TECHNICAL PAPERS
May 15, 2003

Rheological Characterization of Heterogeneous Materials with Evolving Properties

Publication: Journal of Materials in Civil Engineering
Volume 15, Issue 3

Abstract

The paper deals with the rheological characterization of different heterogeneous civil engineering materials that have time-dependent properties. Studies on cellular concrete, mortar, hydraulic concrete, and cold bituminous mixes are presented. The properties are monitored throughout setting and hardening. Such materials are heterogeneous mixtures containing solid particles, binder, fluids, and gas bubbles. For all of these materials, different formulations were investigated, such as water content, binder proportioning, and compaction level. A nondestructive device allows the setting to be monitored and to be clearly characterized. This device makes it possible to simultaneously study the propagation of compressional and shear waves in the same sample of material. To prevent diffraction of waves from heterogeneities, a condition of a long wavelength compared to the heterogeneity size is required, so low frequencies are used (20–1,000 Hz). Velocity and damping coefficients versus time are deduced, then related to rheological viscoelastic properties by an inverse analysis. The linear behavior of these materials under small strains is proved, and the measurements are very repetitive and sensitive to the nature and the component proportioning of the materials. The rheological evolutions of the different materials are presented and compared. It is shown that the normalized evolution of hydraulic concretes follows a single master curve for all of the different formulations investigated. Similar results are established for cellular concretes and mortars.

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References

Arnaud, L., Boutin, C., and Villain, G. (1995). “The setting of cement pastes followed up by the vibroscope.” Proc., Int. Symp. on Non-Destructive Testing in Civil Engineering (NDTE), Schickert and Wiggenhauser, eds., 1323–1330.
Arnaud, L., and Thinet, S. (2000). “A device to monitor continuously the setting of concrete.” Proc., 15th World Conf. on Nondestructive testing.
Arnaud, L., and Thinet, S. (2002). “Rheology of concrete during setting and hardening. Experimental approach and rheological measurements.” Concr. Sci. Eng., in press.
Arnaud, L., Villain, G., and Boutin, C.(2000a). “Mesures rhéologiques sur matériaux en cours de prise.” C. R. Acad. Sc. Paris, 328(IIb), 217–223.
Arnaud, L., Villain, G., and Boutin, C.(2000b). “Rhéologie des matériaux en cours prise: II. Approche théorique.” C. R. Acad. Sc. Paris, 328(IIb), 855–862.
Boutin, C., and Arnaud, L.(1995). “Mechanical characterization of heterogeneous materials during setting.” Eur. J. Mech. A/Solids, 14(4), 633–656.
Boumiz, A., Vernet, C., and Tenoudji, F. C. (1996). Advanced cement based materials 3.
Grosse, C. U., and Reinhardt, H. W. (2000). “Ultrasound technique for quality control of cementitious materials.” Proc., 15th World Conf. on Nondestructive Testing.
Isacsson, U.(1986). “Une synthèse des méthodes de laboratoire pour étudier la stabilité des émulsions bitumineuses.” Bull. Liaison LCPC, 141, 67–80.
Nachbaur, L., Sedran, T., and de Larrard, F. (2001). “Rhéométrie du béton. Comparaison de rhéomètres. Rhéologie du béton hydraulique en cours de prise.” Proc., 36ème Coll. du GFR.
Reinhardt, H.-W., and Grosse, C. U. (1996). “Setting and hardening of concrete continuously monitored by elastic waves.” Proc., Int. RILEM Conf., Cachan Cedex, France, 415–425.
Sanchez-Palencia, E. (1980). “Nonhomogeneous media and vibration theory.” Lect. Notes Phys., 127, Springer, Berlin.
Sayers, C. M., and Dalhin, A.(1993). “Propagation of ultrasound through hydrating cement pastes at early times.” Adv. Cem. Based Mater., 1, 12–21.
Sayers, C. M., and Grenfell, R. L.(1992). Ultrasonics, 31(3), 147–153.
Thinet, S. (2000). “Caractérisation rhéologique de matériaux hétérogènes évolutifs par propagation d’ondes acoustiques.” Thesis Ecole MEGA (ENTPE/INSA).
Villain, G. (1997). “Caractérisation de la prise des matériaux à base de ciment par propagation d’ondes acoustiques et ultrasonores.” Thesis ENTPE/INSA.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 15Issue 3June 2003
Pages: 255 - 265

History

Received: Mar 5, 2002
Accepted: Aug 8, 2002
Published online: May 15, 2003
Published in print: Jun 2003

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Authors

Affiliations

Laurent Arnaud
Ecole Nationale des Travaux Publics de l’Etat, Geomaterials Laboratory, DGCB-LGM, URA CNRS 1652, Rue Maurice Audin, 69518 Vaulx-En-Velin, France.

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