Correlation of DSR Results and FTIR’s Carbonyl and Sulfoxide Indexes: Effect of Aging Temperature on Asphalt Rheology
Publication: Journal of Materials in Civil Engineering
Volume 31, Issue 7
Abstract
This paper investigates the effects of different aging temperatures on the performance of asphalt binders through a comprehensive experimental procedure. Two kinds of asphalt binders with the same 70/100 penetration grade were used in this study. The two types of asphalt binders were short-term aged at three different temperatures: 123°C, 143°C, and 163°C. The short-term aged asphalt binders were long-term aged according to the standard pressure aging vessel (PAV) tests protocol. Dynamic shear rheometer (DSR) and Fourier-transform infrared spectroscopy (FTIR) were adopted to quantify the performance of asphalt binders under different aging conditions. The DSR results showed that different critical aging temperatures can be found for the two kinds of asphalt binders. The Superpave performance grading can reflect the viscoelastic property of asphalt binder, whereas penetration grading cannot do so in grading asphalt binder. The FTIR test results showed that the and bonds were good indicators to evaluate the aging effect of different temperatures. The correlation between and occurred for both asphalt binders under different aging conditions.
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Acknowledgments
The US National Science Foundation (NSF), which funded a research grant through the SusChem/Collaborative Research Program (Award No. 1300286), enabled this study to be completed. The authors also acknowledge the funding from the NSF Division of Materials Research (Award No. 1261910). Any opinions, findings, and conclusions expressed in this material are those of the authors and do not necessarily reflect the views of the National Science Foundation. The financial support to Dongdong Ge and Siyu Chen from the China Scholarship Council is gratefully appreciated. The authors also acknowledge the discussion with RILEM TC CMB TG 3 group, including Bernhard Hofko (Vienna University of Technology, Austria), Lily Poulikakos (Swiss Federal Laboratories for Materials Science and Technology, Switzerland), Xiaohu Lu (Sweden), Francisco Barcelo Martinez (Centro de Tecnologia REPSOL, Spain), Huber Liliane (Institut für Materialprüfung, Switzerland), Augusto Cannone Falchetto (TU Braunschweig—ISBS, Institut für Straßenwesen, Germany), Zhanping You (Michigan Technological University, United States), Laurent Porot (Kraton Chemical, The Netherlands), James Grenfell (Nottingham Transportation Engineering Centre, University of Nottingham, United Kingdom), and Jeroen Besamusca (Kuwait Petroleum Research & Technology, the Netherlands). The authors extend their gratitude to Huijun Shao and Xuelian Li for their valuable comments.
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©2019 American Society of Civil Engineers.
History
Received: Mar 26, 2018
Accepted: Jan 31, 2019
Published online: Apr 30, 2019
Published in print: Jul 1, 2019
Discussion open until: Sep 30, 2019
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