Implications of Sample Size for the Thermal Extraction of Volatiles from Lunar Regolith with the PROSPECT Instrument Package
Publication: Journal of Aerospace Engineering
Volume 30, Issue 3
Abstract
The platform for resource observation and in situ prospecting for exploration, commercial exploitation, and transportation (PROSPECT) instrument package is under development by the European Space Agency for the upcoming Luna-27 mission to the lunar south pole. The purpose of the instrument is to detect and quantify volatiles on the lunar surface with the processing and analysis unit ProSPA. This paper describes the feasibility study and early breadboarding activities on ProSPA sample ovens during the Phase A study. The review of similar sample oven concepts led to the conclusion that none of these concepts satisfies new requirements of ProSPA regarding sample size and target temperatures. The trade studies presented in this paper include the estimation of power demands for scaled-up ovens, the influence of oven insulation, the compatibility of the utilized materials, and an experimental validation of the design. Experimental tests showed that the new oven design allows reaching the target temperatures and following most of the specified heating profiles with an imposed maximum power of 70 W. During the heating tests with the lunar regolith simulant NU-LHT-2M, sintering of the sample, reduction of the FeO content, and the creation of gas cavities were observed.
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Acknowledgments
The presented work was performed at the Institute of Astronautics at Technical University of Munich in the frame of the PROSPECT/ProSPA Phase A study in response to AO 7948 of the European Space Agency, as part of the General Studies Programme (GSP). The ProSPA Phase A activity was led by the Open University in Milton Keynes, U.K.
References
Barber, S. J., et al. (2015). “ProsPA: A miniature chemical laboratory for in situ assessment of lunar volatile resources.” European Lunar Symp., Istituto Nazionale di Fisica Nucleare (INFN), Frascati, Italy.
Biemann, K., et al. (1977). “The search for organic substances and inorganic volatile compounds in the surface of Mars.” J. Geophys. Res., 82(28), 4641–4658.
Boynton, W. V., et al. (2001). “Thermal and evolved gas analyzer: Part of the mars volatile and climate surveyor integrated payload.” J. Geophys. Res., 106(E8), 17683–17698.
Buch, A., et al. (2011). “In situ analysis of organic compounds on mars by gas chromatography-mass spectrometry onboard ExoMars (MOMA).” European Planetary Science Congress, EPSC Abstracts, Nantes, France.
Caps, R., Fricke, J., and Reiss, H. (1985). “Radiative heat transfer in anisotropic scattering fiber insulations.” High Temp-High Pressure, 17, 303–309.
Carpenter, J. D., et al. (2014). “Accessing and assessing lunar resources with PROSPECT.” Annual Meeting of the Lunar Exploration Analysis Group, Lunar and Planetary Institute, Houston.
Colozza, A. J. (1991). “Analysis of lunar regolith thermal energy storage.”, National Aeronautics and Space Administration, Washington, DC.
COMSOL Multiphysics [Computer software]. COMSOL, Burlington, MA.
Cremers, C. J., and Hsia, H. S. (1974). “Thermal conductivity of Apollo 16 lunar fines.” Proc., 5th Lunar ScienceConf., Lunar and Planetary Institute, Houston, 2703–2708.
Desai, P. D., Chu, T. K., James, H. M., and Ho, C. Y. (1984). “Electrical resistivity of selected elements.” J. Phys. Chem. Ref. Data, 13(4), 1069–1096.
Finzi, A. E., et al. (2007). “SD2—How to sample a comet.” Space Sci. Rev., 128(1-4), 281–299.
Fisackerly, R., et al. (2015). “Accessing, drilling and operating at the lunar south pole: Status of European plans and activities.” 13th Symp. on Advanced Space Technologies in Robotics and Automation, European Space Agency, Noordwijk, Netherlands.
Gibson, M. A., and Knudsen, C. W. (1985). “Lunar oxygen production from ilmenite.” Lunar Bases Sp. Act. 21st Century, W. W. Mendel, ed., Lunar and Planetary Institute, Houston, 543–550.
Gillies, D., Lehoczky, S., Palosz, W., Carpenter, P., and Salvail, P. (2007). “Poisoning of heat pipes.” Space Technology and Applications Int. Forum, AIP Publishing, Melville, NY.
Glavin, D. P., et al. (2012). “Volatile analysis by pyrolysis of regolith for planetary resource exploration.” IEEE Aerospace Conf. Proc., IEEE, Piscataway, NJ.
Goesmann, F., et al. (2007). “COSAC, the cometary sampling and composition experiment on Philae.” Space Sci. Rev., 128(1-4), 257–280.
Hayne, P. O., et al. (2015). “Evidence for exposed water ice in the Moon’s south polar regions from Lunar Reconnaissance Orbiter ultraviolet albedo and temperature measurements.” Icarus, 255, 58–69.
Hemingway, B. S., Robie, R. A., and Wilson, W. H. (1973). “Specific heats of lunar soils, Basalt, and Breccias from the Apollo 14, 15, and 16 landing sites, between 90 and 350°K.” Proc., 4th Lunar Science Conf., Lunar and Planetary Institute, Houston, 2481–2487.
Hibbitts, C. A., et al. (2011). “Thermal stability of water and hydroxyl on the surface of the Moon from temperature-programmed desorption measurements of lunar analog materials.” Icarus, 213(1), 64–72.
Horai, K. (1981). “The effect of interstitial gaseous pressure on the thermal conductivity of a simulated Apollo 12 lunar soil sample.” Phys. Earth Planet. Inter., 27(1), 60–71.
Kleinhenz, J. (2014). “Lunar polar environmental testing: Regolith simulant conditioning.” 7th Symp. on Space Resource Utilization, American Institute of Aeronautics and Astronautics, Reston, VA.
LabVIEW [Computer software]. National Instruments, Austin, TX.
Lindemann, A., and Schmidt, J. (2002). “Thermal analytical investigations of metals including the melting range.” Int. Heat Transfer Conf., Societe Francaise de Thermique, Paris, 297–301.
Mahaffy, P. (2008). “Exploration of the habitability of mars: Development of analytical protocols for measurement of organic carbon on the 2009 Mars Science Laboratory.” Space Sci. Rev., 135(1-4), 255–268.
Mahaffy, P. R., et al. (2012). “The sample analysis at mars investigation and instrument suite.” Space Sci. Rev., 170(1-4), 401–478.
McGrath, R. B., and Badcock, G. C. (1987). “New dispersion strengthened platinum alloy.” Platin. Met. Rev., 31(1), 8–11.
Morse, A. D., et al. (2012). “The lunar volatile resources analysis package.” European Lunar Symp., German Aerospace Center, Berlin.
Parzinger, S. (2014). “Analytische modellierung der temperatur- und gasdruckabhängigen effektiven Wärmeleitfähigkeit von Pulvern [Analytical modeling of the temperature- and gas pressure dependent effective thermal conductivity of powders].” Ph.D. dissertation, Technical Univ. of Munich, München, Germany.
Paz, A., Oryshchyn, L., Jensen, S., Sanders, G. B., Lee, K., and Reddington, M. (2013). “Resolve oven field demonstration unit for lunar resource extraction.” 51st AIAA Aerospace Science Meeting, American Institute of Aeronautics and Astronautics, Reston, VA.
Pullan, D., Sims, M. R., Wright, I. P., Pillinger, C. T., and Trautner, R. (2004). “Beagle 2: The exobiological lander of mars express.” European Space Agency, Paris.
Reiss, P., Hager, P., Hoehn, A., Rott, M., and Walter, U. (2014). “Flowability of lunar regolith simulants under reduced gravity and vacuum in hopper-based conveying devices.” J. Terramechanics, 55, 61–72.
Rosenberg, S. D., Beegle, R. L., Jr., Guter, G. A., Miller, F. E., and Rothenberg, M. (1992). “The onsite manufacture of propellant oxygen from lunar resources.” Space resources materials, M. F. McKay, D. S. McKay, and M. B. Duke, eds., 162–185.
Rosenberg, S. D., Musbah, O., and Rice, E. E. (1996). “Carbothermal reduction of lunar materials for oxygen production on the moon: Reduction of lunar simulants with carbon.” Lunar Planetary Science Conf. XXVII, Lunar and Planetary Institute, Houston, 1103–1104.
Schreiner, S. S., Dominguez, J. A., Sibille, L., and Hoffman, J. A. (2016). “Thermophysical property models for lunar regolith.” Adv. Sp. Res., 57(5), 1209–1222.
Schwandt, C., Hamilton, J. A., Fray, D. J., and Crawford, I. A. (2012). “Oxygen from lunar regolith.” Moon, V. Badescu, ed., Springer, Berlin, 165–187.
Seboldt, W., et al. (1993). “Lunar oxygen extraction using fluorine.” Resources of near-earth space, J. Lewis, M. S. Matthews, and M. L. Guerrieri, eds., University of Arizona Press, Tucson, AZ and London, 129–147.
Special Metals Corporation. (2005). INCONEL alloy 693—Excellent resistance to metal dusting and high temperature corrosion, Huntington, WV.
Steiniger, H., et al. (2012). “Mars organic molecule analyzer (MOMA) onboard ExoMars 2018.” Int. Workshop on Instrumentation for Planetary Missions, National Aeronautics and Space Administration, Washington, DC.
Stokes, J. (1987). “Platinum in the glass industry.” Platin. Met. Rev., 31(2), 54–62.
Taylor, L. A., and Carrier, W. D. (1993). “Oxygen production on the moon: An overview and evaluation.” Resources of near earth space, J. Lewis, M. S. Matthews, and M. L. Guerrieri, eds., University of Arizona Press, Tucson, AZ, and London, 69–108.
ten Kate, I. L., et al. (2010). “VAPoR—Volatile analysis by pyrolysis of regolith—An instrument for in situ detection of water, noble gases, and organics on the Moon.” Planet. Space Sci., 58(7-8), 1007–1017.
USGS. (2008). “Material safety data sheet NU-LHT-2M.” Reston, VA.
Vaithinathan, K., and Lanam, R. (2005). “Features and benefits of different platinum alloy.” Technical articles: Alloy, Platinum Guild International, Iselin, NJ.
Wiener, M., Reichenauer, G., Braxmeier, S., Hemberger, F., and Ebert, H.-P. (2009). “Carbon aerogel-based high-temperature thermal insulation.” Int. J. Thermophys., 30(4), 1372–1385.
Wright, I. P., et al. (2007). “Ptolemy—An instrument to measure stable isotopic ratios of key volatiles on a cometary nucleus.” Space Sci. Rev., 128(1-4), 363–381.
Wright, I. P., et al. (2012). “L-VRAP—A lunar volatile resources analysis package for lunar exploration.” Planet. Space Sci., 74(1), 254–263.
Yoshida, H., Watanabe, T., Kanamori, H., Yoshida, T., Ogiwara, S., and Eguchi, K. (2000). “Experimental study on water production by hydrogen reduction of lunar soil simulant in a fixed bed reactor.” Second Space Resources Roundtable, Colorado School of Mines, Golden, CO.
Zeng, X., He, C., and Wilkinson, A. (2010). “Geotechnical properties of NU-LHT-2M lunar highland simulant.” J. Aerosp. Eng., 213–218.
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© 2016 American Society of Civil Engineers.
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Received: Mar 22, 2016
Accepted: Jul 8, 2016
Published online: Sep 22, 2016
Discussion open until: Feb 22, 2017
Published in print: May 1, 2017
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