Novel 3DOM CeO2 Supported LaFeO3 as an Effective Heterogeneous Fenton Catalyst for Degradation of Methylene Blue
Publication: Journal of Environmental Engineering
Volume 148, Issue 9
Abstract
A three-dimensional ordered macroporous cerium dioxide () was synthesized using a template method combining the sol-gel method, and was synthesized and immobilized on via the sol-gel method combining the impregnation method. The thermogravimetric (TG), scanning electron microscope (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), Brunauer-Emmett-Teller (BET), X-ray photoelectron spectroscopy (XPS), and inductively coupled plasma optical emission spectrometry (ICP-OES) were used to characterize the samples. The catalytic performance and reaction mechanism of the catalyst were studied with methylene blue (MB) as the model pollutant. The MB catalytic behavior showed that the addition of increased the specific surface area of the pristine perovskite. At the same time, there was a synergistic effect between ceria support and perovskite, which significantly improved the activity and stability of the pristine perovskite catalyst. had a wider pH range and higher utilization rate than homogeneous Fenton catalyst. At the same time, in the test range, the leaching concentration of Fe in was less than , which is conducive to reducing the production of iron sludge and greatly controlling the secondary pollution. Furthermore, the catalyst also possessed superior stability of activity and structure in 10 cycles. The results of quenching tests and electron spin resonance (ESR) analyses showed that the catalytic degradation of MB was mainly completed under the action of high-activity . The redox cycle between and is conducive to improving the efficiency of electron transfer, thereby increasing the production efficiency of in the heterogeneous Fenton process. Catalytic degradation of MB approximately conformed to first-order kinetics. The aforementioned results indicate that the novel has great application potential in the field of heterogeneous Fenton treatment of organic pollutants.
Practical Applications
A novel ceria-perovskite composite was successfully prepared in this experiment, and the catalytic performance and reaction mechanism of the catalyst were studied with methylene blue (MB) as the model pollutant. The has higher catalytic activity and stability than prepared by the sol-gel method, and it has higher pH adaptation range and hydrogen peroxide utilization than . At the same time, in the test range, the Fe leaching concentration in is lower than , which significantly reduces the generation of metal sludge and greatly controls the secondary pollution. Furthermore, the catalyst also possessed superior stability of activity and structure in 10 cycles. During the reaction, there were and cycles on the surface of during the reaction process. The two cyclic reactions synergistically initiated the efficient Fenton reaction, resulting in a large number of highly active , thereby realizing the efficient degradation of MB. In summary, can be used as an excellent heterogeneous Fenton catalyst for the treatment of organic pollutants.
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Data Availability Statement
All data, models, and code generated or used during the study appear in the published paper.
Acknowledgments
Fund project: Shijiazhuang Science and Technology Research and Development Program (211240043A).
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Information
Published In
Journal of Environmental Engineering
Volume 148 • Issue 9 • September 2022
Copyright
© 2022 American Society of Civil Engineers.
History
Received: Jan 19, 2022
Accepted: Apr 28, 2022
Published online: Jul 13, 2022
Published in print: Sep 1, 2022
Discussion open until: Dec 13, 2022
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- Engineering fundamentals
- Environmental engineering
- Fourier analysis
- Heterogeneity
- Methodology (by type)
- Pollution
- Radiation
- Structural engineering
- Structural members
- Structural systems
- X rays
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