Technical Papers
Dec 17, 2019

Combination Effect of Limestone Filler and Slag on Delayed Ettringite Formation in Heat-Cured Mortar

Publication: Journal of Materials in Civil Engineering
Volume 32, Issue 3

Abstract

The present paper analyzes the combination effect of slag and limestone filler on the expansion caused by delayed ettringite formation (DEF). Tests were carried out on heat-cured ternary cement mortars with various replacement levels of cement by both limestone filler and slag (15%, 25%, and 45%). The expansion of heat-cured cement mortars was evaluated and verified by measuring their length change, dynamic elastic modulus, and compressive strength over more than 750 days. The addition of limestone filler and slag to portland cement was found to be beneficial to reducing the expansion caused by DEF. It was found that the use of 10% and 20% slag ternary cements with 5% limestone filler delayed the beginning of the expansion and caused a decrease in the long-term expansion. Meanwhile, the use of 40% slag with 5% limestone filler suppressed the expansion caused by DEF.

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References

Adu-Amankwah, S., M. Zajac, C. Stabler, B. Lothenbach, and L. Black. 2017. “Influence of limestone on the hydration of ternary slag cements.” Cem. Concr. Res. 100 (Oct): 96–109. https://doi.org/10.1016/j.cemconres.2017.05.013.
Amine, Y., N. Leklou, and O. Amiri. 2017. “Effects of ternary cements with limestone filler on DEF in concrete.” ACI Mater. 320: 20.1–20.14.
Arora, A., G. Sant, and N. Neithalath. 2016. “Ternary blends containing slag and interground/blended limestone: Hydration, strength, and pore structure.” Constr. Build. Mater. 102 (1): 113–124. https://doi.org/10.1016/j.conbuildmat.2015.10.179.
Atahan, H. N., and D. Dikme. 2011. “Use of mineral admixtures for enhanced resistance against sulfate attack.” Constr. Build. Mater. 25 (8): 3450–3457. https://doi.org/10.1016/j.conbuildmat.2011.03.036.
Ballim, Y., and P. C. Graham. 2009. “The effects of supplementary cementing materials in modifying the heat of hydration of concrete.” Mater. Struct. 42 (6): 803–811. https://doi.org/10.1617/s11527-008-9425-3.
Beushausen, H., M. Alexander, and Y. Ballim. 2012. “Early-age properties, strength development and heat of hydration of concrete containing various South African slags at different replacement ratios.” Constr. Build. Mater. 29 (Apr): 533–540. https://doi.org/10.1016/j.conbuildmat.2011.06.018.
Deboucha, W., N. Leklou, and A. Khelidj. 2018. “Blast furnace slag addition effects on delayed ettringite formation in heat-cured mortars.” KSCE J. Civ. Eng. 22 (9): 3484–3490. https://doi.org/10.1007/s12205-017-0642-6.
Deboucha, W., N. Leklou, A. Khelidj, and M. N. Oudjit. 2017. “Hydration development of mineral additives blended cement using thermogravimetric analysis (TGA): Methodology of calculating the degree of hydration.” Constr. Build. Mater. 146 (Aug): 687–701. https://doi.org/10.1016/j.conbuildmat.2017.04.132.
Deboucha, W., M. N. Oudjit, A. Bouzid, and L. Belagraa. 2015. “Effect of incorporating blast furnace slag and natural pozzolana on compressive strength and capillary water absorption of concrete.” Procedia Eng. 108: 254–261. https://doi:10.1016/j.proeng.2015.06.145.
Grattan-Bellew, P. E. 2000. “A discussion of the paper ‘Delayed ettringite formation in heat- cured portland cement mortars’ by R. Yang, C. D. Lawrence, C. J. Lynsdale, J. H. Sharp.” Cem. Concr. Res. 30 (4): 665–666. https://doi.org/10.1016/S0008-8846(99)00235-5.
Leklou, N., V. Nguyen, and P. Mounanga. 2016. “The effect of the partial cement substitution with fly ash on delayed ettringite formation in heat-cured mortars.” KSCE J. Civ. Eng. 21 (4): 1359–1366. https://doi.org/10.1007/s12205-016-0778-9.
Mounanga, P., M. Irfan, A. Khokhar, R. El hachem, and A. Loukili. 2011. “Improvement of the early-age reactivity of fly ash and blast furnace slag cementitious systems using limestone filler.” Mater. Struct. 44 (2): 437–453. https://doi.org/10.1617/s11527-010-9637-1.
NF. 1994. Méthodes d’essais des ciments: Détermination du retrait et du gonflement. NF P15-433. Paris: Association Française de Normalisation.
NF. 2000. Cement. 1: Composition, specifications and conformity criteria for common cements. NF EN 197-1. Paris: Association Française de Normalisation.
NF. 2006. Methods of testing cement. 1: Determination of strength. NF EN196-1. Paris: Association Française de Normalisation.
Nguyen, V. H. 2012. “Effets d’additions minérales et organiques sur l’apparition de la RSI : étude paramétrique et développement et optimisation de méthodes accélérées.” Thèse de Doctorat, Institut de Recherche en Génie Civil et Mécanique, Univ. de Nantes.
Nguyen, V. H., N. Leklou, J. E. Aubert, and P. Mounanga. 2013. “The effect of natural pozzolan on delayed ettringite formation of the heat-cured mortars.” Constr. Build. Mater. 48 (Nov): 479–484. https://doi.org/10.1016/j.conbuildmat.2013.07.016.
Pavoine, A., X. Brunetaud, and L. Divet. 2012. “The impact of cement parameters on delayed ettringite formation” Cem. Concr. Res. 34 (4): 521–528. https://doi.org/10.1016/j.cemconcomp.2011.11.012.
Ramlochan, T., M. D. A. Thomas, and R. D. Hooton. 2004. “The effect of pozzolans and slag on the expansion of mortars cured at elevated temperature. Part II: Microstructural and microchemical investigations.” Cem. Concr. Res. 34 (8): 1341–1356. https://doi.org/10.1016/j.cemconres.2003.12.026.
Ramlochan, T., P. Zacarias, M. D. A. Thomas, and R. D. Hooton. 2003. “The effect of pozzolans and slag on the expansion of mortars cured at elevated temperature. Part I: Expansive behaviour.” Cem. Concr. Res. 33 (6): 807–814. https://doi.org/10.1016/S0008-8846(02)01066-9.
Schindler, A. K., and K. J. Folliard. 2005. “Heat of hydration models for cementitious materials.” ACI Mater. J. 102 (1): 24–33. https://doi.org/10.14359/14246.
Yang, R., C. D. Lawrence, and J. H. Sharp. 1999. “Effect of type of aggregate on delayed ettringite formation.” Adv. Cem. Res. 11 (3): 119–132. https://doi.org/10.1680/adcr.1999.11.3.119.
Zajac, M., A. Rossberg, G. Le Saout, and B. Lothenbach. 2014. “Influence of limestone and anhydrite on the hydration of portland cements.” Cem. Concr. Compos. 46 (Feb): 99–108. https://doi.org/10.1016/j.cemconcomp.2013.11.007.
Zhang, Z., J. Olek, and S. Diamond. 2002. “Studies on delayed ettringite formation in early age, heat-cured mortars. I: Expansion measurements, changes in dynamic modulus of elasticity and weight gains.” Cem. Concr. Res. 32 (11): 1729–1736. https://doi.org/10.1016/S0008-8846(02)00862-1.

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Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 32Issue 3March 2020

History

Received: Oct 28, 2018
Accepted: Jul 11, 2019
Published online: Dec 17, 2019
Published in print: Mar 1, 2020
Discussion open until: May 17, 2020

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Authors

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Walid Deboucha, Ph.D. [email protected]
Université Grenoble Alpes, Université Savoie Mont Blanc, CNRS, LOCIE, Campus Scientifique Savoie Technolac, Le Bourget du Lac Cedex 73376, Chambéry, France; Research Institute in Civil Engineering and Mechanics, LUNAM Univ., Univ. of Nantes–IUT Saint-Nazaire, GeM, CNRS UMR 6183 Nantes, France (corresponding author). Email: [email protected]
Nordine Leklou
Associate Professor, Research Institute in Civil Engineering and Mechanics, Univ. of Nantes–IUT Saint-Nazaire, LUNAM Univ., GeM, CNRS UMR 6183 Nantes, France.
Abdelhafid Khelidj
Professor, Research Institute in Civil Engineering and Mechanics, LUNAM Univ., Univ. of Nantes–IUT Saint-Nazaire, GeM, CNRS UMR 6183 Nantes, France.
Olivier Plé
Professor, Université Grenoble Alpes, Université Savoie Mont Blanc, CNRS, LOCIE, Campus Scientifique Savoie Technolac, Le Bourget du Lac Cedex 73376, Chambéry, France.
Associate Professor, Faculty of Engineering, Centre for Innovative Construction Technology, Dept. of Civil Engineering, Univ. of Malaya, Kuala Lumpur 50603, Malaysia. ORCID: https://orcid.org/0000-0001-9358-2975

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