Technical Notes
Jan 9, 2018

Prompt Phase Analyses of Ultrahigh-Performance Concrete

Publication: Journal of Materials in Civil Engineering
Volume 30, Issue 3

Abstract

Powder X-ray diffraction is a time-consuming and challenging task, especially for preparation of sensitive phases like ettringite and calcium-silicate-hydrate (C-S-H) phases. Fine-grained ultrahigh-performance concrete (UHPC) with an average grain size <100  μm could be investigated directly without time-consuming milling. As a proof of concept, small UHPC cylinders with plain surfaces were investigated with a newly designed sample holder. The comparison with conventionally prepared powder shows the feasibility of fast qualitative phase analysis using this approach. As a great benefit, a depth-dependent analysis, as well as a comparison of surface layers and core material, was carried out.

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Acknowledgments

The authors thank their colleagues in the BAM workshop for construction of the special sample holder. The research on UHPC was funded by Deutsche Forschungsgemeinschaft (DFG) (Sachbeihilfe ME 1461/11-1).

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Published In

Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 30Issue 3March 2018

History

Received: Mar 8, 2017
Accepted: Aug 15, 2017
Published online: Jan 9, 2018
Published in print: Mar 1, 2018
Discussion open until: Jun 9, 2018

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Authors

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Sebastian Simon [email protected]
Dept. of Building Materials, Bundesanstalt für Materialforschung und -prüfung (BAM), Headquarters, Unter den Eichen 87, 12205 Berlin, Germany (corresponding author). E-mail: [email protected]
Christian Selleng
Dept. of Building Materials, Bundesanstalt für Materialforschung und -prüfung (BAM), Headquarters, Unter den Eichen 87, 12205 Berlin, Germany.
Birgit Meng
Dept. of Building Materials, Bundesanstalt für Materialforschung und -prüfung (BAM), Headquarters, Unter den Eichen 87, 12205 Berlin, Germany.

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