Technical Papers
Dec 28, 2022

Laboratory Investigation on the Rutting and Fracture Resistance of Hot-Mix Asphalt Containing Nanographene Oxide

Publication: Journal of Materials in Civil Engineering
Volume 35, Issue 3

Abstract

The use of nanomaterials has brought about a huge revolution in the development of various industries. Moreover, in the pavement industry, researchers have been applying nanomaterials for many years due to their unique properties to enhance the features of asphalt mixtures and increase their resistance to various failures. In this study, nanographene oxide (GO) has been used in the amount of 0.2, 0.5, and 0.8 percent of consumed bitumen to improve the low-temperature cracking resistance and the high-temperature rutting resistance of hot-mix asphalt (HMA). For this purpose, to examine the impact of this material on the HMA, the semicircular bending (SCB) fracture test and Hamburg wheel tracking (HWT) test were applied. In addition, conventional bitumen tests were performed to investigate the impact of nanoGO on virgin bitumen in this study. The outcomes of conventional bitumen experiments displayed that the addition of nanoGO to pure bitumen augments viscosity, specific gravity, and softening point and reduces the penetration and ductility of pure bitumen. Furthermore, outcomes of the SCB fracture test indicated that nanoGO enhances the stress intensity factor (SIF) of the asphalt mixture and improves the low-temperature cracking resistance of asphalt specimens. Moreover, the addition of nanoGO to the asphalt mixture increased rutting resistance and decreased rutting depth. In addition, the results of the ANCOVA statistical analysis demonstrated the significant effect of this nanomaterial on the improvement of the low-temperature cracking resistance and the rutting resistance of HMA.

Get full access to this article

View all available purchase options and get full access to this article.

Data Availability Statement

Some or all data, models, or code that support the findings of this study are available from the corresponding author upon reasonable request.

References

AASHTO. 2009. Standard method of test for evaluation of superpave gyratory compactor (SGC) internal angle of gyration using simulated loading. AASHTO TP-71. Washington, DC: AASHTO.
AASHTO. 2014. Standard method of test for hamburg wheel-track testing of compacted hot-mix asphalt (HMA). AASHTO T 324-14. Washington, DC: AASHTO.
AASHTO. 2019. Standard method of test for preparing and determining the density of asphalt mixture specimens by means of the superpave gyratory compactor. AASHTO T 312. Washington, DC: AASHTO.
Adnan, A. M., X. Luo, C. Lü, J. Wang, and Z. Huang. 2020. “Improving mechanics behavior of hot mix asphalt using graphene-oxide.” Constr. Build. Mater. 254 (Sep): 119261. https://doi.org/10.1016/j.conbuildmat.2020.119261.
Aliha, M. R. M., F. Berto, A. Mousavi, and S. M. J. Razavi. 2017a. “On the applicability of ASED criterion for predicting mixed mode I + II fracture toughness results of a rock material.” Theor. Appl. Fract. Mech. 92 (Dec): 198–204. https://doi.org/10.1016/j.tafmec.2017.07.022.
Aliha, M. R. M., H. Fazaeli, S. Aghajani, and F. M. Nejad. 2015. “Effect of temperature and air void on mixed mode fracture toughness of modified asphalt mixtures.” Constr. Build. Mater. 95 (Oct): 545–555. https://doi.org/10.1016/j.conbuildmat.2015.07.165.
Aliha, M. R. M., A. Razmi, and A. Mansourian. 2017b. “The influence of natural and synthetic fibers on low temperature mixed mode I + II fracture behavior of warm mix asphalt (WMA) materials.” Eng. Fract. Mech. 182 (Sep): 322–336. https://doi.org/10.1016/j.engfracmech.2017.06.003.
Ameri, M., A. Mansourian, S. Pirmohammad, M. R. M. Aliha, and M. R. Ayatollahi. 2012. “Mixed mode fracture resistance of asphalt concrete mixtures.” Eng. Fract. Mech. 93 (Oct): 153–167. https://doi.org/10.1016/j.engfracmech.2012.06.015.
ASTM. n.d. Standard test method for resistance to plastic flow of bituminous mixtures using Marshall apparatus. ASTM D1559. West Conshohocken, PA: ASTM.
ASTM. 2007. Standard test method for ductility of bituminous materials. ASTM D113. West Conshohocken, PA: ASTM.
ASTM. 2009. Standard test method for density of semi-solid bituminous materials (pycnometer method). ASTM D70. West Conshohocken, PA: ASTM.
ASTM. 2010. Standard test method for resistance to degradation of small-size coarse aggregate by abrasion and impact in the Los Angeles machine. ASTM C-131. West Conshohocken, PA: ASTM.
ASTM. 2013a. Standard test method for penetration of bituminous materials. ASTM D5. West Conshohocken, PA: ASTM.
ASTM. 2013b. Standard test method for saybolt viscosity. ASTM D88. West Conshohocken, PA: ASTM.
ASTM. 2014. Standard test method for softening point of bitumen (ring-and-ball apparatus). ASTM D36/D36M. West Conshohocken, PA: ASTM.
ASTM. 2016a. Standard test method for sand equivalent value of soils and fine aggregate. ASTM D-2419. West Conshohocken, PA: ASTM.
ASTM. 2016b. Standard test method for relative density (specific gravity) and absorption of coarse aggregate. ASTM C-127. West Conshohocken, PA: ASTM.
ASTM. 2016c. Standard test method for relative density (specific gravity) and absorption of fine aggregate. ASTM C-128. West Conshohocken, PA: ASTM.
ASTM. 2017a. Standard test method for determining the percentage of fractured particles in coarse aggregate. ASTM D-5821. West Conshohocken, PA: ASTM.
ASTM. 2017b. Standard test methods for specific gravity of soil solids by water pycnometer. ASTM D-854. West Conshohocken, PA: ASTM.
Ayatollahi, M. R., M. R. M. Aliha, and H. Saghafi. 2011. “An improved semi-circular bend specimen for investigating mixed mode brittle fracture.” Eng. Fract. Mech. 78 (1): 110–123. https://doi.org/10.1016/j.engfracmech.2010.10.001.
Chaturabong, P., and H. U. Bahia. 2017. “Mechanisms of asphalt mixture rutting in the dry Hamburg Wheel Tracking test and the potential to be alternative test in measuring rutting resistance.” Constr. Build. Mater. 146 (Aug): 175–182. https://doi.org/10.1016/j.conbuildmat.2017.04.080.
Chen, J., B. Yao, C. Li, and G. Shi. 2013. “An improved Hummers method for eco-friendly synthesis of graphene oxide.” Carbon N. Y. 64 (Nov): 225–229. https://doi.org/10.1016/j.carbon.2013.07.055.
Chen, J.-S., M.-C. Liao, and M.-S. Shiah. 2002. “Asphalt modified by styrene-butadiene-styrene triblock copolymer: Morphology and model.” J. Mater. Civ. Eng. 14 (3): 224–229. https://doi.org/10.1061/(ASCE)0899-1561(2002)14:3(224).
Chen, S., D. Ge, D. Jin, X. Zhou, C. Liu, S. Lv, and Z. You. 2020. “Investigation of hot mixture asphalt with high ground tire rubber content.” J. Cleaner Prod. 277 (Dec): 124037. https://doi.org/10.1016/j.jclepro.2020.124037.
Fakhri, M., E. H. Kharrazi, and M. R. M. Aliha. 2018. “Mixed mode tensile–In plane shear fracture energy determination for hot mix asphalt mixtures under intermediate temperature conditions.” Eng. Fract. Mech. 192 (Apr): 98–113. https://doi.org/10.1016/j.engfracmech.2018.02.007.
Fakhri, M., and A. R. Mottahed. 2021. “Improving moisture and fracture resistance of warm mix asphalt containing RAP and nanoclay additive.” Constr. Build. Mater. 272 (Feb): 121900. https://doi.org/10.1016/j.conbuildmat.2020.121900.
Fakhri, M., and E. Shahryari. 2021. “The effects of nano zinc oxide (ZnO) and nano reduced graphene oxide (RGO) on moisture susceptibility property of stone mastic asphalt (SMA).” Case Stud Constr Mater. 15 (Dec): e00655. https://doi.org/10.1016/j.cscm.2021.e00655.
Fakhri, M., E. Shahryari, and T. Ahmadi. 2022. “Investigate the use of recycled polyvinyl chloride (PVC) particles in improving the mechanical properties of stone mastic asphalt (SMA).” Constr. Build. Mater. 326 (Apr): 126780. https://doi.org/10.1016/j.conbuildmat.2022.126780.
Fakhri, M., S. A. Siyadati, and M. R. M. Aliha. 2020. “Impact of freeze–thaw cycles on low temperature mixed mode I/II cracking properties of water saturated hot mix asphalt: An experimental study.” Constr. Build. Mater. 261 (Nov): 119939. https://doi.org/10.1016/j.conbuildmat.2020.119939.
Falchetto, A. C., K. H. Moon, D. Wang, C. Riccardi, and M. P. Wistuba. 2018. “Comparison of low-temperature fracture and strength properties of asphalt mixture obtained from IDT and SCB under different testing configurations.” Road Mater. Pavement Des. 19 (3): 591–604. https://doi.org/10.1080/14680629.2018.1418722.
Guerrero-Contreras, J., and F. Caballero-Briones. 2015. “Graphene oxide powders with different oxidation degree, prepared by synthesis variations of the Hummers method.” Mater. Chem. Phys. 153 (Mar): 209–220. https://doi.org/10.1016/j.matchemphys.2015.01.005.
Guo, Q., H. Wang, Y. Gao, Y. Jiao, F. Liu, and Z. Dong. 2020. “Investigation of the low-temperature properties and cracking resistance of fiber-reinforced asphalt concrete using the DIC technique.” Eng. Fract. Mech. 229 (Apr): 106951. https://doi.org/10.1016/j.engfracmech.2020.106951.
Hafeez, M., N. Ahmad, M. A. Kamal, J. Rafi, S. B. A. Zaidi, and M. A. Nasir. 2019. “Experimental investigation into the structural and functional performance of graphene nano-platelet (GNP)-doped asphalt.” Appl. Sci. 9 (4): 686. https://doi.org/10.3390/app9040686.
Huang, W., and N. Tang. 2015. “Characterizing SBS modified asphalt with sulfur using multiple stress creep recovery test.” Constr. Build. Mater. 93 (Sep): 514–521. https://doi.org/10.1016/j.conbuildmat.2015.06.041.
Jyothirmai, B., M. H. Kiranmai, and K. Vagdevi. 2020. “Graphene reinforces asphalt–Doubles durability of road.” In AIP Conf. Proc., 30085. Melville, NY: AIP Publishing LLC.
Ksaibati, K., and E. Hunter. 2002. Evaluating moisture susceptibility of asphalt mixes. Laramie, WY: Mountain Plains Consortium, Univ. of Wyoming.
Lim, I. L., I. W. Johnston, and S. K. Choi. 1993. “Stress intensity factors for semi-circular specimens under three-point bending.” Eng. Fract. Mech. 44 (3): 363–382. https://doi.org/10.1016/0013-7944(93)90030-V.
Liu, K., K. Zhang, and X. Shi. 2018. “Performance evaluation and modification mechanism analysis of asphalt binders modified by graphene oxide.” Constr. Build. Mater. 163 (Feb): 880–889. https://doi.org/10.1016/j.conbuildmat.2017.12.171.
Liu, K., J. Zhu, K. Zhang, J. Wu, J. Yin, and X. Shi. 2019. “Effects of mixing sequence on mechanical properties of graphene oxide and warm mix additive composite modified asphalt binder.” Constr. Build. Mater. 217 (Aug): 301–309. https://doi.org/10.1016/j.conbuildmat.2019.05.073.
Lv, Q., W. Huang, H. Sadek, F. Xiao, and C. Yan. 2019. “Investigation of the rutting performance of various modified asphalt mixtures using the Hamburg wheel-tracking device test and multiple stress creep recovery test.” Constr. Build. Mater. 206 (May): 62–70. https://doi.org/10.1016/j.conbuildmat.2019.02.015.
Mamun, A. A., and M. Arifuzzaman. 2018. “Nano-scale moisture damage evaluation of carbon nanotube-modified asphalt.” Constr. Build. Mater. 193 (Dec): 268–275. https://doi.org/10.1016/j.conbuildmat.2018.10.155.
Mansourian, A., A. Razmi, and M. Razavi. 2016. “Evaluation of fracture resistance of warm mix asphalt containing jute fibers.” Constr. Build. Mater. 117 (Aug): 37–46. https://doi.org/10.1016/j.conbuildmat.2016.04.128.
Moreno-Navarro, F., M. Sol-Sánchez, F. Gámiz, and M. C. Rubio-Gámez. 2018. “Mechanical and thermal properties of graphene modified asphalt binders.” Constr. Build. Mater. 180 (Aug): 265–274. https://doi.org/10.1016/j.conbuildmat.2018.05.259.
Mukhtar, A., X. Luo, C. Lü, J. Wang, Z. Huang, A. M. Adnan, X. Luo, C. Lü, J. Wang, and Z. Huang. 2020. “Improving mechanics behavior of hot mix asphalt using graphene-oxide.” Constr. Build. Mater. 254 (Sep): 119261. https://doi.org/10.1016/j.conbuildmat.2020.119261.
Najjar, S., A. M. Moghaddam, A. Sahaf, M. R. Yazdani, and A. Delarami. 2019. “Evaluation of the mixed mode (I/II) fracture toughness of cement emulsified asphalt mortar (CRTS-II) using mixture design of experiments.” Constr. Build. Mater. 225 (Nov): 812–828. https://doi.org/10.1016/j.conbuildmat.2019.07.243.
Pirmohammad, S., Y. Majd-Shokorlou, and B. Amani. 2020a. “Experimental investigation of fracture properties of asphalt mixtures modified with Nano Fe2O3 and carbon nanotubes.” Road Mater. Pavement Des. 21 (8): 2321–2343. https://doi.org/10.1080/14680629.2019.1608289.
Pirmohammad, S., Y. M. Shokorlou, and B. Amani. 2020b. “Corrigendum to ‘Laboratory investigations on fracture resistance of asphalt concretes reinforced with carbon and kenaf fibers at 15°C’ [Eng. Fract. Mech. 226 (2020) 106875].” Eng. Fract. Mech. 230 (May): 106977. https://doi.org/10.1016/j.engfracmech.2020.106977.
Pirmohammad, S., Y. M. Shokorlou, and B. Amani. 2020c. “Laboratory investigations on fracture toughness of asphalt concretes reinforced with carbon and kenaf fibers.” Eng. Fract. Mech. 226 (Mar): 106875. https://doi.org/10.1016/j.engfracmech.2020.106875.
Razavi, S., and A. Kavussi. 2020. “The role of nanomaterials in reducing moisture damage of asphalt mixes.” Constr. Build. Mater. 239 (Apr): 117827. https://doi.org/10.1016/j.conbuildmat.2019.117827.
Razavi, S. M. J., M. R. M. Aliha, and F. Berto. 2018. “Application of an average strain energy density criterion to obtain the mixed mode fracture load of granite rock tested with the cracked asymmetric four-point bend specimens.” Theor. Appl. Fract. Mech. 97 (Oct): 419–425. https://doi.org/10.1016/j.tafmec.2017.07.004.
Razmi, A., and M. M. Mirsayar. 2018. “Fracture resistance of asphalt concrete modified with crumb rubber at low temperatures.” Int. J. Pavement Res. Technol. 11 (3): 265–273. https://doi.org/10.1016/j.ijprt.2017.10.003.
Shafabakhsh, G., M. Sadeghnejad, and R. Ebrahimnia. 2021. “Fracture resistance of asphalt mixtures under mixed-mode I/II loading at low-temperature: Without and with nano SiO2.” Constr. Build. Mater. 266 (Jan): 120954. https://doi.org/10.1016/j.conbuildmat.2020.120954.
Shahryari, E., and M. Fakhri. 2022. “Investigation of mechanical properties of stone mastic asphalt mix (SMA) modified with Nano Reduced Graphene Oxide.” J. Transp. Infrastruct. Eng. 8 (2): 1–20. https://doi.org/10.22075/JTIE.2022.26070.1586.
Singh, B. B., F. Mohanty, S. S. Das, and S. K. Swain. 2020. “Graphene sandwiched crumb rubber dispersed hot mix asphalt.” J. Traffic Transp. Eng. (English Ed) 7 (5): 652–667. https://doi.org/doi.org/10.1016/j.jtte.2019.02.003.
Sivashankari, P. R., and M. Prabaharan. 2017. “Chitosan/carbon-based nanomaterials as scaffolds for tissue engineering.” In Biopolymer-based composites, 381–397. Amsterdam, Netherlands: Elsevier. https://doi.org/10.1016/B978-0-08-101914-6.00012-0.
Tang, Z., X. Wu, B. Guo, L. Zhang, and D. Jia. 2012. “Preparation of butadiene–styrene–vinyl pyridine rubber–graphene oxide hybrids through co-coagulation process and in situ interface tailoring.” J. Mater. Chem. 22 (15): 7492–7501. https://doi.org/10.1039/c2jm00084a.
Tarcan, R., O. Todor-Boer, I. Petrovai, C. Leordean, S. Astilean, and I. Botiz. 2020. “Reduced graphene oxide today.” J. Mater. Chem. C 8 (4): 1198–1224. https://doi.org/10.1039/C9TC04916A.
Walubita, L. F., A. N. M. Faruk, S. I. Lee, D. Nguyen, R. Hassan, and T. Scullion. 2014. HMA shear resistance, permanent deformation, and rutting tests for Texas mixes: Final year-2 report. Dallas: Texas A&M Transportation Institute.
Wang, J., H. Jia, Y. Tang, D. Ji, Y. Sun, X. Gong, and L. Ding. 2013. “Enhancements of the mechanical properties and thermal conductivity of carboxylated acrylonitrile butadiene rubber with the addition of graphene oxide.” J. Mater. Sci. 48 (4): 1571–1577. https://doi.org/10.1007/s10853-012-6913-1.
Wang, R., M. Yue, Y. Xiong, and J. Yue. 2021. “Experimental study on mechanism, aging, rheology and fatigue performance of carbon nanomaterial/SBS-modified asphalt binders.” Constr. Build. Mater. 268 (Jan): 121189. https://doi.org/10.1016/j.conbuildmat.2020.121189.
Wang, T., F. Xiao, S. Amirkhanian, W. Huang, and M. Zheng. 2017. “A review on low temperature performances of rubberized asphalt materials.” Constr. Build. Mater. 145 (Aug): 483–505. https://doi.org/10.1016/j.conbuildmat.2017.04.031.
Wu, S., and O. Tahri. 2019. “State-of-art carbon and graphene family nanomaterials for asphalt modification.” Road Mater. Pavement Des. 22 (4): 735–756. https://doi.org/10.1080/14680629.2019.1642946.
Xu, G., and H. Wang. 2017. “Molecular dynamics study of oxidative aging effect on asphalt binder properties.” Fuel 188 (Jan): 1–10. https://doi.org/10.1016/j.fuel.2016.10.021.
Yalghouzaghaj, M. N., A. Sarkar, G. H. Hamedi, and P. Hayati. 2021. “Application of the surface free energy method on the mechanism of low-temperature cracking of asphalt mixtures.” Constr. Build. Mater. 268 (Jan): 121194. https://doi.org/10.1016/j.conbuildmat.2020.121194.
Zaaba, N. I., K. L. Foo, U. Hashim, S. J. Tan, W.-W. Liu, and C. H. Voon. 2017. “Synthesis of graphene oxide using modified hummers method: Solvent influence.” Procedia Eng. 184 (Jan): 469–477. https://doi.org/10.1016/j.proeng.2017.04.118.
Zeng, Q., Y. Liu, Q. Liu, P. Liu, Y. He, and Y. Zeng. 2020. “Preparation and modification mechanism analysis of graphene oxide modified asphalts.” Constr. Build. Mater. 238 (Mar): 117706. https://doi.org/10.1016/j.conbuildmat.2019.117706.
Zhao, W., X. Xie, G. Li, J. Geng, M. Bao, and M. Wang. 2020. “Research on the influence of nanocarbon/copolymer SBS/rubber powder composite modification on the properties of asphalt and mixtures.” Adv. Mater. Sci. Eng. 2020 (Dec): 8820202. https://doi.org/doi.org/10.1155/2020/8820202.
Zhou, F., S. Im, S. Hu, D. Newcomb, and T. Scullion. 2017. “Selection and preliminary evaluation of laboratory cracking tests for routine asphalt mix designs.” Supplement, Road Mater. Pavement Des. 18 (S1): 62–86. https://doi.org/10.1080/14680629.2016.1266741.
Zhu, J., K. Zhang, K. Liu, and X. Shi. 2019. “Performance of hot and warm mix asphalt mixtures enhanced by nano-sized graphene oxide.” Constr. Build. Mater. 217 (Aug): 273–282. https://doi.org/10.1016/j.conbuildmat.2019.05.054.
Zhu, J., K. Zhang, K. Liu, and X. Shi. 2020. “Adhesion characteristics of graphene oxide modified asphalt unveiled by surface free energy and AFM-scanned micro-morphology.” Constr. Build. Mater. 244 (May): 118404. https://doi.org/10.1016/j.conbuildmat.2020.118404.

Information & Authors

Information

Published In

Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 35Issue 3March 2023

History

Received: Apr 22, 2022
Accepted: Jul 6, 2022
Published online: Dec 28, 2022
Published in print: Mar 1, 2023
Discussion open until: May 28, 2023

Permissions

Request permissions for this article.

Authors

Affiliations

Assistant Professor, Faculty of Civil Engineering, Semnan Univ., Semnan 3513119111, Iran (corresponding author). ORCID: https://orcid.org/0000-0002-9359-5095. Email: [email protected]
Master of Science, Faculty of Civil Engineering, K. N. Toosi Univ. of Technology, Tehran 3513119111, Iran. ORCID: https://orcid.org/0000-0001-5513-5453. Email: [email protected]
Amir Mohammad Hamedipour [email protected]
Master of Science, Faculty of Civil Engineering, Semnan Univ., Semnan 3513119111, Iran. Email: [email protected]
Gholamali Shafabakhsh [email protected]
Professor, Faculty of Civil Engineering, Semnan Univ., Semnan 3513119111, Iran. Email: [email protected]

Metrics & Citations

Metrics

Citations

Download citation

If you have the appropriate software installed, you can download article citation data to the citation manager of your choice. Simply select your manager software from the list below and click Download.

View Options

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Get Access

Access content

Please select your options to get access

Log in/Register Log in via your institution (Shibboleth)
ASCE Members: Please log in to see member pricing

Purchase

Save for later Information on ASCE Library Cards
ASCE Library Cards let you download journal articles, proceedings papers, and available book chapters across the entire ASCE Library platform. ASCE Library Cards remain active for 24 months or until all downloads are used. Note: This content will be debited as one download at time of checkout.

Terms of Use: ASCE Library Cards are for individual, personal use only. Reselling, republishing, or forwarding the materials to libraries or reading rooms is prohibited.
ASCE Library Card (5 downloads)
$105.00
Add to cart
ASCE Library Card (20 downloads)
$280.00
Add to cart
Buy Single Article
$35.00
Add to cart

Media

Figures

Other

Tables

Share

Share

Copy the content Link

Share with email

Email a colleague

Share