complex fracture networks inside coal. The study provides an important reference for tight reservoir simulation of cryogenic fracturing.

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Acknowledgments

The authors would like to thank the National Natural Science Foundation of China (Grants. 51574270 and 51504280), the Changjiang Scholars and Innovative Research Team in University (Grant IRT_14R58), the Qingdao Science and Technology Project (Grant 15-9-1-55-jch), the Independent Innovation Research Project of Central University (Grant 16CX02022A), and the Talent Introduction Project of the China University of Petroleum (East China) (Grant YJ201601094) for their financial support.

References

Abaqus [Computer software]. SIMULIA, Providence, RI.
Aguilera, R. F., Ripple, R. D., and Aguilera, R. (2014). “Link between endowments, economics and environment in conventional and unconventional gas reservoirs.” Fuel, 126(Jun), 224–238.
Alqatahni, N. B., et al. (2016). “Experimental investigation of cryogenic fracturing of rock specimens under true triaxial confining stresses.” Proc., SPE Europec featured at the 78th EAGE Conf. and Exhibition, Society of Petroleum Engineers, Richardson, TX.
Aoki, K., Hibiya, K., and Yoshida, T. (1990). “Storage of refrigerated liquefied gases in rock caverns: Characteristics of rock under very low temperatures.” Tunnelling Underground Space Technol., 5(4), 319–325.
Biance, A. L., Clanet, C., and Quéré, D. (2003). “Leidenfrost drops.” Phys. Fluids, 15(6), 1632–1637.
Boudet, H., Clarke, C., Bugden, D., Maibach, E., Roser-Renouf, C., and Leiserowitz, A. (2014). “‘Fracking’ controversy and communication: Using national survey data to understand public perceptions of hydraulic fracturing.” Energy Policy, 65(Feb), 57–67.
Brannon, H. D. (2010). “Hydraulic fracturing materials: Application trends and consideration.” Proc., SPE Distinguished Lecture Program, Society of Petroleum Engineers, Richardson, TX.
Cai, C. Z., Gao, F., Li, G. S., Huang, Z. W., and Hou, P. (2016). “Evaluation of coal damage and cracking characteristics due to liquid nitrogen cooling on the basis of the energy evolution laws.” J. Nat. Gas Sci. Eng., 29, 30–36.
Cai, C. Z., Li, G. S., Huang, Z. W., Shen, Z. H., Tian, S. C., and Wei, J. W. (2014). “Experimental study of the effect of liquid nitrogen cooling on rock pore structure.” J. Nat. Gas Sci. Eng., 21, 507–517.
Cai, C. Z., Li, G. S., Huang, Z. W., Tian, S. C., Shen, Z. H., and Fu, X. (2015). “Experiment of coal damage due to super-cooling with liquid nitrogen.” J. Nat. Gas Sci. Eng., 22, 42–48.
Cha, M. S., et al. (2014). “Cryogenic fracturing for reservoir stimulation–Laboratory studies.” J. Pet. Sci. Eng., 124, 436–450.
Chaki, S., Takarli, M., and Agbodjan, W. P. (2008). “Influence of thermal damage on physical properties of a granite rock: Porosity, permeability and ultrasonic wave evolutions.” Constr. Build. Mater., 22(7), 1456–1461.
Chen, T. C., Yeung, M. R., and Mori, N. (2004). “Effect of water saturation on deterioration of welded tuff due to freeze-thaw action.” Cold Reg. Sci. Technol., 38(2), 127–136.
De Simone, S., Carrera, J., and Gómez-Castro, B. M. (2017). “A practical solution to the mechanical perturbations induced by non-isothermal injection into a permeable medium.” Int. J. Rock Mech. Min. Sci., 91, 7–17.
De Simone, S., Vilarrasa, V., Carrera, J., Alcolea, A., and Meier, P. (2013). “Thermal coupling may control mechanical stability of geothermal reservoirs during cold water injection.” Phys. Chem. Earth, 64, 117–126.
Filipussi, D. A., Guzmán, C. A., Xargay, H. D., Hucailuk, C., and Torres, D. N. (2015). “Study of acoustic emission in a compression test of andesite rock.” Procedia Mater. Sci., 9, 292–297.
Finnie, I., Cooper, G. A., and Berlie, J. (1979). “Fracture propagation in rock by transient cooling.” Int. J. Rock Mech. Min. Sci., 16(1), 11–21.
Gensterblum, Y., et al. (2015). “Gas transport and storage capacity in shale gas reservoirs–A review. Part A: Transport processes.” J. Unconv. Oil Gas Resour., 12(Dec), 87–122.
Gradeck, M., Seiler, N., Ruyer, P., and Maillet, D. (2013). “Heat transfer for Leidenfrost drops bouncing onto a hot surface.” Exp. Therm. Fluid Sci., 47(May), 14–25.
Grundmann, S. R., Rodvelt, G. D., Dials, G. A., and Allen, R. E. (1998). “Cryogenic nitrogen as a hydraulic fracturing fluid in the Devonian shale.” Proc., SPE Eastern Regional Meeting, Society of Petroleum Engineers, Richardson, TX.
Huang, Z. W., Wei, J. W., Li, G. S., and Cai, C. Z. (2016). “An experimental study of tensile and compressive strength of rocks under cryogenic nitrogen freezing.” Rock Soil Mech., 37(3), 694–700 (in Chinese).
Kocabas, I. (2004). “An analytical model of temperature and stress fields during cold water injection into an oil reservoir.” Proc., Abu Dhabi Int. Conf. and Exhibition, Abu Dhabi, United Arab Emirates, Society of Petroleum Engineers, Richardson, TX.
Li, G., Tang, C. A., and Liang, Z. Z. (2017). “Development of a parallel FE simulator for modeling the whole trans-scale failure process of rock from meso- to engineering-scale.” Comput. Geosci., 98, 73–86.
Li, Y. J., and Guo, H. (2006). “Quickly develop coal-bed methane industry.” Nat. Gas Ind., 2(2), 149–151 (in Chinese).
Li, Z. F., Xu, H. F., and Zhang, C. Y. (2016). “Liquid nitrogen gasification fracturing technology for shale gas development.” J. Pet. Sci. Eng., 138, 253–256.
Mcdaniel, B. W., Grundmann, S. R., Kendrick, W. D., Wilson, D. R., and Jordan, S. W. (1997). “Field applications of cryogenic nitrogen as a hydraulic fracturing fluid.” Proc., SPE Annual Technical Conf. and Exhibition, Society of Petroleum Engineers, Richardson, TX.
Perkins, T. K., and Gonzalez, J. A. (1985). “The effect of thermoelastic stresses on injection well fracturing.” SPE J., 25(1), 78–88.
Piane, C. D., Arena, A., Sarout, J., Esteban, L., and Cazes, E. (2015). “Micro-crack enhanced permeability in tight rocks: An experimental and microstructural study.” Tectonophysics, 665, 149–156.
Qiu, Z. J., and Deng, S. T. (2012). “Strategic position of unconventional natural gas resources in China.” Nat. Gas Ind., 32(1), 1–5 (in Chinese).
Raven, K. G., and Gale, J. E. (1985). “Water flow in natural rock fractures as a function of stress and sample size.” Int. J. Rock Mech. Min. Sci., 22(4), 251–261.
Sander, R., Pan, Z. J., and Connell, L. D. (2017). “Laboratory measurement of low permeability unconventional gas reservoir rocks: A review of experimental methods.” J. Nat. Gas Sci. Eng., 37, 248–279.
Siddiqi, G., and Evans, B. (2015). “Permeability and thermal cracking at pressure in Sioux quartzite.” J. Geol. Soc. London, 409(1), 49–66.
Singh, K. K., Singh, D. N., and Gamage, R. P. (2016). “Effect of sample size on the fluid flow through a single fractured granitoid.” J. Rock Mech. Geotech. Eng., 8(3), 329–340.
Singh, K. K., Singh, D. N., and Ranjith, P. G. (2015). “Laboratory simulation of flow through single fractured granite.” Rock Mech. Rock Eng., 48(3), 987–1000.
Tang, C. A., Wang, S. H., and Fu, F. Y. (2002). Numerical simulation of rock failure process, Science Press, Beijing (in Chinese).
Tang, S. B., Zhang, H., Tang, C. A., and Liu, H. Y. (2016). “Numerical model for the cracking behavior of heterogeneous brittle solids subjected to thermal shock.” Int. J. Solids Struct., 80(Feb), 520–531.
Vilarrasa, V., and Rutqvist, J. (2016). “Thermal effects on geologic carbon storage.” Earth Sci. Rev., 165, 245–256.
Wang, L., et al. (2016). “Waterless fracturing technologies for unconventional reservoirs-opportunities for liquid nitrogen.” J. Nat. Gas Sci. Eng., 35, 160–174.
Wang, L., and Li, S. B. (2011). “Numerical simulation of damage pattern growth in quasi-brittle materials.” Eng. Mech., 28(4), 238–244 (in Chinese).
Wang, Q., Zhu, W., Xu, T., Niu, L., and Wei, J. (2017). “Numerical simulation of rock creep behavior with a damage-based constitutive law.” Int. J. Geomech., 04016044.
Wang, X. S. (2012). “France continues to say ‘no’ to hydraulic fracturing.” ⟨http://www.nea.gov.cn/2012-09/27/c_131874729.htm⟩ (Sep. 27, 2012).
Wang, Y., and Dusseault, M. B. (2003). “A coupled conductive-convective thermo-poroelastic solution and implications for wellbore stability.” J. Petrol. Sci. Eng., 38(3–4), 187–198.
Winkler, E. M. (1968). “Frost damage to stone and concrete: Geological considerations.” Eng. Geol., 2(5), 315–323.
Witherspoon, P. A., Amick, C. H., Gale, J. E., and Iwai, K. (1979). “Observations of a potential size effect in experimental determination of the hydraulic properties of fractures.” Water Resour. Res., 15(5), 1142–1146.
Xia, M. F., Ke, F. J., and Bai, J. (1999). “Ensemble statistic of fracture pattern growth induced catastrophe.” Chin. Sci. Bull., 44(6), 562–572 (in Chinese).
Xu, G. M., and Liu, Q. S. (2005). “Analysis of mechanism of rock failure due to freeze-thaw cycling and mechanical testing study on frozen-thawed rocks.” Chin. J. Rock Mech. Eng., 24(17), 3076–3082 (in Chinese).
Yavuz, H., Altindag, R., Sarac, S., Ugur, I., and Sengun, N. (2006). “Estimating the index properties of deteriorated carbonate rocks due to freeze-thaw and thermal shock weathering.” Int. J. Rock Mech. Min. Sci., 43(5), 767–775.
Yin, S. Y., Zhao, D. J., and Zhai, G. B. (2016). “Investigation into the characteristics of rock damage caused by ultrasonic vibration.” Int. J. Rock Mech. Min. Sci., 84, 159–164.
Zhang, X. Y., Zhang, Q., and Wu, S. C. (2017). “Acoustic emission characteristics of the rock-like material containing a single flaw under different compressive loading rates.” Comput. Geotech., 83, 83–97.
Zhao, M. J., and Xu, R. (2000). “The rock damage and strength study based on ultrasonic velocity.” Chin. J. Geotech. Eng., 22(6), 720–722 (in Chinese).
Zhu, W. C., and Tang, C. A. (2002). “Numerical simulation on shear fracture process of concrete using mesoscopic mechanical model.” Constr. Build. Mater., 16(8), 453–463.

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Go to International Journal of Geomechanics
International Journal of Geomechanics
Volume 17Issue 12December 2017

History

Received: Jan 6, 2017
Accepted: Jun 15, 2017
Published online: Sep 29, 2017
Published in print: Dec 1, 2017
Discussion open until: Mar 1, 2018

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Yuanfang Cheng
Professor, School of Petroleum Engineering, China Univ. of Petroleum (East China), Qingdao 266580, China.
Ph.D. Candidate, School of Petroleum Engineering, China Univ. of Petroleum (East China), Qingdao 266580, China (corresponding author). E-mail: [email protected]
Huaidong Wang
Master’s Candidate, School of Petroleum Engineering, China Univ. of Petroleum (East China), Qingdao 266580, China.
Ubedullah Ansari
Ph.D. Candidate, School of Petroleum Engineering, China Univ. of Petroleum (East China), Qingdao 266580, China.
Zhongying Han
Lecturer, School of Petroleum Engineering, China Univ. of Petroleum (East China), Qingdao 266580, China.
Jiping Ding
Master’s Candidate, School of Petroleum Engineering, China Univ. of Petroleum (East China), Qingdao 266580, China.

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