TECHNICAL PAPERS
Apr 12, 2010

Thermoviscoelastic Analysis and Creep Testing of Ambient Temperature Cure Epoxies Used in Adhesive Anchor Applications

Publication: Journal of Materials in Civil Engineering
Volume 22, Issue 10

Abstract

Thermoviscoelastic properties and creep response of two commercial ambient temperature cure epoxy structural adhesives were analyzed and compared. The adhesives were formulated by the same manufacturer and appeared to be chemically similar; however, one system contained accelerators to shorten its cure time. In the laboratory, dynamic mechanical temperature/frequency sweeps were performed on both systems to generate dynamic mechanical and creep compliance master curves using time-temperature superposition principles. Differences were observed in the dynamic mechanical properties of the two adhesive systems as well as in their calculated creep compliance, which have been attributed to differences in their curing agent(s) and accelerator(s). Full-scale creep tests were carried out on anchors installed in concrete slabs and subjected to sustained loads for 82 days. These results were in good agreement with the creep compliance estimated using time-temperature superposition, suggesting that dynamic mechanical testing can be a useful metrology for characterizing trends in creep behavior.

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References

ASTM. (2009). “Standard test method for assignment of the glass transition temperature by dynamic mechanical analysis.” E1640-04, West Conshohocken, Pa.
Behm, D. T., and Gannon, J. (1990). “Epoxies.” Engineered materials handbook, Vol. 3, ASM International, Metals Park, Ohio, 94–102.
Cohen, R. E., and Ramos, A. R. (1979). “Homogeneous and heterogeneous blends of polybutadiene, polyisoprene, and corresponding diblock copolymers.” Macromolecules, 12(1), 131–134.
Cook, R. A., and Konz, R. C. (2001). “Factors influencing bond strength of adhesive anchors.” ACI Struct. J., 98(1), 76–86.
Ferry, J. D. (1980). Viscoelastic properties of polymers, John Wiley and Sons, New York.
Gillham, J. K., and Enns, J. B. (1994). “On the cure and properties of thermosetting polymers using torsional braid analysis.” Trends Polym. Sci., 2(12), 406–418.
Hunston, D. L., Carter, W., and Rushford, J. L. (1980). “Mechanical properties of solid polymers as modeled by a simple epoxy.” Developments in adhesives—2, A. J. Kinloch, ed., Applied Science Publishers Ltd., London.
Karbhari, V. M., Engineer, M., and Eckel, D. A., II. (1997). “On the durability of composite rehabilitation schemes for concrete: Use of a peel test.” J. Mater. Sci., 32, 147–156.
Ninomiya, K., and Ferry, J. D. (1959). “Some approximate equations useful in the phenomenological treatment of linear viscoelastic data.” J. Colloid Sci., 14, 36–48.
Ocel, J. M., Hartmann, J., and Fuchs, P. (2007). “I-90 seaport portal tunnel partial ceiling collapse investigation: Sustained load behavior of powers fasteners power-past+adhesive anchors.” Federal Highway Administration Turner-Fairbank Highway Research Center Rep., Federal Highway Administration, McLean, Va.
Perera, D. Y. (2004). “Effect of pigmentation on organic coating characteristics.” Prog. Org. Coat., 50, 247–262.
Steckel, G. L., Hawkins, G. F., and Bauer, J. L. (1998). “Environmental durability of composites for seismic retrofit of bridge columns.” Proc., 2nd Int. Conf. on Composites in Infrastructure, H. Saadatmanesh and M. R. Ehsani, eds., Tucson, Ariz.
Williams, M. L., Landel, R. F., and Ferry, J. D. (1955). “The temperature dependence of relaxation mechanisms in amorphous polymers and other glass-forming liquids.” J. Am. Chem. Soc., 77(14), 3701–3707.

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Published In

Go to Journal of Materials in Civil Engineering
Journal of Materials in Civil Engineering
Volume 22Issue 10October 2010
Pages: 1039 - 1046

History

Received: Aug 11, 2008
Accepted: Apr 7, 2010
Published online: Apr 12, 2010
Published in print: Oct 2010

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Authors

Affiliations

Joannie Chin [email protected]
Materials Research Engineer, Building and Fire Research Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899 (corresponding author). E-mail: [email protected]
Aaron Forster [email protected]
Materials Research Engineer, Building and Fire Research Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899. E-mail: [email protected]
Justin Ocel [email protected]
Research Structural Engineer, Turner-Fairbank Hwy Research Center, Federal Hwy Administration, McLean, VA 22101. E-mail: [email protected]
Joseph Hartmann [email protected]
Senior Research Structural Engineer, Turner-Fairbank Hwy Research Center, Federal Hwy Administration, McLean, VA 22101. E-mail: [email protected]
President, Fuchs Consulting, Inc., Leesburg, VA 20176. E-mail: [email protected]
Donald Hunston [email protected]
Research Associate, Building and Fire Research Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899. E-mail: [email protected]

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