Technical Papers
Jul 14, 2021

Aging Property of Oil Recycled Asphalt Binders with Reclaimed Asphalt Materials

Publication: Journal of Materials in Civil Engineering
Volume 33, Issue 9

Abstract

The reuse of high content of reclaimed asphalt pavement and reclaimed asphalt shingles in hot mixtures by adding recycling oils has attracted wide attention and interest in the paving industry. However, the aging property and the durability of oil recycled asphalt binders with reclaimed asphalt materials are not well understood. This study prepared 12 oil recycled asphalt binders with base binder, extracted binders from reclaimed asphalt pavement and reclaimed asphalt shingles, and three types of oils, including two bio-oils and one re-refined engine oil bottom oil. Multiple stress creep recovery and oscillation tests were performed to evaluate the rheological change with aging, and Fourier-transform infrared spectroscopy was used to track the chemical evolution. Aging performance of these blends was evaluated using the aging indexes. Results showed that the recovery and nonrecoverable creep compliance were highly related. The aging indexes of nonrecoverable creep compliance at 3.2 kPa and complex modulus indicated that adding oils may impair the durability of asphalt binders with reclaimed asphalt materials. However, the aging index of carbonyl suggested that the oils do not have much effect on the chemical reaction (oxidation). The correlating analysis indicated that rheological and chemical change had a good correlation relationship, but also showed material dependency.

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Data Availability Statement

All data generated or analyzed during the study are included in the published paper.

Acknowledgments

The authors are grateful for the financial support by the National Key R&D Program of China (Grant No. 2018YFE0103800), the National Natural Science Foundation of China (Grant No. 51908056), and the Innovative Talent Promotion Program-Scientific and Technological Innovation Team in Shaanxi Province (No. 2017KCT-13).

References

AASHTO. 2016. Standard practice for accelerated aging of asphalt binder using a pressurized aging vessel (PAV). AASHTO R 28. Washington, DC: AASHTO.
AASHTO. 2017a. Standard method of test for effect of heat and air on a moving film of asphalt binder (rolling thin-film oven test). AASHTO T 240. Washington, DC: AASHTO.
AASHTO. 2017b. Standard practice for design design considerations when using reclaimed asphalt shingles (RAS) in asphalt mixtures. AASHTO PP 78. Washington, DC: AASHTO.
AASHTO. 2019. Standard method of test for multiple stress creep recovery (MSCR) test of asphalt binder using a dynamic shear rheometer (DSR). AASHTO T 350. Washington, DC: AASHTO.
AASHTO. 2020. Standard method of test for determining the rheological properties of asphalt binder using a dynamic shear rheometer (DSR). AASHTO T 315. Washington, DC: AASHTO.
Anderson, M., P. Kriz, G. King, and J. P. Planche. 2011. “Evaluation of the relationship between asphalt binder properties and non-load related cracking.” J. Assoc. Asphalt Paving Technol. 80 (4): 615–664. https://doi.org/10.1016/j.apm.2010.07.024.
AOCS (American Oil Chemists’ Society). 2017. Smoke, flash, and fire points, Cleveland open cup method. AOCS Cc 9a-48. Urbana, IL: AOCS.
ASTM. 2015. Standard test method for viscosity determination of asphalt at elevated temperatures using a rotational viscometer. ASTM D4402. West Conshohocken, PA: ASTM.
ASTM. 2018. Standard test method for determination of the acidity as free fatty acids/acid number in the presence of ammonium or triethanolamine soaps. ASTM D5562-95. West Conshohocken, PA: ASTM.
ASTM. 2020. Standard test method for density of liquid coatings, inks, and related products. ASTM D1475-13. West Conshohocken, PA: ASTM.
Baek, S.-H., J.-P. Hong, S. U. Kim, J.-S. Choi, and K.-W. Kim. 2011. “Evaluation of fracture toughness of semirigid asphalt concretes at low temperatures.” Transp. Res. Rec. 2210 (1): 30–36. https://doi.org/10.3141/2210-04.
Behnood, A. 2019. “Application of rejuvenators to improve the rheological and mechanical properties of asphalt binders and mixtures: A review.” J. Cleaner Prod. 231 (Sep): 171–182. https://doi.org/10.1016/j.jclepro.2019.05.209.
Behnood, A., and J. Olek. 2017. “Rheological properties of asphalt binders modified with styrene-butadiene-styrene (SBS), ground tire rubber (GTR), or polyphosphoric acid (PPA)” Constr. Build. Mater. 151 (Oct): 464–478. https://doi.org/10.1016/j.conbuildmat.2017.06.115.
Bennert, T., C. Ericson, D. Pezeshki, and R. Corun. 2016. “Laboratory performance of re-refined engine oil bottoms (REOB) modified asphalt.” Transp. Res. Rec. 2574 (1): 1–16. https://doi.org/10.3141/2574-01.
Cai, J., C. Song, B. Zhou, Y. Tian, R. Li, J. Zhang, and J. Pei. 2019. “Investigation on high-viscosity asphalt binder for permeable asphalt concrete with waste materials.” J. Cleaner Prod. 228 (Aug): 40–51. https://doi.org/10.1016/j.jclepro.2019.04.010.
Cavalli, M. C., M. N. Partl, and L. D. Poulikakos. 2017. “Measuring the binder film residues on black rock in mixtures with high amounts of reclaimed asphalt.” J. Cleaner Prod. 149 (Apr): 665–672. https://doi.org/10.1016/j.jclepro.2017.02.055.
Cavalli, M. C., M. Zaumanis, E. Mazza, M. N. Partl, and L. D. Poulikakos. 2018. “Effect of ageing on the mechanical and chemical properties of binder from RAP treated with bio-based rejuvenators.” Composites Part B 141 (May): 174–181. https://doi.org/10.1016/j.compositesb.2017.12.060.
Cong, P., W. Luo, P. Xu, and H. Zhao. 2015. “Investigation on recycling of SBS modified asphalt binders containing fresh asphalt and rejuvenating agents.” Constr. Build. Mater. 91 (Aug): 225–231. https://doi.org/10.1016/j.conbuildmat.2015.05.041.
D’Angelo, J., K. Grzybowski, and S. Lewis. 2012. “Asphalt binder modification with re-refined heavy vacuum distillation oil (RHVDO).” In Proc., 57th Conf. of the Canadian Technical Asphalt Association. Vancouver, BC, Canada: Canadian Technical Asphalt Association.
D’Angelo, J., K. Grzybowski, S. Lewis, and R. Walker. 2013. “Evaluation of the performance properties of asphalt mixes produced with re-refined heavy vacuum distillate bottoms.” In Proc., 58th Conf. of the Canadian Technical Asphalt Association. Vancouver, BC, Canada: Canadian Technical Asphalt Association.
Fini, E. H., I. L. Al-Qadi, Z. You, B. Zada, and J. Mills-Beale. 2012. “Partial replacement of asphalt binder with bio-binder: characterisation and modification.” Int. J. Pavement Eng. 13 (6): 515–522. https://doi.org/10.1080/10298436.2011.596937.
Guo, X., S. Wang, W. Qi, Z. Guo, and Z. Luo. 2011. “Properties of bio-oil from fast pyrolysis of rice husk.” Chin. J. Chem. Eng. 19 (1): 116–121. https://doi.org/10.1016/S1004-9541(09)60186-5.
Hesp, S. A. M., and H. F. Shurvell. 2010. “X-ray fluorescence detection of waste engine oil residue in asphalt and its effect on cracking in service.” Int. J. Pavement Eng. 11 (6): 541–553. https://doi.org/10.1080/10298436.2010.488729.
Huang, W., and N. Tang. 2015. “Characterizing SBS modified asphalt with sulfur using multiple stress creep recovery test.” Constr. Build. Mater. 93 (Sep): 514–521. https://doi.org/10.1016/j.conbuildmat.2015.06.041.
Johnson, K.-A. N., and S. A. M. Hesp. 2014. “Effect of waste engine oil residue on quality and durability of SHRP materials reference library binders.” Transp. Res. Rec. 2444 (1): 102–109. https://doi.org/10.3141/2444-12.
Lesueur, D. 2009. “The colloidal structure of bitumen: Consequences on the rheology and on the mechanisms of bitumen modification.” Adv. Colloid Interface Sci. 145 (1–2): 42–82. https://doi.org/10.1016/j.cis.2008.08.011.
Li, H., G. Liu, B. Dong, G. Zhao, P. Guo, J. Huang, and Y. Sheng. 2019. “Research on the development and regeneration performance of asphalt rejuvenator based on the mixed waste engine oil and waste cooking oil.” Int. J. Pavement Res. Technol. 12 (3): 336–346. https://doi.org/10.1007/s42947-019-0040-1.
Li, X., M. O. Marasteanu, R. C. Williams, and T. R. Clyne. 2008. “Effect of reclaimed asphalt pavement (proportion and type) and binder grade on asphalt mixtures.” Transp. Res. Rec. 2051 (Jan): 90–97. https://doi.org/10.3141/2051-11.
Liu, S., A. Peng, J. Wu, and S. B. Zhou. 2018. “Waste engine oil influences on chemical and rheological properties of different asphalt binders.” Constr. Build. Mater. 191 (Dec): 1210–1220. https://doi.org/10.1016/j.conbuildmat.2018.10.126.
Lu, X., and U. Isacsson. 2002. “Effect of aging on bitumen chemistry and rheology.” Constr. Build. Mater. 16 (1): 15–22. https://doi.org/10.1016/S0950-0618(01)00033-2.
Ma, Y., W. Hu, P. A. Polaczyk, B. Han, R. Xiao, M. Zhang, and B. Huang. 2020. “Rheological and aging characteristics of the recycled asphalt binders with different rejuvenator incorporation methods.” J. Cleaner Prod. 262 (Jul): 121249. https://doi.org/10.1016/j.jclepro.2020.121249.
Mensching, D., A. Andriescu, C. DeCarlo, X. Li, and J. Youtcheff. 2017. “Effect of extended aging on asphalt materials containing re-refined engine oil bottoms.” Transp. Res. Rec. 2632 (1): 60–69. https://doi.org/10.3141/2632-07.
Nazzal, M. D., W. Mogawer, S. Kaya, and T. Bennert. 2014. “Multiscale evaluation of the composite asphalt binder in high–reclaimed asphalt pavement mixtures.” J. Mater. Civ. Eng. 26 (7): 04014019. https://doi.org/10.1061/(ASCE)MT.1943-5533.0000825.
Petersen, J. C., and R. Glaser. 2011. “Asphalt oxidation mechanisms and the role of oxidation products on age hardening revisited.” Road Mater Pavement Des. 12 (4): 795–819. https://doi.org/10.1080/14680629.2011.9713895.
Qin, Q., J. F. Schabron, R. B. Boysen, and M. J. Farrar. 2014. “Field aging effect on chemistry and rheology of asphalt binders and rheological predictions for field aging.” Fuel 121 (Apr): 86–94. https://doi.org/10.1016/j.fuel.2013.12.040.
Rinaldini, E., P. Schuetz, M. N. Partl, G. Tebaldi, and L. D. Poulikakos. 2014. “Investigating the blending of reclaimed asphalt with virgin materials using rheology, electron microscopy and computer tomography.” Composites Part B 67 (Dec): 579–587. https://doi.org/10.1016/j.compositesb.2014.07.025.
Shen, J., S. Amirkhanian, and B. Tang. 2007. “Effects of rejuvenator on performance based properties of rejuvenated asphalt binder and mixtures.” Constr. Build. Mater. 21 (May): 958–964. https://doi.org/10.1016/j.conbuildmat.2006.03.006.
Sun, D., T. Lu, F. Xiao, X. Zhu, and G. Sun. 2017. “Formulation and aging resistance of modified bio-asphalt containing high percentage of waste cooking oil residues.” J. Cleaner Prod. 161 (Sep): 1203–1214. https://doi.org/10.1016/j.jclepro.2017.06.155.
Zhang, L., H. Bahia, and Y.-Q. Tan. 2015. “Effect of bio-based and refined waste oil modifiers on low temperature performance of asphalt binders.” Constr. Build. Mater. 86 (Jul): 95–100. https://doi.org/10.1016/j.conbuildmat.2015.03.106.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 33Issue 9September 2021

History

Received: May 14, 2020
Accepted: Sep 9, 2020
Published online: Jul 14, 2021
Published in print: Sep 1, 2021
Discussion open until: Dec 14, 2021

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Authors

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Jing Xu, Ph.D. [email protected]
School of Highway, Chang’an Univ., Xi’an 710064, China. Email: [email protected]
Hui Chen, Ph.D. [email protected]
Dept. of Civil and Environmental Engineering, Univ. of Wisconsin–Madison, Madison, WI 53706. Email: [email protected]
Yong Wen, Ph.D. [email protected]
Lecturer, School of Highway, Chang’an Univ., Xi’an 710064, China. Email: [email protected]
Bin Xue, Ph.D. [email protected]
School of Highway, Chang’an Univ., Xi’an 710064, China. Email: [email protected]
Professor, School of Highway, Chang’an Univ., Xi’an 710064, China. Email: lirui.chd.edu.cn
Jianzhong Pei [email protected]
Professor, School of Highway, Chang’an Univ., Xi’an 710064, China (corresponding author). Email: [email protected]

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Cited by

  • Performance of Nano- Composite Modified Asphalt, Journal of Materials in Civil Engineering, 10.1061/JMCEE7.MTENG-15897, 35, 11, (2023).
  • Chemical and rheological properties evaluation of a novel synchronous rejuvenated aged SBS modified asphalt, Journal of Cleaner Production, 10.1016/j.jclepro.2022.135213, 381, (135213), (2022).

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