Abstract

This study evaluates the feasibility of proposed simplifications of the universal simple aging test (USAT) to simulate the short-term aging of asphalt binders (STUSAT). Rutting and fatigue parameters of four neat and four modified binders (two asphalt-rubbers and two polymer-modified ones) were determined after aging the materials in both the STUSAT and the regular rolling thin-film oven test (RTFOT). Rheological tests included multiple stress creep and recovery (MSCR) and linear amplitude sweep (LAS). The fatigue parameter (|G*|.sinδ) and the Glover–Rowe parameter were also determined. Overall, the findings of the MSCR and fatigue parameters for the STUSAT-aged binders are in close agreement with the ones derived from the RTFOT-aged ones. The same can be said for the high performance grades (PG) and the assigned traffic levels for each material. Moreover, STUSAT does not appear to mask the formulations that are overly stress sensitive in the MSCR tests, and it does not seem to penalize the binders that can withstand high traffic levels or modify the classification of the binder according to stress sensitivity. The mass loss for both procedures is equivalent, but STUSAT presented higher variations due to the small amount of sample. The ranking order based on the three fatigue indicators for both aging protocols converged in terms of which are the best and worst materials: polymer-modified binder C1 was the best one, followed by one of the two asphalt-rubbers (B1 or B2), with the neat binders A4, A1, and A2 as the worst materials. These findings suggest that STUSAT is a feasible alternative to regular RTFOT, once the procedure demands a simple set of equipment. Future studies are recommended to validate the applicability of STUSAT using a higher number of asphalt binders.

Practical Applications

The findings of this paper may provide civil engineers and highway agencies with an easy-to-use, short-term aging test, designated as the short-term universal simple aging test (STUSAT), which is a simplified version of the universal simple aging test (USAT). The test described here is intended to be an alternative to the regular rolling thin-film oven test (RTFOT). It requires only a regular forced-air oven, silicone apparatuses, and aluminum plates to age the binder and simulate the actual aging the material experiences during plant production, hauling, and compaction. This method is especially useful for asphalt laboratories in developing countries, which typically do not have a rolling thin-film oven to conduct the regular short-term aging tests per the ASTM and AASHTO standards. Moreover, STUSAT demands a smaller mass of binder (only 3.0 g) and a lower test time (50 min) when compared with RTFOT. The test temperature (150°C) is also lower than the one in RTFOT (163°C), thereby saving energy and time during the regular operations in the laboratory.

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Data Availability Statement

All data, models, and code generated or used during the study appear in the published article.

Acknowledgments

This study was financed in part by the Coordination of Superior Level Staff Improvement–Brasil (CAPES)–Finance Code 001.
Author contributions: L. G. Buzon: Conceptualization, Data curation, Formal analysis, Investigation, Methodology, Software, Writing–original draft. M. D. I. Domingos: Validation, Visualization, Writing–original draft, Writing–review and editing. A. L. Faxina: Project administration, Resources, Supervision, Writing–review and editing. P. H. Osmari: Project administration, Resources, Supervision, Writing–review and editing.

References

AASHTO. 2014. Standard method of test for estimating damage tolerance of asphalt binders using the linear amplitude sweep. AASHTO TP 101-14. Washington, DC: AASHTO.
Airey, G. D. 2003. “State of the art report on ageing test methods for bituminous pavement materials.” Int. J. Pavement Eng. 4 (3): 165–176. https://doi.org/10.1080/1029843042000198568.
Ameri, M., A. Mansourkhaki, and D. Daryaee. 2018. “Evaluation of fatigue behavior of high reclaimed asphalt binder mixes modified with rejuvenator and softer bitumen.” Constr. Build. Mater. 191 (Dec): 702–712. https://doi.org/10.1016/j.conbuildmat.2018.09.182.
ANP (Agência Nacional do Petróleo, Gás e Biocombustíveis). 2005. Especificação para cimento asfáltico de petróleo por penetração. Rio de Janeiro, Brazil: ANP.
ASTM. 2015. Standard test method for determining the rheological properties of asphalt binder using a dynamic shear rheometer. ASTM D7175-15. West Conshohocken, PA: ASTM.
ASTM. 2016. Standard practice for determining the continuous grading temperatures and continuous grades for PG graded asphalt binders. ASTM D7643-16. West Conshohocken, PA: ASTM.
ASTM. 2019a. Standard specification for gravity-convection and forced-ventilation ovens. ASTM E145-19. West Conshohocken, PA: ASTM.
ASTM. 2019b. Standard test method for effect of heat and air on a moving film of asphalt (rolling thin-film oven test). ASTM D2872-19. West Conshohocken, PA: ASTM.
ASTM. 2020. Standard test method for multiple stress creep and recovery (MSCR) of asphalt binder using a dynamic shear rheometer. ASTM D7405-20. West Conshohocken, PA: ASTM.
ASTM. 2021a. Standard specification for performance-graded asphalt binder. ASTM D6373-21. West Conshohocken, PA: ASTM.
ASTM. 2021b. Standard specification for performance-graded asphalt binder using multiple stress creep recovery (MSCR) test. ASTM D8239-21. West Conshohocken, PA: ASTM.
Bahia, H. U., D. I. Hanson, M. Zeng, H. Zhai, M. A. Khatri, and R. M. Anderson. 2001. Characterization of modified asphalt binders in Superpave mix design. Washington, DC: National Academy Press.
Behnia, B., W. G. Buttlar, and H. Reis. 2014. “Cooling cycle effects on low temperature cracking characteristics of asphalt concrete mixture.” Mater. Struct. 47 (8): 1359–1371. https://doi.org/10.1617/s11527-014-0310-y.
Behnood, A., and J. Olek. 2017. “Rheological properties of asphalt binders modified with styrene-butadiene-styrene (SBS), ground tire rubber (GTR), or polyphosphoric acid (PPA).” Constr. Build. Mater. 151 (Oct): 464–478. https://doi.org/10.1016/j.conbuildmat.2017.06.115.
Behnood, A., A. Shah, R. S. McDaniel, M. Beeson, and J. Olek. 2016. “High-temperature properties of asphalt binders: Comparison of multiple stress creep recovery and performance grading systems.” Transp. Res. Rec. 2574 (1): 131–143. https://doi.org/10.3141/2574-15.
Benešová, L., and J. Valentin. 2017. “Influence of selected test parameters on measured values during the MSCR test.” IOP Conf. Ser. Mater. Sci. Eng. 236 (1): 012016. https://doi.org/10.1088/1757-899X/236/1/012016.
Bessa, I. S. 2017. “Laboratory and field study of fatigue cracking prediction in asphalt pavements.” Doctoral thesis, Escola Politécnica, Univ. of São Paulo.
Bonnetti, K. S., K. Nam, and H. U. Bahia. 2002. “Measuring and defining fatigue behavior of asphalt binders.” Transp. Res. Rec. 1810 (1): 33–43. https://doi.org/10.3141/1810-05.
Borghi, A., A. J. B. Carrión, D. Lo Presti, and F. Giustozzi. 2017. “Effects of laboratory aging on properties of biorejuvenated asphalt binders.” J. Mater. Civ. Eng. 29 (10): 04017149. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001995.
Christensen, D. W., and N. Tran. 2022. Relationships between the fatigue properties of asphalt binders and the fatigue performance of asphalt mixtures. Washington, DC: National Cooperative Highway Research Program.
D’Angelo, J. 2018. “What is Jnr diff and what does it mean?” Accessed October 13, 2023. https://asphalt.mydigitalpublication.com/articles/what-is-jnr-diff-.
D’Angelo, J. A. 2009. “The relationship of the MSCR test to rutting.” Road Mater. Pavement Des. 10 (1): 61–80. https://doi.org/10.1080/14680629.2009.9690236.
Daniel, J. S., N. Gibson, S. Tarbox, A. Copeland, and A. Andriescu. 2013. “Effect of long-term ageing on RAP mixtures: Laboratory evaluation of plant-produced mixtures.” Road Mater. Pavement Des. 14 (2): 173–192. https://doi.org/10.1080/14680629.2013.812840.
DNIT (Departamento Nacional de Infraestrutura de Transportes). 2009. Pavimentação flexível–cimento asfáltico modificado por borracha de pneus inservíveis pelo processo via úmida, do tipo “Terminal Blending”–Especificação de material. Rio de Janeiro, Brazil: DNIT.
DNIT (Departamento Nacional de Infraestrutura de Transportes). 2011. Cimento asfáltico de petróleo modificado por polímero elastomérico–Especificação de material. Rio de Janeiro, Brazil: DNIT.
Domingos, M. D. I., and A. L. Faxina. 2015. “Rheological analysis of asphalt binders modified with Elvaloy® terpolymer and polyphosphoric acid on the multiple stress creep and recovery test.” Mater. Struct. 48 (5): 1405–1416. https://doi.org/10.1617/s11527-013-0242-y.
Domingos, M. D. I., and A. L. Faxina. 2016. “Susceptibility of asphalt binders to rutting: Literature review.” J. Mater. Civ. Eng. 28 (2): 04015134. https://doi.org/10.1061/(ASCE)MT.1943-5533.0001364.
Duarte, G. M., and A. L. Faxina. 2021. “High-temperature rheological properties of asphalt binders modified with recycled low-density polyethylene and crumb rubber.” Constr. Build. Mater. 298 (Jun): 123852. https://doi.org/10.1016/j.conbuildmat.2021.123852.
Espinoza, J., C. Medina, A. Calabi-Floody, E. Sánchez-Alonso, G. Valdés, and A. Quiroz. 2020. “Evaluation of reductions in fume emissions (VOCs and SVOCs) from warm mix asphalt incorporating natural zeolite and reclaimed asphalt pavement for sustainable pavements.” Sustainability 12 (22): 9546. https://doi.org/10.3390/su12229546.
Farrar, M., R. W. Grimes, T. F. Turner, and J.-P. Planche. 2015. The universal simple aging test (USAT) and low temperature performance grading using small plate dynamic shear rheometry: An alternative to standard RTFO, PAV, and BBR for HMA and WMA. Laramie, WY: Western Research Institute.
Farrar, M. J., R. W. Grimes, C. Sui, J. P. Planche, S. C. Huang, T. F. Turner, and R. Glaser. 2012. “Thin film oxidative aging and low temperature performance grading using small plate dynamic shear rheometry: An alternative to standard RTFO, PAV, and BBR.” In Proc., 5th Eurasphalt & Eurobitume Congress. Brussels, Belgium: European Asphalt Pavement Association.
Fernández-Gómez, W. D., H. R. Quintana, and F. Reyes Lizcano. 2013. “A review of asphalt and asphalt mixture aging.” Ingeniería e Investigación 33 (1): 5–12. https://doi.org/10.15446/ing.investig.v33n1.37659.
FHWA (Federal Highway Administration). 2016. The universal simple aging test. Washington, DC: FHWA.
Gaspar, M. S., B. Nogueira, K. L. Vasconcelos, L. F. M. Leite, and L. L. B. Bernucci. 2021. “Effect of different creep and recovery times on the MSCR test for highly modified asphalt binder.” J. Test. Eval. 49 (1): 313–328. https://doi.org/10.1520/JTE20180584.
Harman, T., J. Youtucheff, and J. Bukowski. 2011. The multiple stress creep recovery (MSCR) procedure. Washington, DC: Federal Highway Administration.
Hintz, C. 2012. “Understanding mechanisms leading to asphalt binder fatigue.” Ph.D. dissertation, Dept. of Civil and Environmental Engineering, Univ. of Wisconsin–Madison.
Johnson, C. L. 2010. “Estimating asphalt binder fatigue resistance using an accelerated test method.” Ph.D. dissertation, Dept. of Civil and Environmental Engineering, Univ. of Wisconsin–Madison.
Klinsky, L. M. G., V. S. S. Bardini, and V. C. Faria. 2020. “Evaluation of permanent deformation of asphalt rubber using multiple stress creep recovery tests and flow number tests.” Transportes 28 (2): 76–86. https://doi.org/10.14295/transportes.v28i2.2110.
Lesueur, D. 2009. “The colloidal structure of bitumen: Consequences on the rheology and on the mechanisms of bitumen modification.” Adv. Colloid Interface Sci. 145 (1–2): 42–82. https://doi.org/10.1016/j.cis.2008.08.011.
Majidifard, H., B. Jahangiri, P. Rath, A. H. Alavi, and W. G. Buttlar. 2021. “A deep learning approach to predict Hamburg rutting curve.” Road Mater. Pavement Des. 22 (9): 2159–2180. https://doi.org/10.1080/14680629.2021.1886160.
Martins, A. T. 2014. “Contribuição para a validação do ensaio de resistência ao dano por fadiga para ligantes asfálticos.” M.Sc. thesis, Programa de Engenharia Civil, Federal Univ. of Rio de Janeiro.
Possebon, E. P. 2021. “Advanced characterization of Brazilian bitumens and mixtures.” Ph.D. dissertation, Programa de Pós-Graduação em Engenharia Civil, Federal Univ. of Santa Maria.
Shalaby, A. 2002. “Modelling short-term aging of asphalt binders using the rolling thin film oven test.” Can. J. Civ. Eng. 29 (1): 135–144. https://doi.org/10.1139/l01-086.
Sirin, O., D. K. Paul, E. Kassem, and M. Ohiduzzaman. 2019. “Evaluation of short-term aging protocol for asphalt mixtures.” Appl. Sci. 9 (14): 2783. https://doi.org/10.3390/app9142783.
Underwood, B. S. 2011. “Multiscale constitutive modeling of asphalt concrete.” Ph.D. dissertation, Dept. of Civil Engineering, North Carolina State Univ.
Wang, H., X. Liu, M. Ven, G. Lu, S. Erkens, and A. Skarpas. 2020. “Fatigue performance of long-term aged crumb rubber modified bitumen containing warm-mix additives.” Constr. Build. Mater. 239 (Apr): 117824. https://doi.org/10.1016/j.conbuildmat.2019.117824.
Yin, F., E. Arámbula-Mercado, A. Epps Martin, D. Newcomb, and N. Tran. 2017. “Long-term ageing of asphalt mixtures.” Road Mater. Pavement Des. 18 (1): 2–27. https://doi.org/10.1080/14680629.2016.1266739.
Zegeye, E. T., K. H. Moon, M. Turos, T. R. Clyne, and M. O. Marasteanu. 2012. “Low temperature fracture properties of polyphosphoric acid modified asphalt mixtures.” J. Mater. Civ. Eng. 24 (8): 1089–1096. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000488.
Zeinali, A., P. B. Blankenship, and K. C. Mahboub. 2014. “Effect of long-term ambient storage of compacted asphalt mixtures on laboratory-measured dynamic modulus and flow number.” Transp. Res. Rec. 2447 (1): 109–116. https://doi.org/10.3141/2447-12.
Zhang, H., K. Shen, G. Xu, J. Tong, R. Wang, D. Cai, and X. Chen. 2020. “Fatigue resistance of aged asphalt binders: An investigation of different analytical methods in linear amplitude sweep test.” Constr. Build. Mater. 241 (Apr): 118099. https://doi.org/10.1016/j.conbuildmat.2020.118099.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 36Issue 10October 2024

History

Received: Nov 22, 2023
Accepted: Mar 6, 2024
Published online: Aug 1, 2024
Published in print: Oct 1, 2024
Discussion open until: Jan 1, 2025

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Civil Engineer, Dept. of Transportation Engineering, São Carlos School of Engineering, Univ. of São Paulo, Avenida Trabalhador São-Carlense, 400, Parque Arnold Schimidt, São Carlos, SP 13566-590, Brazil (corresponding author). ORCID: https://orcid.org/0000-0001-7677-0165. Email: [email protected]
Matheus David Inocente Domingos, Ph.D. https://orcid.org/0000-0002-2514-9915 [email protected]
Professor of Transportation Engineering, Academic Dept. of Civil Construction, Federal Univ. of Technology-Parana (UTFPR), Rua Deputado Heitor Alencar Furtado, 5000, Ecoville, Curitiba, PR 81280-340, Brazil. ORCID: https://orcid.org/0000-0002-2514-9915. Email: [email protected]
Professor of Transportation Engineering, Dept. of Transportation Engineering, São Carlos School of Engineering, Univ. of São Paulo, Avenida Trabalhador São-Carlense, 400, Parque Arnold Schimidt, São Carlos, SP 13566-590, Brazil. ORCID: https://orcid.org/0000-0002-8087-3551. Email: [email protected]
Professor of Transportation Engineering, Dept. of Transportation Engineering, São Carlos School of Engineering, Univ. of São Paulo, Avenida Trabalhador São-Carlense, 400, Parque Arnold Schimidt, São Carlos, SP 13566-590, Brazil. ORCID: https://orcid.org/0000-0003-1812-0820. Email: [email protected]

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